CN214571629U

CN214571629U - Device for purifying tobias acid from tobias acid waste liquid

Info

Publication number: CN214571629U
Application number: CN202120292530.3U
Authority: CN
Inventors: 焦国富; 王万峰; 郭强; 祁恩东
Original assignee: Gansu Yonghong Dyeing Chemical Co ltd
Current assignee: Gansu Yonghong Dyeing Chemical Co ltd
Priority date: 2021-02-02
Filing date: 2021-02-02
Publication date: 2021-11-02
Anticipated expiration: 2031-02-02

Abstract

The utility model belongs to the technical field of purification of tobias acid, in particular to a device for purifying tobias acid from waste liquid of tobias acid, which comprises a bottom plate, wherein two supporting plates are fixedly arranged on the upper end surface of the bottom plate, a box body is fixedly arranged on the upper end surface of the two supporting plates, a filter cylinder is fixedly arranged at the left end of the upper end surface inside the box body, a feed inlet is arranged on the upper end surface of the filter cylinder, the upper end of the feed inlet penetrates through the box body and extends to the upper part of the box body, a filter plate is arranged inside the filter cylinder, the bottom end surface of the filter cylinder is communicated with a connecting pipe, so that when a motor drives a sliding cover to rotate along a sliding chute, a stirring rod automatically transmits and does circular motion along the stirring cylinder to stir the waste liquid of tobias acid at each corner in the stirring cylinder, thereby achieving the effect of uniform stirring, and the waste liquid of tobias acid in the stirring cylinder is heated by the two heating plates, the activity of the solution is increased, thereby improving the mixing efficiency and facilitating the extraction.

Description

Device for purifying tobias acid from tobias acid waste liquid

Technical Field

The utility model relates to an acid purification technical field of tobias, concretely relates to a device that is used for acid waste liquid purification of tobias acid.

Background

Tobias acid, white needle crystal, slightly soluble in cold water, soluble in hot water, and slightly soluble in ethanol and ether; the product is an azo dye intermediate and is used for preparing dyes such AS J acid, gamma acid, naphthol AS-SW, reactive red K-1613, organic mauve, lithol mauve and lithol scarlet.

The existing device for purifying the tobias acid from the tobias acid waste liquid has insufficient mixing of the extracting agent and the waste liquid in the purification process, so that the extraction effect is not good enough, and the final purification effect is not good.

SUMMERY OF THE UTILITY MODEL

For solving the problem that proposes among the above-mentioned background art, the utility model provides a device for tobias acid waste liquid purification tobias acid has the tobias acid waste liquid that makes each corner in the churn and stirs, reaches the effect of stirring, and two hot plates heat the tobias acid waste liquid in the churn, increase the activity of solution to improve mixing efficiency's characteristics.

In order to achieve the above object, the utility model provides a following technical scheme: a device for purifying tobias acid from tobias acid waste liquid comprises a bottom plate, wherein two support plates are fixedly mounted on the upper end surface of the bottom plate, a box body is fixedly mounted on the upper end surfaces of the two support plates, a filter cylinder is fixedly mounted at the left end of the upper end surface in the box body, a feed inlet is mounted on the upper end surface of the filter cylinder, the upper end of the feed inlet penetrates through the box body and extends to the upper part of the box body, a filter plate is mounted in the filter cylinder, a connecting pipe is communicated with the bottom end surface of the filter cylinder, a stirring cylinder is communicated with one end of the connecting pipe, a motor is arranged on the right side of the filter cylinder, the motor is fixedly mounted on the top end surface in the box body, a first gear is fixedly sleeved at the output end of the motor, a second gear is meshed with the outer side wall of the first gear, a stirring rod is fixedly mounted on the bottom end surface of the second gear, and a sliding cover is arranged on the upper end surface of the stirring cylinder, the bottom of puddler runs through the sliding closure and extends to the inside of churn, the bottom face intercommunication of churn has the discharging pipe, the solenoid valve is installed to the lateral wall of discharging pipe, the other end of discharging pipe runs through the bottom face and the intercommunication of box and has centrifuge, the discharging pipe extends to the lateral wall of box below and installs the solenoid valve, centrifuge's the left and right sides all communicates there is the fluid-discharge tube, two the electrovalve is all installed to the lateral wall of fluid-discharge tube, the right side wall fixed mounting of box has the cutting ferrule, the inside joint of cutting ferrule has the medicament bottle.

In order to make the stable rotation of sliding closure, as the utility model relates to a device that is used for acid waste liquid purification of tobias acid is preferred, the output of motor and the up end fixed connection of sliding closure, the spout has been seted up at the top of churn inside wall, the lateral wall and the spout sliding connection of sliding closure.

In order to increase the activity of solution, the stirring of being convenient for, as the utility model relates to a device that is used for tobias acid waste liquid purification tobias acid is preferred, the equal fixed mounting in both ends has the hot plate about the churn lateral wall.

In order to be convenient for discharge the filter residue through the scum pipe, conduct the utility model relates to a device that is used for the sour waste liquid purification of tobias acid is preferred, the left side wall intercommunication of cartridge filter has the scum pipe, the scum pipe is located the top of filter.

In order to facilitate adding the inside to the churn with the extractant in the medicament bottle, conduct the utility model relates to a device that is used for tobias acid waste liquid purification tobias acid is preferred, the bottom intercommunication of medicament bottle has the liquid medicine pipe, the other end of liquid medicine pipe runs through the right side wall of box and extends to the inside of box and communicate with the churn.

In order to facilitate passing through each part work of control panel control, thereby convenient operation, conduct the utility model relates to a device that is used for tuo shi acid waste liquid purification tuo shi acid is preferred, the right side wall fixed mounting of box has control panel, equal and the control panel electric connection of motor, two hot plates, solenoid valve and two electric valves.

Compared with the prior art, the beneficial effects of the utility model are that:

1. the device for purifying the tobias acid in the tobias acid waste liquid comprises a feed inlet, a filter plate, a filter tube, a liquid discharge tube, a slide cover, a first gear, a second gear, a stirring rod, a liquid discharge tube, a liquid level sensor, a liquid level controller and a liquid level controller, wherein the feed inlet is used for adding the tobias acid waste liquid into the filter tube, the filter plate is used for filtering impurities in the tobias acid waste liquid, so that the tobias acid in the waste liquid can be purified, the filtered filter residue is discharged through the liquid discharge tube, the tobias acid waste liquid falls into the stirring tube through the connection tube, an extracting agent is added into the liquid level sensor, so that the extracting agent flows into the stirring tube through the liquid level sensor, the liquid level sensor is used for driving the slide cover and the slide cover to drive the slide cover and the first gear to rotate through the first gear, at the same time, the slide cover to drive the second gear and the stirring rod to rotate along the slide cover to rotate along the sliding chute, so that the slide cover to make the stirring tube to automatically transmit and to stir the liquid along the stirring tube to stir the liquid level sensor, the activity of the solution is increased, the mixing efficiency is improved, then the solution is kept stand to perform extraction operation, after extraction is completed, the electromagnetic valve is opened, so that the tobias acid waste liquid in the mixing drum flows into the centrifuge through the discharge pipe, the centrifuge is started to perform solid-liquid separation on the tobias acid waste liquid, and the waste liquid and tobias acid crystals are collected by respectively opening two electric valves on two liquid discharge pipes, so that the purification operation is completed.

In conclusion, this kind of a device for tobias acid waste liquid purification tobias acid is when driving the sliding closure through the motor and rotating along the spout for the puddler is from passing and be circular motion along the churn, stirs the tobias acid waste liquid of each corner in the churn, thereby reaches the effect of stirring, and two hot plates heat the tobias acid waste liquid in the churn, increase the activity of solution, thereby improve mixing efficiency, the extraction of being convenient for.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention. In the drawings:

FIG. 1 is a structural diagram of a device for purifying tobias acid from tobias acid waste liquid;

FIG. 2 is a view showing a structure of the chute of FIG. 1 according to the present invention;

fig. 3 is a right structural view of fig. 1 according to the present invention.

In the figure, 1, a bottom plate; 101. a support plate; 2. a box body; 201. a control panel; 3. a filter cartridge; 301. a feed inlet; 302. a filter plate; 303. a slag discharge pipe; 304. a connecting pipe; 4. a motor; 401. a first gear; 402. A second gear; 403. a stirring rod; 5. a mixing drum; 501. a chute; 502. a sliding cover; 503. heating plates; 6. a discharge pipe; 601. an electromagnetic valve; 7. a centrifuge; 701. a liquid discharge pipe; 702. an electric valve; 8. a card sleeve; 9. a medicament bottle; 901. a liquid medicine tube.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more clearly understood, the present invention is further described in detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.

In the description of the present invention, it is to be understood that the terms "length", "width", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on those shown in the drawings, and are merely for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention. In addition, in the description of the present invention, "a plurality" means two or more unless specifically limited otherwise.

Referring to fig. 1-3, the present invention provides the following technical solutions: a device for purifying tobias acid from tobias acid waste liquid comprises a base plate 1, two support plates 101 are fixedly mounted on the upper end face of the base plate 1, a box body 2 is fixedly mounted on the upper end faces of the two support plates 101, a filter cylinder 3 is fixedly mounted at the left end of the upper end face inside the box body 2, a feed inlet 301 is mounted on the upper end face of the filter cylinder 3, the upper end of the feed inlet 301 penetrates through the box body 2 and extends to the upper side of the box body 2, a filter plate 302 is mounted inside the filter cylinder 3, a connecting pipe 304 is communicated with the bottom end face of the filter cylinder 3, one end of the connecting pipe 304 is communicated with a stirring cylinder 5, a motor 4 is arranged on the right side of the filter cylinder 3, the motor 4 is fixedly mounted on the top end face inside the box body 2, a first gear 401 is fixedly sleeved on the output end of the motor 4, a second gear 402 is engaged with the outer side wall of the first gear 401, and a stirring rod 403 is fixedly mounted on the bottom end face of the second gear 402, the up end of churn 5 is provided with sliding closure 502, the bottom of puddler 403 runs through sliding closure 502 and extends to the inside of churn 5, the bottom face intercommunication of churn 5 has discharging pipe 6, solenoid valve 601 is installed to the lateral wall of discharging pipe 6, the other end of discharging pipe 6 runs through the bottom face and the intercommunication of box 2 has centrifuge 7, discharging pipe 6 extends to the lateral wall of box 2 below and installs the left and right sides that solenoid valve 601 centrifuge 7 all communicates there is the fluid-discharge tube 701, electrovalve 702 is all installed to the lateral wall of two fluid-discharge tubes 701, the right side wall fixed mounting of box 2 has cutting ferrule 8, the inside joint of cutting ferrule 8 has medicament bottle 9.

In this embodiment: adding tobias acid waste liquid into the interior of the filter cylinder 3 through the feed inlet 301, filtering impurities in the tobias acid waste liquid by the filter plate 302, so as to purify tobias acid in the waste liquid, then dropping the tobias acid waste liquid into the interior of the mixing drum 5 through the connecting pipe 304, adding an extractant into the liquid medicine pipe 901, so that the extractant flows into the interior of the mixing drum 5 through the liquid medicine pipe 901, starting the motor 4, driving the sliding cover 502 and the first gear 401 to rotate by the motor 4, so that the second gear 402 and the stirring rod 403 are driven to rotate by the first gear 401, at this time, while the sliding cover 502 rotates along the sliding groove 501, the stirring rod 403 is self-transmitted and makes circular motion along the mixing drum 5, so as to stir the tobias acid waste liquid at each corner in the mixing drum 5, thereby achieving the effect of uniform stirring, then standing for extraction operation, after extraction is completed, by opening the electromagnetic valve 601, the tobias acid waste liquid in the mixing drum 5 flows into the centrifuge 7 through the discharge pipe 6, the centrifuge 7 is started to perform solid-liquid separation on the tobias acid waste liquid, and the waste liquid and tobias acid crystals are collected by respectively opening the two electrovalves 702 on the two liquid discharge pipes 701, so that the purification operation is completed.

As a technical optimization scheme of the utility model, motor 4's output and sliding closure 502's up end fixed connection, spout 501, sliding closure 502's lateral wall and spout 501 sliding connection have been seted up at the top of 5 inside walls of churn.

In this embodiment: by starting the motor 4, the motor 4 drives the sliding cover 502 to rotate, so that the sliding cover 502 rotates along the sliding groove 501, and the sliding groove 501 limits the sliding cover 502, so that the sliding cover 502 rotates stably.

As a technical optimization scheme of the utility model, the equal fixed mounting in both ends has hot plate 503 about 5 lateral walls of churn.

In this embodiment: by arranging the two heating plates 503, the two heating plates 503 heat the tobias acid waste liquid in the stirring cylinder 5, so that the activity of the solution is increased, and the stirring is convenient.

As a technical optimization scheme of the utility model, the left side wall intercommunication of cartridge filter 3 has row's sediment pipe 303, and row's sediment pipe 303 is located the top of filter 302.

In this embodiment: through setting up row sediment pipe 303, filter 302 filters the back with the impurity in the acid waste liquid of tobias, is convenient for discharge the filter residue through row sediment pipe 303.

As a technical optimization scheme of the utility model, the bottom intercommunication of medicament bottle 9 has medicine liquid pipe 901, and the other end of medicine liquid pipe 901 runs through the right side wall of box 2 and extends to the inside of box 2 and communicate with churn 5.

In this embodiment: by arranging the liquid medicine tube 901, the extractant in the medicine bottle 9 can be conveniently added into the stirring cylinder 5.

As a technical optimization scheme of the utility model, the right side wall fixed mounting of box 2 has control panel 201, motor 4, two hot plates 503, solenoid valve 601 and two electrovalves 702 all with control panel 201 electric connection.

In this embodiment: by installing the control panel 201, the control panel 201 is convenient to control the work of each component, and the operation is convenient.

The utility model discloses a theory of operation and use flow: firstly, the tobias acid waste liquid is added into the interior of the filter cylinder 3 through the feed inlet 301, the filter plate 302 filters impurities in the tobias acid waste liquid, so as to purify the tobias acid in the waste liquid, the filtered residue is discharged through the residue discharge pipe 303, then the tobias acid waste liquid falls into the interior of the mixing drum 5 through the connecting pipe 304, the extractant is added into the liquid medicine pipe 901, so that the extractant flows into the interior of the mixing drum 5 through the liquid medicine pipe 901, the motor 4 is started, the motor 4 drives the sliding cover 502 and the first gear 401 to rotate, so that the first gear 401 drives the second gear 402 and the mixing rod 403 to rotate, at this time, the sliding cover 502 rotates along the sliding chute 501, so that the mixing rod 403 is self-transmitted and does circular motion along the mixing drum 5, the tobias acid waste liquid at each corner in the mixing drum 5 is mixed, thereby achieving the effect of uniform mixing, and the tobias acid waste liquid in the mixing drum 5 is heated through the two heating plates 503, the activity of the solution is increased, the mixing efficiency is improved, the extraction operation is carried out by two standing operations, after the extraction is finished, the electromagnetic valve 601 is opened, so that the tobias acid waste liquid in the mixing drum 5 flows into the centrifuge 7 through the discharge pipe 6, the centrifuge 7 is started to carry out solid-liquid separation on the tobias acid waste liquid, and the waste liquid and tobias acid crystals are collected by respectively opening the two electric valves 702 on the two discharge pipes 701, thereby finishing the purification operation.

The above description is only exemplary of the present invention and should not be construed as limiting the present invention, and any modifications, equivalents and improvements made within the spirit and principles of the present invention are intended to be included within the scope of the present invention.

Claims

1. The utility model provides a device that is used for tobias acid waste liquid purification tobias acid, includes bottom plate (1), its characterized in that: the upper end face of the bottom plate (1) is fixedly provided with two supporting plates (101), the upper end faces of the two supporting plates (101) are fixedly provided with a box body (2), the left end of the upper end face inside the box body (2) is fixedly provided with a filter cartridge (3), the upper end face of the filter cartridge (3) is provided with a feed inlet (301), the upper end of the feed inlet (301) penetrates through the box body (2) and extends to the upper part of the box body (2), the inside of the filter cartridge (3) is provided with a filter plate (302), the bottom end face of the filter cartridge (3) is communicated with a connecting pipe (304), one end of the connecting pipe (304) is communicated with a stirring cylinder (5), the right side of the filter cartridge (3) is provided with a motor (4), the motor (4) is fixedly arranged on the top end face inside the box body (2), and the output end of the motor (4) is fixedly sleeved with a first gear (401), the outer side wall of the first gear (401) is connected with a second gear (402) in a meshing manner, a stirring rod (403) is fixedly installed on the bottom end face of the second gear (402), a sliding cover (502) is arranged on the upper end face of the stirring drum (5), the bottom of the stirring rod (403) penetrates through the sliding cover (502) and extends into the stirring drum (5), a discharge pipe (6) is communicated with the bottom end face of the stirring drum (5), the other end of the discharge pipe (6) penetrates through the bottom end face of the box body (2) and is communicated with a centrifugal machine (7), an electromagnetic valve (601) is installed on the outer side wall, extending to the lower portion of the box body (2), of the discharge pipe (6), liquid discharge pipes (701) are communicated with the left side and the right side of the centrifugal machine (7), electric valves (702) are installed on the outer side walls of the two liquid discharge pipes (701), and a clamping sleeve (8) is fixedly installed on the right side wall of the box body (2), the inner part of the cutting sleeve (8) is clamped with a medicament bottle (9).

2. The apparatus for purifying tobias acid from tobias acid waste liquid as claimed in claim 1, wherein: the output end of the motor (4) is fixedly connected with the upper end face of the sliding cover (502), the top of the inner side wall of the mixing drum (5) is provided with a sliding groove (501), and the outer side wall of the sliding cover (502) is in sliding connection with the sliding groove (501).

3. The apparatus for purifying tobias acid from tobias acid waste liquid as claimed in claim 2, wherein: heating plates (503) are fixedly mounted at the left end and the right end of the outer side wall of the mixing drum (5).

4. The apparatus for purifying tobias acid from tobias acid waste liquid as claimed in claim 1, wherein: the left side wall intercommunication of cartridge filter (3) has row sediment pipe (303), row sediment pipe (303) are located the top of filter (302).

5. The apparatus for purifying tobias acid from tobias acid waste liquid as claimed in claim 1, wherein: the bottom of the medicine bottle (9) is communicated with a medicine liquid pipe (901), and the other end of the medicine liquid pipe (901) penetrates through the right side wall of the box body (2), extends into the box body (2) and is communicated with the stirring drum (5).

6. The apparatus for purifying tobias acid from tobias acid waste liquid as claimed in claim 3, wherein: the right side wall fixed mounting of box (2) has control panel (201), motor (4), two hot plate (503), solenoid valve (601) and two electrovalves (702) all with control panel (201) electric connection.