CN214438966U

CN214438966U - Reaction kettle for producing glycine metal chelate

Info

Publication number: CN214438966U
Application number: CN202022816574.XU
Authority: CN
Inventors: 姜红军; 王姗姗; 杨启邦
Original assignee: Weifang Taixing Biological Chemical Co ltd
Current assignee: Weifang Taixing Biological Chemical Co ltd
Priority date: 2020-11-30
Filing date: 2020-11-30
Publication date: 2021-10-22
Anticipated expiration: 2030-11-30

Abstract

A reaction kettle for producing glycine metal chelate relates to the technical field of chemical equipment, and comprises a kettle cover, a kettle body and a kettle bottom, wherein a stirring rod is arranged in the kettle body, the upper end of the stirring rod is connected with a driving mechanism arranged at the center of the top of the kettle cover, the lower end of the stirring rod is fixedly connected with two cross rods with the same structure, heating wires are arranged in the two cross rods, two ends of the two cross rods are respectively connected with the upper end and the lower end of a vertical plate, one sides of the two vertical plates, which are opposite to the inner wall of the kettle body, are provided with brush hair, the bottom of the stirring rod is in bolted connection with an arc-shaped plate, and one side of the arc-shaped plate, which is opposite to the inner bottom of the kettle body, is provided with brush hair; meanwhile, when the material is discharged, the inner wall of the reaction device is easily stained to increase the cleaning difficulty, and the inner wall of the reaction device is easily corroded by cleaning in time after the reaction is finished, so that the service life is shortened, and the cost is not saved.

Description

Reaction kettle for producing glycine metal chelate

Technical Field

The utility model relates to a chemical industry equipment technical field, concretely relates to reation kettle is used in glycine metal chelate production.

Background

The reaction kettle is a pressure container which has a physical or chemical reaction container, realizes the heating, evaporation, cooling and low-speed mixing functions required by the process by the structural design and parameter configuration of the container, is widely applied to petroleum, chemical engineering, rubber, pesticides, dyes, medicines and foods, and is used for completing the processes of vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like.

In the existing devices, most of reaction devices directly put reaction raw materials into reaction liquid for stirring reaction, but the reaction under the condition of needing heating is easy to suffer from the problem of uneven heating, and partial reaction raw materials sink to the bottom of a reaction kettle and cannot be stirred fully; meanwhile, when the material is discharged, the inner wall of the reaction device is easily stained to increase the cleaning difficulty, and the inner wall of the reaction device is easily corroded by cleaning the reaction device untimely after the reaction is finished, so that the service life is shortened, and the cost is not favorably saved.

SUMMERY OF THE UTILITY MODEL

The utility model aims at providing a reaction kettle for producing glycine metal chelate, which can solve the problem that the heating is uneven easily when the reaction is carried out under the condition of heating, and part of reaction raw materials can sink into the bottom of the reaction kettle and can not be stirred fully; meanwhile, when the material is discharged, the inner wall of the reaction device is easily stained to increase the cleaning difficulty, and the reaction device is not cleaned in time after the reaction is finished, so that the inner wall of the reaction device is easily corroded, the service life is shortened, and the cost is not favorably saved.

In order to achieve the above object, the present invention provides the following technical solutions:

a reaction kettle for producing glycine metal chelate comprises a semicircular kettle cover and a semicircular kettle bottom, wherein a cylindrical kettle body is arranged between the kettle cover and the kettle bottom, the opening diameters of the kettle cover, the kettle body and the kettle bottom are equal, a stirring rod coaxial with the kettle body is arranged in the kettle body, the upper end of the stirring rod is connected with a driving mechanism arranged at the center of the top of the kettle cover, a feeding pipe and an observation window are respectively arranged at two sides of the driving mechanism, an exhaust port is also arranged on the kettle cover, a discharging pipe is arranged at the center of the bottom of the kettle bottom, two cross rods with the same structure are fixedly connected at the lower end of the stirring rod, heating wires are arranged in the two cross rods and are connected with a power switch outside the kettle body, two ends of the two cross rods are respectively connected with the upper end and the lower end of a vertical plate, bristles are arranged at one side of the two vertical plates opposite to the inner wall of the kettle body, and are in contact with the inner wall of the kettle body, the bottom of the stirring rod is connected with an arc plate through bolts, bristles are arranged on one side, opposite to the inner bottom of the kettle body, of the arc plate, the bristles are in contact with the inner wall of the kettle bottom, and two ends of the arc plate are in contact with the bottoms of the two vertical plates.

The heating wires are arranged in the two cross rods, so that the reaction liquid is heated uniformly and rapidly, and the reaction rate is improved; two ends of the two cross rods are respectively connected with the upper end and the lower end of the vertical plate, so that the vertical plate is favorably fixed, and the vertical plate is prevented from being separated from the cross rods due to large resistance of reaction liquid to the stirring rod when the stirring rod rotates; contact with the reation kettle inner wall through setting up brush hair and brush hair, do benefit to and prevent that the reactant from gluing to cover can not fully carry out the blending reaction with the reaction liquid on the inner wall, simultaneously after reaction work accomplishes, the rotatory brush hair that drives of puddler rotates and can fall the reaction liquid brush of reation kettle inner wall, finally discharges from arranging the material pipe, does benefit to and prevents that the reaction liquid from being stained with and cover on the inner wall, need rinse inside repeatedly, increases the washing degree of difficulty.

Preferably, the junction of kettle cover, the cauldron body and the cauldron bottom is the flange face, pass through bolted connection between two flange faces, still be equipped with sealed the pad between two flange faces.

All set up to the flange face through the junction with kettle cover, the cauldron body and cauldron bottom, through bolted connection between two flange faces, can realize disassembling reation kettle, conveniently maintain the inner structure, still be equipped with sealed the pad between two flanges simultaneously, increase the leakproofness of junction, prevent the weeping.

Preferably, the connection mode of riser and horizontal pole is for dismantling to be connected, and detachable connection mode does benefit to and changes the riser, and the brush hair on the riser uses and to have wearing and tearing after a period, need change after reaching not the optimal result of use, can change again after separating the cauldron body and kettle cover.

Preferably, an anticorrosive coating is coated on the inner wall of the reaction kettle, the thickness of the anticorrosive coating is 3-5mm, a temperature sensor is arranged on the outer wall of the reaction kettle, and the temperature sensor is positioned at one third of the lower end of the kettle body.

The anti-corrosion layer is arranged on the inner wall of the reaction kettle, so that liquid can be prevented from splashing to any place on the inner wall of the reaction kettle when the reaction liquid is stirred, the reaction liquid is prevented from being corroded, and the service life is shortened; through setting up temperature sensor, do benefit to the temperature of control reation kettle interior reaction liquid.

Preferably, the reaction kettle further comprises a controller, wherein the controller is arranged on the kettle body, the output end of the temperature sensor is connected with the input end of the controller, the output end of the controller is connected with the power switch and the driving mechanism, and whether the reaction liquid needs to be heated and stirred or not is controlled by arranging the controller, so that intelligent operation is realized.

Preferably, the discharge pipe is provided with a discharge valve, and whether discharge is needed or not is controlled by opening or closing the discharge valve.

Compared with the prior art, the beneficial effects of the utility model are that:

the utility model provides a glycine metal chelate production uses reation kettle, drives the puddler through setting up actuating mechanism and rotates, fully stirs the reaction liquid inside the reation kettle for reactant and reaction liquid fully fuse, heat simultaneously in the stirring process, do benefit to the reaction rate who improves the reaction liquid, and then promote work efficiency; after the reaction is finished, the bristles on the vertical plates and the arc plates are driven to rotate through rotation of the stirring rods, and reaction liquid can be discharged and collected to the maximum extent, so that the difficulty in cleaning the inner wall of the reaction kettle is reduced, and water is saved.

Drawings

In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings needed to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments described in the present invention, and other drawings can be obtained by those skilled in the art according to these drawings.

FIG. 1 is a schematic view of a three-dimensional structure of a reaction kettle for producing glycine metal chelate.

FIG. 2 is the internal structure diagram of a reaction kettle for producing glycine metal chelate provided by the utility model.

Description of reference numerals:

1-kettle cover, 2-kettle bottom, 3-kettle body, 4-stirring rod, 5-driving mechanism, 6-feeding pipe, 7-observation window, 8-exhaust port, 9-discharging pipe, 10-cross bar, 11-heating wire, 12-vertical plate, 13-brush hair, 14-arc plate, 15-flange surface, 16-sealing gasket, 17-anticorrosive layer, 18-temperature sensor, 19-controller and 20-discharging valve.

Detailed Description

The invention will be described in detail below with reference to the drawings attached hereto by way of example, and it will be apparent that the described embodiments are only some, but not all, embodiments of the invention.

As shown in fig. 1-2, a reaction kettle for producing glycine metal chelate comprises a semicircular kettle cover 1 and a semicircular kettle bottom 2, wherein a cylindrical kettle body 3 is arranged between the kettle cover 1 and the kettle bottom 2, the opening diameters of the kettle cover 1, the kettle body 3 and the kettle bottom 2 are all equal, the joints of the kettle cover 1, the kettle body 3 and the kettle bottom 2 are flange surfaces 15, the two flange surfaces 15 are connected through bolts, and a sealing gasket 16 is further arranged between the two flange surfaces 15. The internal puddler 4 rather than coaxial that is equipped with of cauldron, the upper end and the actuating mechanism 5 that sets up at 1 top center of kettle cover of puddler 4 are connected, actuating mechanism 5 is the motor, the output of motor passes through the shaft coupling and is connected with puddler 4, 5 both sides of actuating mechanism are provided with inlet pipe 6 and observation window 7 respectively, can observe the reaction conditions in the reation kettle at any time through observation window 7, still be equipped with gas vent 8 on the

kettle cover

1, 2 bottom centers at the bottom of the kettle are equipped with row material pipe 9, be provided with relief valve 20 on arranging material pipe 9, whether need arrange the material through opening or closing of relief valve 20. The utility model discloses a kettle, including 4 lower extremes of puddler, two horizontal poles 10 that the structure is the same of puddler fixedly connected with, be equipped with heater strip 11 in two horizontal poles 10, heater strip 11 couples with the switch of the 3 outsides of the cauldron body, the both ends of two horizontal poles 10 are connected with the upper and lower both ends of riser 12 respectively, riser 12 is connected for dismantling with the connected mode of horizontal pole 10, does benefit to and changes riser 12 and brush hair 13. The relative one side of two risers 12 and the 3 inner walls of the cauldron body is provided with brush hair 13, two brush hairs 13 contact with the 3 inner walls of the cauldron body, 4 bottom bolted connections of puddler have arc 14, one side that arc 14 and the 3 inner bottoms of the cauldron body are relative is provided with brush hair 13, brush hair 13 contacts with 2 inner walls at the bottom of the cauldron, the both ends of arc 14 with the bottom of two risers 12 contacts, prevents to produce and leaves over, causes to scrub unevenly.

The inner wall of the reaction kettle is coated with an anticorrosive coating 17, the thickness of the anticorrosive coating 17 is 3-5mm, preferably 4mm, the inner wall of the reaction kettle is prevented from being corroded by reaction liquid, the outer wall of the reaction kettle is provided with a temperature sensor 18, and the temperature sensor 18 is positioned at one third of the lower end of the kettle body 3.

The kettle further comprises a controller 19, the controller 19 is arranged on the kettle body 3, the output end of the temperature sensor 18 is connected with the input end of the controller 19, and the output end of the controller 19 is connected with the power switch and the driving mechanism 5.

The working principle is as follows: when the device is used, a discharge valve 20 on a discharge pipe 9 is closed, glycine metal chelate is added from a feed pipe 6 and falls into an inner cavity of a reaction kettle, when a temperature sensor 18 detects that the temperature in the reaction kettle is lower than a set reaction temperature, a signal is transmitted to a controller 19, the controller 19 controls a power switch to electrify a heating wire 11, and simultaneously controls a motor to operate to drive a stirring rod 4 to stir reaction liquid, the bristles 13 on two vertical plates 12 and an arc-shaped plate 14 can wash out reactants adhered on the inner wall of the reaction kettle to fully fuse the reactants, waste gas generated by the reaction liquid is discharged from an exhaust port 8 due to heating in the reaction process, and the reaction condition can be known in real time through an observation window 7; after the reaction is accomplished, open relief valve 20, the reaction liquid is discharged from row material pipe 9, and puddler 4 lasts the rotation this moment, and 19 control switch of controller cut off the power supply, stop to the heater strip 11 heating, erode the reaction liquid on with the reation kettle inner wall through brush hair 13 and arrange material pipe 9 and discharge, and furthest's collection can also alleviate follow-up cleaning work to the reation kettle inner wall simultaneously, reduces and washs the degree of difficulty.

The utility model can realize the reaction of the glycine metal chelate under the condition of heating, and is easy to encounter the problem of uneven heating, and part of reaction raw materials can sink into the bottom of the reaction kettle and can not be stirred fully; meanwhile, when the material is discharged, the inner wall of the reaction device is easily stained to increase the cleaning difficulty, and the reaction device is not cleaned in time after the reaction is finished, so that the inner wall of the reaction device is easily corroded, the service life is shortened, and the cost is not favorably saved.

The above description is only the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can substitute or change the technical solution and the application concept of the present invention within the technical scope disclosed in the present invention.

Claims

1. The utility model provides a reation kettle is used in production of glycine metal chelate, includes at the bottom of semi-circular kettle cover (1) and the semi-circular kettle (2), be equipped with cylindrical kettle body (3) between at the bottom of kettle cover (1) and the kettle (2), the opening diameter homogeneous phase of at the bottom of kettle cover (1), the kettle body (3) and the kettle (2) equals, be equipped with rather than coaxial puddler (4) in the kettle body (3), the upper end and the actuating mechanism (5) of setting at kettle cover (1) top center of puddler (4) are connected, actuating mechanism (5) both sides are provided with inlet pipe (6) and observation window (7) respectively, still be equipped with gas vent (8) on kettle cover (1), the bottom of the kettle (2) bottom center is equipped with row material pipe (9), its characterized in that: the utility model discloses a kettle, including puddler (4), puddler (4) lower extreme fixedly connected with two horizontal poles (10) that the structure is the same, be equipped with heater strip (11) in two horizontal poles (10), heater strip (11) and the hookup of the outside switch of the cauldron body (3), the both ends of two horizontal poles (10) are connected with the upper and lower both ends of riser (12) respectively, one side that two riser (12) are relative with cauldron body (3) inner wall is provided with brush hair (13), two brush hairs (13) contact with cauldron body (3) inner wall, puddler (4) bottom bolted connection has arc (14), one side that arc (14) are relative with cauldron body (3) inner bottom is provided with brush hair (13), brush hair (13) contact with cauldron bottom (2) inner wall, the both ends of arc (14) with the bottom of two riser (12) contacts.

2. The reaction kettle for producing the glycine metal chelate as claimed in claim 1, wherein: the kettle cover (1), the kettle body (3) and the kettle bottom (2) are connected through a flange face (15), the two flange faces (15) are connected through bolts, and a sealing gasket (16) is arranged between the two flange faces (15).

3. The reaction kettle for producing the glycine metal chelate as claimed in claim 1, wherein: the vertical plates (12) are detachably connected with the cross rods (10).

4. The reaction kettle for producing the glycine metal chelate as claimed in claim 1, wherein: scribble anticorrosive coating (17) on the reation kettle inner wall, the thickness of anticorrosive coating (17) is 3-5mm, be equipped with temperature sensor (18) on the reation kettle outer wall, temperature sensor (18) are located cauldron body (3) lower extreme third department.

5. The reaction kettle for producing the glycine metal chelate as claimed in claim 4, wherein: still include controller (19), controller (19) set up on the cauldron body (3), the output of temperature sensor (18) and the input hookup of controller (19), the output and switch of controller (19) and actuating mechanism (5) hookup.

6. The reaction kettle for producing the glycine metal chelate as claimed in claim 1, wherein: the discharge pipe (9) is provided with a discharge valve (20).