CN214635137U - Tail gas volatile liquid recovery device - Google Patents

Tail gas volatile liquid recovery device Download PDF

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Publication number
CN214635137U
CN214635137U CN202023007795.9U CN202023007795U CN214635137U CN 214635137 U CN214635137 U CN 214635137U CN 202023007795 U CN202023007795 U CN 202023007795U CN 214635137 U CN214635137 U CN 214635137U
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heat exchange
tail gas
volatile liquid
fixedly connected
tube
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CN202023007795.9U
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宋培剑
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Shandong Qingshui Chemical Co ltd
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Shandong Qingshui Chemical Co ltd
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Abstract

A tail gas volatile liquid recovery device relates to the technical field of recovery devices and comprises a cooling box, wherein a flow divider is rotatably mounted in the cooling box, a cylindrical heat exchange tube which is coiled is fixedly connected in the cooling box, the inner diameter of the cylindrical heat exchange tube is gradually enlarged from top to bottom, an S-shaped heat exchange runner is arranged in the cooling box through an extended heat exchange tube group, and a liquid outlet is formed in the bottom surface of the cooling box; and when the tail gas exchanges heat in the heat exchanger, the tail gas can not exchange heat with the heat exchanger for many times in unit time, and the condensation efficiency of the gas is low.

Description

Tail gas volatile liquid recovery device
Technical Field
The utility model relates to a recovery unit technical field, concretely relates to volatile liquid recovery unit of tail gas.
Background
In the production of chemical plants, the problem of generating tail gas is always a difficult problem to be solved urgently, the tail gas generated by our company is mainly organic gas such as toluene, xylene and the like, if direct emission is not allowed, in the cooling and washing processes of coal gasification and gasification gas of new energy sources such as coal chemical industry, methanol, ether, dimethyl ether and the like and chemical enterprises, because the temperature is reduced and the pressure is higher, a large amount of ammonia gas, carbon dioxide, a small amount of hydrogen sulfide, carbon monoxide, hydrogen and the like are condensed and dissolved in condensate, and a conversion gas condensate rich in ammonia gas and carbon dioxide is formed. Wherein the carbon dioxide content is 10-20g/L, the ammonia gas content is 4-8g/L, the hydrogen sulfide content is 0.1-0.3g/L, the carbon monoxide content is 0.2-0.5g/L, and the hydrogen gas content is 0.02-0.1/L. The conversion condensate belongs to high ammonia nitrogen wastewater and cannot be directly discharged, if the conversion condensate is introduced into a wastewater biochemical treatment system of an enterprise, the ammonia nitrogen load of the biochemical system is directly increased, the wastewater cannot be discharged up to the standard, most enterprises remove ammonia nitrogen and carbon dioxide by adopting a gas stripping ammonia evaporation mode, and qualified liquid after gas stripping is recycled to an enterprise gasification system. Because the temperature of the mixed gas after the gas stripping is condensed is 60-80 ℃, the content and the water content of ammonia gas are higher, a sulfur recovery system and a torch in the later period are frequently flamed out, the normal operation cannot be realized, and new nitrogen oxide pollution is easily formed; in addition, when the mixed gas stripped out from the tower is condensed at the top of the tower, ammonium carbamate and hydrogen sulfide are greatly enriched at the bottom of the condenser, the concentration is greatly increased, the condenser is seriously corroded and cannot be used in less than three months, and therefore most enterprises directly discharge the part of gas (stripping tail gas) to form more serious atmospheric pollution. With the implementation of new environmental protection and energy conservation standards and the increase of supervision, the wastewater and the waste gas must be treated and the comprehensive utilization of resources is realized.
The patent of CN103861313A is disclosed in the prior art, the scheme comprises a tail gas pipeline, a refrigerant coil pipe arranged outside a condensation section of the tail gas pipeline, and a recovery opening arranged at an outlet of the pipeline, wherein the condensation section of the tail gas pipeline forms an angle of 30-75 degrees with the whole tail gas pipeline, and the condensation section of the tail gas pipeline is provided with an induced draft fan. The invention has the advantages and positive effects that: by adopting the technical scheme, the organic gas in the tail gas can be condensed in a condensation mode and recovered; and because the condensation section and the whole tail gas pipeline form a downward 30-75-degree angle, under the action of the induced draft fan, the tail gas continuously enters, and the organic matters condensed into liquid flow to the recovery port under the action of gravity to be recovered. The device simple structure, reasonable in design has reduced the waste of raw materials, can be when effectively getting rid of the toxic gas in the tail gas, reduction in production cost.
However, the device gradually exposes the defects of the technology in production and use, and mainly shows the following aspects:
first, the device has reduced the condensation efficiency to gas because the area of contact of tail gas and heat exchanger is little, and the heat exchange time is short.
Secondly, when the tail gas exchanges heat in the heat exchanger, the tail gas can not exchange heat with the heat exchanger for many times in unit time, so that the condensing efficiency of the gas is lower.
In view of the above, the prior art is obviously inconvenient and disadvantageous in practical use, and needs to be improved.
SUMMERY OF THE UTILITY MODEL
Aiming at the defects in the prior art, the utility model provides a tail gas volatile liquid recovery device, which is used for solving the problems that the contact area between the tail gas and a heat exchanger is small and the heat exchange time is short in the device in the traditional technology; and when the tail gas exchanges heat in the heat exchanger, the tail gas can not exchange heat with the heat exchanger for many times in unit time, and the condensation efficiency of the gas is low.
In order to achieve the above object, the utility model provides a following technical scheme:
the utility model provides a volatile liquid recovery unit of tail gas, includes the cooler bin, the shunt is installed to the cooler bin internal rotation, the rigid coupling has the tube-shape heat exchange tube that coils the setting in the cooler bin, the internal diameter of tube-shape heat exchange tube is the formula setting that gradually expands by last under to, still arrange through extending the heat exchange tube in the cooler bin and be S-shaped heat transfer runner, the leakage fluid dram has been seted up on the bottom surface of cooler bin.
As an optimized scheme, the extension heat exchange tube is communicated with the cylindrical heat exchange tube, one end connected with the extension heat exchange tube is an inlet, and the other end connected with the cylindrical heat exchange tube is an outlet.
As an optimized scheme, the extension heat exchange tube comprises a first heat exchange fin and a second heat exchange fin which are sequentially and alternately arranged in parallel, the upper end part of the first heat exchange fin is fixedly connected with the inner top surface of the cooling box, the lower end part of the second heat exchange fin is fixedly connected with the inner bottom surface of the cooling box, and an S-shaped heat exchange flow passage is formed between the lower end part of the first heat exchange fin and the upper end part of the second heat exchange fin.
As an optimized scheme, the first heat exchange plate and the second heat exchange plate respectively comprise S-shaped roundabout heat exchange tubes, and the first heat exchange plate and the second heat exchange plate are communicated and integrally formed.
As an optimized scheme, the flow divider comprises a rotating drum vertically and rotatably mounted on the top surface of the cooling tank, a lower port of the rotating drum is arranged in a sealed mode, splitter blades are arranged on the peripheral wall, close to the lower port, of the rotating drum in a surrounding mode, and splitter holes are further formed in the area, between the adjacent splitter blades, of the peripheral wall of the rotating drum.
As an optimized scheme, a baffle disc is further coaxially sleeved and fixedly connected to the rotating drum, and the lower surface of the baffle disc is fixedly connected with the upper end portions of the plurality of splitter blades.
As an optimized scheme, the baffle disc is an arc-shaped disc, and the convex surface of the arc-shaped disc is arranged upwards.
In an optimized scheme, a gear is further fixedly connected to the portion, above the top surface of the cooling box, of the rotary drum, and a driving machine for driving the gear to rotate is further fixedly connected to the top surface of the cooling box.
As an optimized scheme, an inlet flange cylinder is further rotatably inserted into the upper end opening of the rotary cylinder, and a sealing ring is arranged between the outer wall of the inlet flange cylinder and the inner wall of the rotary cylinder.
As an optimized scheme, the liquid outlet is positioned below the cylindrical heat exchange tube.
As an optimized scheme, a guide cylinder which is arranged in a downward tapered mode is fixedly connected to the edge of the liquid outlet, and a discharge flange cylinder is fixedly connected to the lower port of the guide cylinder.
Compared with the prior art, the beneficial effects of the utility model are that:
the rotary cooling box is characterized in that force is applied to tail gas entering the cooling box through the rotationally arranged splitter blades, the tail gas can rapidly flow in the cylindrical heat exchange tube, the tail gas can rapidly exchange heat with the cylindrical heat exchange tube, gas in the tail gas can be condensed, the gas primarily condensed by the cylindrical heat exchange tube can enter the S-shaped heat exchange flow channel again along with flowing, secondary condensation of the gas is realized by the aid of the extension heat exchange tube, the gas is further condensed, the contact area of the tail gas and the heat exchange tube is increased, and the condensation efficiency is improved; simple and convenient operation and control, easy large-scale manufacture and installation and wide application range.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the embodiments or the technical solutions in the prior art will be briefly described below. Throughout the drawings, like elements or portions are generally identified by like reference numerals. In the drawings, elements or portions are not necessarily drawn to scale.
Fig. 1 is a schematic structural view of the present invention;
in the figure: 1-a cooling box; 2-cylindrical heat exchange tubes; 3-a first heat exchanger fin; 4-a second heat exchange fin; 5-an inlet; 6-an outlet; 7-a liquid discharge port; 8-a guide cylinder; 9-discharge flange cylinder; 10-a drum; 11-a shunt hole; 12-splitter blades; 13-a catch disc; 14-entering a flange cylinder; 15-gear; 16-a driver; and 17-a smoke exhaust tube.
Detailed Description
Embodiments of the present invention will be described in detail below with reference to the accompanying drawings. The following examples are only for illustrating the technical solutions of the present invention more clearly, and therefore are only examples, and the protection scope of the present invention is not limited thereby.
As shown in fig. 1, the tail gas volatile liquid recovery device comprises a cooling box 1, a flow divider is installed in the cooling box 1 in a rotating mode, a cylindrical heat exchange tube 2 which is arranged in a coiling mode is fixedly connected in the cooling box 1, the inner diameter of the cylindrical heat exchange tube 2 is gradually enlarged from top to bottom, an S-shaped heat exchange flow channel is arranged in the cooling box 1 through an extension heat exchange tube, and a liquid discharge port 7 is formed in the bottom surface of the cooling box 1.
The extension heat exchange tube is communicated with the cylindrical heat exchange tube 2, one end connected with the extension heat exchange tube is an inlet 5, one end connected with the cylindrical heat exchange tube 2 is an outlet 6, wherein the extension heat exchange tube and the cylindrical heat exchange tube 2 are also manufactured by integrally molding the heat exchange tubes,
the extension heat exchange tube comprises a first heat exchange fin 3 and a second heat exchange fin 4 which are sequentially arranged in parallel in an alternating mode, the upper end portion of the first heat exchange fin 3 is fixedly connected with the inner top surface of the cooling box 1, the lower end portion of the second heat exchange fin 4 is fixedly connected with the inner bottom surface of the cooling box 1, and an S-shaped heat exchange flow channel is formed between the lower end portion of the first heat exchange fin 3 and the upper end portion of the second heat exchange fin 4.
The first heat exchange fins 3 and the second heat exchange fins 4 are provided with a plurality of groups according to requirements.
The first heat exchange fins 3 and the second heat exchange fins 4 are composed of S-shaped heat exchange tubes in a roundabout mode, gaps are formed among the S-shaped heat exchange tubes in the roundabout mode, and the first heat exchange fins 3 are communicated with the second heat exchange fins 4 and are integrally formed.
The shunt includes that vertical rotation installs the rotary drum 10 on 1 top surfaces of cooler bin, and the lower port of rotary drum 10 seals the setting, and the rotary drum 10 encloses on being close to the perisporium of lower port and is equipped with splitter blade 12, and the region that the perisporium of rotary drum 10 is in between adjacent splitter blade 12 has still seted up reposition of redundant personnel hole 11, realizes entering into the tail gas in the cooler bin 1 and increases its flow velocity, increase and the heat exchange tube between contact efficiency.
The rotating drum 10 is further coaxially sleeved and fixedly connected with a baffle disc 13, and the lower surface of the baffle disc 13 is fixedly connected with the upper end parts of the plurality of splitter blades 12, so that the flow direction of the tail gas is limited.
The baffle disc 13 is an arc disc, and the convex surface of the arc disc is arranged upwards.
The portion of the drum 10 above the top surface of the cooling box 1 is further fixedly connected with a gear 15, and the top surface of the cooling box 1 is further fixedly connected with a driving machine 16 for driving the gear 15 to rotate.
The upper port of the rotary drum 10 is also rotatably inserted with an inlet flange cylinder 14, a sealing ring is arranged between the outer wall of the inlet flange cylinder 14 and the inner wall of the rotary drum 10 to realize sealing arrangement, and the inlet flange cylinder 14 and the rotary drum 10 are rotatably arranged to prevent the inlet flange cylinder 14 from rotating when the rotary drum 10 rotates.
The liquid outlet 7 is positioned below the cylindrical heat exchange tube 2.
The edge of the liquid outlet 7 is fixedly connected with a guide tube 8 which is arranged in a downward tapered mode, and the lower port of the guide tube 8 is fixedly connected with a discharge flange tube 9, so that the cooled liquid is discharged today.
The side wall of the cooling box 1 is also fixedly connected with a smoke exhaust 17, and the smoke exhaust 17 is close to the extension heat exchange tube.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; although the present invention has been described in detail with reference to the foregoing embodiments, it should be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; such modifications and substitutions do not substantially depart from the scope of the embodiments of the present invention, and are intended to be covered by the claims and the specification.

Claims (10)

1. The utility model provides a volatile liquid recovery unit of tail gas which characterized in that: including cooler bin (1), the shunt is installed to cooler bin (1) internal rotation, the rigid coupling has tube-shape heat exchange tube (2) that coil the setting in cooler bin (1), the internal diameter of tube-shape heat exchange tube (2) is the formula setting of gradually expanding by last under to, it is S-shaped heat transfer runner still to arrange through extending the heat exchange tube in cooler bin (1), leakage fluid dram (7) have been seted up on the bottom surface of cooler bin (1).
2. The recovery device for volatile liquid in tail gas as claimed in claim 1, wherein: the extension heat exchange tube is communicated with the cylindrical heat exchange tube (2), one end of the extension heat exchange tube is an inlet (5), and the other end of the extension heat exchange tube is an outlet (6).
3. The recovery device for volatile liquid in tail gas as claimed in claim 2, wherein: the extension heat exchange tube comprises a first heat exchange fin (3) and a second heat exchange fin (4) which are sequentially and alternately arranged in parallel, the upper end portion of the first heat exchange fin (3) is fixedly connected with the inner top surface of the cooling box (1), the lower end portion of the second heat exchange fin (4) is fixedly connected with the inner bottom surface of the cooling box (1), and the S-shaped heat exchange flow channel is formed between the lower end portion of the first heat exchange fin (3) and the upper end portion of the second heat exchange fin (4).
4. The recycling device for volatile liquid in tail gas of claim 3, wherein: the heat exchanger is characterized in that the first heat exchange fins (3) and the second heat exchange fins (4) are composed of S-shaped heat exchange tubes arranged in a roundabout mode, and the first heat exchange fins (3) are communicated with the second heat exchange fins (4) and are integrally formed.
5. The recovery device for volatile liquid in tail gas as claimed in claim 1, wherein: the flow divider comprises a rotating drum (10) vertically and rotatably mounted on the top surface of the cooling box (1), the lower port of the rotating drum (10) is sealed, splitter blades (12) are arranged on the peripheral wall, close to the lower port, of the rotating drum (10), and splitter holes (11) are further formed in the region, between the adjacent splitter blades (12), of the peripheral wall of the rotating drum (10).
6. The recycling device for volatile liquid in tail gas of claim 5, wherein: the rotating drum (10) is further coaxially sleeved and fixedly connected with a baffle disc (13), and the lower surface of the baffle disc (13) is fixedly connected with the upper end parts of the plurality of splitter blades (12).
7. The recycling device for volatile liquid in tail gas of claim 6, wherein: the baffle disc (13) is an arc disc, and the convex surface of the arc disc is arranged upwards.
8. The recycling device for volatile liquid in tail gas of claim 7, wherein: a gear (15) is fixedly connected to the part of the rotating cylinder (10) above the top surface of the cooling box (1), and a driving machine (16) for driving the gear (15) to rotate is fixedly connected to the top surface of the cooling box (1).
9. The recycling device for volatile liquid in tail gas of claim 8, wherein: an inlet flange cylinder (14) is further rotatably inserted into the upper port of the rotary cylinder (10), and a sealing ring is arranged between the outer wall of the inlet flange cylinder (14) and the inner wall of the rotary cylinder (10).
10. The recovery device for volatile liquid in tail gas as claimed in claim 1, wherein: the liquid discharge port (7) is located below the cylindrical heat exchange tube (2), a guide tube (8) which is arranged in a downward tapered mode is fixedly connected to the edge of the liquid discharge port (7), and a discharge flange tube (9) is fixedly connected to the lower end opening of the guide tube (8).
CN202023007795.9U 2020-12-15 2020-12-15 Tail gas volatile liquid recovery device Active CN214635137U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202023007795.9U CN214635137U (en) 2020-12-15 2020-12-15 Tail gas volatile liquid recovery device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202023007795.9U CN214635137U (en) 2020-12-15 2020-12-15 Tail gas volatile liquid recovery device

Publications (1)

Publication Number Publication Date
CN214635137U true CN214635137U (en) 2021-11-09

Family

ID=78499464

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202023007795.9U Active CN214635137U (en) 2020-12-15 2020-12-15 Tail gas volatile liquid recovery device

Country Status (1)

Country Link
CN (1) CN214635137U (en)

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