CN214486902U - Novel individual layer reation kettle - Google Patents
Novel individual layer reation kettle Download PDFInfo
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- CN214486902U CN214486902U CN202120624183.XU CN202120624183U CN214486902U CN 214486902 U CN214486902 U CN 214486902U CN 202120624183 U CN202120624183 U CN 202120624183U CN 214486902 U CN214486902 U CN 214486902U
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- reaction kettle
- bottle
- fixing piece
- heating device
- reflux
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Abstract
The utility model relates to a novel single-layer reaction kettle, which comprises a bracket and a heating system, wherein the lower end of the bracket is provided with a heating device, and a resistance heating pipe is arranged inside the heating device; the support is fixedly provided with a bottle clamping ring, the bottle clamping ring is connected with a reaction kettle body, and the upper end of the reaction kettle body is provided with a reaction kettle cover; the stirring system is characterized in that a lower fixing piece and an upper fixing piece are arranged at the upper end of the reaction kettle cover, a stirring rod is clamped between the lower fixing piece and the upper fixing piece, the stirring rod is vertically arranged, and the stirring rod is connected with a motor; the reaction kettle cover is connected with a reflux bottle, and the reflux bottle is connected with a condenser; the reaction kettle cover is connected with a constant pressure funnel through a standard opening; the side surface of the heating device is provided with an electric cabinet; the utility model has the advantages of high production efficiency, high reaction efficiency and reasonable structure.
Description
Technical Field
The utility model belongs to the technical field of reation kettle, concretely relates to novel individual layer reation kettle.
Background
The glass reaction kettle is an accurate instrument which can maintain homogeneous stirring, material concentration, vacuum reaction, transparent visual inspection and control of evaporation and reflux of reaction solution, temperature zone and temperature point under the conditions of high temperature, medium temperature and low temperature.
At present, when a conducting medium of a glass reaction kettle adopted in the market is water, a temperature zone is between room temperature and 97 ℃; when the conducting medium is oil, the temperature zone is between room temperature and 174 ℃; when the conducting medium is ethanol, the temperature zone is at room temperature (-20 ℃); the prior art structure is comparatively complicated, and can't accelerate reaction efficiency, leads to production efficiency low.
SUMMERY OF THE UTILITY MODEL
The utility model aims at overcoming the defects of the prior art and providing a novel single-layer reaction kettle with high production efficiency, high reaction efficiency and reasonable structure.
The purpose of the utility model is realized like this: a novel single-layer reaction kettle comprises a bracket and a reaction kettle body
The heating system is characterized in that a heating device is arranged at the lower end of the bracket, and a resistance heating pipe is arranged in the heating device;
the support is fixedly provided with a bottle clamping ring, the bottle clamping ring is connected with a reaction kettle body, and the upper end of the reaction kettle body is provided with a reaction kettle cover;
the stirring system is characterized in that a lower fixing piece and an upper fixing piece are arranged at the upper end of the reaction kettle cover, a stirring rod is clamped between the lower fixing piece and the upper fixing piece, the stirring rod is vertically arranged, and the stirring rod is connected with a motor;
the reaction kettle cover is connected with a reflux bottle, and the reflux bottle is connected with a condenser;
the reaction kettle cover is connected with a constant pressure funnel through a standard opening;
and the side surface of the heating device is provided with an electric cabinet.
And a feeding piston is also arranged on the reaction kettle cover.
The bottle clamping ring is arranged on the upper portion of the reaction kettle body and used for clamping the reaction kettle body.
The lower extreme of backward flow bottle is provided with backward flow bottle trunnion ring for support backward flow bottle.
The reflux bottle supporting ring is fixedly connected with the support through a rod.
The motor is connected with a support frame, and the support frame is fixed on the support through a cross angle.
And a discharge valve is arranged at the lower end of the reaction kettle body.
The utility model has the advantages that: the utility model has the advantages of the glass part all adopts high-quality borosilicate glass, possess good physics, chemical properties. The stirring motor adopts a speed reducing motor, so that the stirring motor is stable in operation, large in torque, free of sparks and long in service life; the PTFE component is sealed, a special technology is adopted, good vacuum degree can be guaranteed, and the service life is long. The whole structure is stable and can move integrally. The PTFE emptying valve with the minimum or no dead angle can effectively reduce the stirring dead angle. The kettle body and the interface can be customized according to the requirements of customers; the matched product can be produced according to the requirements of customers no matter refrigeration or heating; the overall structure science, novelty, practicality, pleasing to the eye has good practicality, and other beneficial effects are specified in detail in the embodiment.
Drawings
Fig. 1 is a front view of the novel single-layer reaction kettle of the present invention.
Fig. 2 is a perspective view of fig. 1.
Fig. 3 is a perspective view of another perspective view of fig. 1.
Fig. 4 is a sectional view of the central vertical plane of fig. 1.
In the figure: 1. a heating device; 2. a support; 3. an electric cabinet; 4. a reaction kettle body; 5. clamping the bottle ring; 6. a reaction kettle cover; 7. a reflux bottle; 8. a reflux bottle backing ring; 9. a condenser; 10. a charging piston; 11. a cross corner; 12. a support frame; 13. a motor; 14. a constant pressure funnel; 15. an upper fixing member; 16. a lower fixing member; 17. a stirring rod; 18. a discharge valve.
Detailed Description
The technical solution in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, rather than all embodiments, and all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention based on the embodiments of the present invention.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs, and the terms used herein are for the purpose of describing particular embodiments only and are not intended to be limiting of the invention, and terms such as "and/or" as used herein include any and all combinations of one or more of the associated listed items; furthermore, the technical features mentioned in the different embodiments of the invention described below can be combined with each other as long as they do not conflict with each other.
Examples
As shown in fig. 1-4, a novel single-layer reaction kettle comprises a support 2 and a heating system, wherein a heating device 1 is arranged at the lower end of the support 2, and a resistance heating pipe is arranged inside the heating device 1; a support system, wherein a bottle clamping ring 5 is fixedly arranged on the support 2, the bottle clamping ring 5 is connected with a reaction kettle body 4, and a reaction kettle cover 6 is arranged at the upper end of the reaction kettle body 4; the reaction kettle comprises a stirring system, wherein a lower fixing piece 16 and an upper fixing piece 15 are arranged at the upper end of the reaction kettle cover 6, a stirring rod 17 is clamped between the lower fixing piece 16 and the upper fixing piece 15, the stirring rod 17 is vertically arranged, and the stirring rod 17 is connected with a motor 13; the reaction kettle cover 6 is connected with a reflux bottle 7, and the reflux bottle 7 is connected with a condenser 9; the reaction kettle cover 6 is connected with a constant pressure funnel 14 through a standard opening; and the side surface of the heating device 1 is provided with an electric cabinet 3.
Further, a feeding piston 10 is further arranged on the reaction kettle cover 6.
Further, the bottle clamping ring 5 is arranged on the upper portion of the reaction kettle body 4 and used for clamping the reaction kettle body 4.
Furthermore, the lower end of the reflux bottle 7 is provided with a reflux bottle 7 support ring for supporting the reflux bottle 7.
Furthermore, the backing ring of the reflux bottle 7 is fixedly connected with the bracket 2 through a rod.
Further, the motor 13 is connected with a support frame 12, and the support frame 12 is fixed on the support 2 through a cross angle 11.
Further, the lower end of the reaction kettle body 4 is provided with a discharge valve 18.
The working principle of the method is that reaction materials are put in a glass reaction kettle, and the glass reaction kettle can be vacuumized to perform stirring reaction; the external water (oil) bath kettle can be added with water or heated with oil for heating reaction; and can control the evaporation and reflux of the reaction solution, and the constant pressure feeding. (optionally preparing a cold component and matching with a cold source to perform low-temperature reaction); a reflux bottle 7 is arranged on the reaction kettle cover 6, the reflux bottle 7 is supported by a reflux bottle supporting ring 8, the reflux bottle 7 is connected with a condenser 9, and a cooling coil is arranged on the condenser 9 and used for circulating cooling liquid; the upper end of the stirring rod 17 is connected with the output end of the motor 13 through a universal joint and then inserted into the reaction kettle body 4, a plate is arranged on the stirring rod 17 and horizontally arranged, and the plate is arranged between the lower fixing piece 16 and the upper fixing piece 15 and used for keeping the stability during stirring; heating device 1's structure is that inside is provided with resistance heating pipe, sets up around 4 rounds of reation kettle body, and the lower extreme of stirring rod 17 is provided with the stirring piece, and the structure is the slice, is four blade distributions, and constant voltage funnel 14 is passive regulation pressure, makes in the funnel liquid flow into the cauldron body smoothly through the constant voltage funnel, is because the internal pressure variation of cauldron drives the flow of the interior liquid of constant voltage funnel.
The present invention is further described in the detailed description, rather than in the limited form thereof, and it will be obvious to those skilled in the art that changes may be made in the structure without departing from the spirit and scope of the invention, and it is intended that all such changes be covered by the appended claims.
Claims (7)
1. The utility model provides a novel individual layer reation kettle, it includes support (2), its characterized in that: the heating device is characterized by further comprising a heating system, wherein a heating device (1) is arranged at the lower end of the support (2), and a resistance heating pipe is arranged inside the heating device (1);
a bottle clamping ring (5) is fixedly arranged on the support (2), the bottle clamping ring (5) is connected with a reaction kettle body (4), and a reaction kettle cover (6) is designed at the upper end of the reaction kettle body (4);
the reaction kettle comprises a stirring system, wherein a lower fixing piece (16) and an upper fixing piece (15) are arranged at the upper end of the reaction kettle cover (6), a stirring rod (17) is clamped between the lower fixing piece (16) and the upper fixing piece (15), the stirring rod (17) is vertically arranged, and the stirring rod (17) is connected with a motor (13) through a universal joint;
the reaction kettle cover (6) is connected with a reflux bottle (7), and the reflux bottle (7) is connected with a condenser (9);
the reaction kettle cover (6) is connected with a constant pressure funnel (14) through a standard opening;
and the side surface of the heating device (1) is provided with an electric cabinet (3).
2. The novel single-layer reaction kettle according to claim 1, characterized in that: and a feeding piston (10) is also arranged on the reaction kettle cover (6).
3. The novel single-layer reaction kettle according to claim 1, characterized in that: the bottle clamping ring (5) is arranged on the upper portion of the reaction kettle body (4) and used for clamping the reaction kettle body (4).
4. The novel single-layer reaction kettle according to claim 1, characterized in that: the lower end of the reflux bottle (7) is provided with a reflux bottle supporting ring (8) for supporting the reflux bottle (7).
5. The novel single-layer reaction kettle according to claim 4, wherein: the reflux bottle supporting ring (8) is fixedly connected with the bracket (2) through a rod.
6. The novel single-layer reaction kettle according to claim 1, characterized in that: the motor (13) is connected with a support frame (12), and the support frame (12) is fixed on the support (2) through a cross corner (11).
7. The novel single-layer reaction kettle according to claim 1, characterized in that: the lower end of the reaction kettle body (4) is provided with a discharge valve (18).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120624183.XU CN214486902U (en) | 2021-03-26 | 2021-03-26 | Novel individual layer reation kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120624183.XU CN214486902U (en) | 2021-03-26 | 2021-03-26 | Novel individual layer reation kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214486902U true CN214486902U (en) | 2021-10-26 |
Family
ID=78200592
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120624183.XU Active CN214486902U (en) | 2021-03-26 | 2021-03-26 | Novel individual layer reation kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214486902U (en) |
-
2021
- 2021-03-26 CN CN202120624183.XU patent/CN214486902U/en active Active
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