CN212983030U - Water jacket for magnesium metal crystallization and crystallization device - Google Patents

Water jacket for magnesium metal crystallization and crystallization device Download PDF

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Publication number
CN212983030U
CN212983030U CN202021198762.4U CN202021198762U CN212983030U CN 212983030 U CN212983030 U CN 212983030U CN 202021198762 U CN202021198762 U CN 202021198762U CN 212983030 U CN212983030 U CN 212983030U
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water jacket
crystallization
inner sleeve
plate
water
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CN202021198762.4U
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孙玉仓
王建喜
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Hequ Yongchang Machinery Manufacturing Co ltd
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Hequ Yongchang Machinery Manufacturing Co ltd
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Abstract

The utility model discloses a water jacket for magnesium metal crystallization and a crystallization device, wherein one end of the water jacket is connected with a reduction tank, the other end is connected with a water jacket big cover, the water jacket comprises an inner jacket and an outer jacket, the outer jacket is connected with a water inlet pipe and a water outlet pipe, a water-stop sheet is arranged between the water inlet pipe and the water outlet pipe, the outer jacket is provided with an arc concave part, a vacuum tube is arranged inside the arc concave part and does not contact with the arc concave part, and the vacuum tube is; a crystallization barrel is arranged in the inner sleeve, a short joint is arranged on one side of the inner sleeve, and the inner sleeve is connected with a reduction tank through the short joint; the crystallization barrel is conical, the outer wall of the large-diameter end of the crystallization barrel is in close contact with the short joint, and a crystallization barrel support ring and a radial positioning piece are arranged outside the small-diameter end; the device simple structure need not to use the straw rope, avoids pressing from both sides the jar, reduces the safety risk, improves the life of device.

Description

Water jacket for magnesium metal crystallization and crystallization device
Technical Field
The utility model belongs to the technical field of the equipment of silicothermic process production magnesium metal, concretely relates to magnesium metal crystallization water jacket and crystallization device.
Background
The smelting method of the magnesium metal mainly comprises a thermal reduction method and an electrolytic method. Currently, ferrosilicon is generally adopted as a reducing agent for the thermal reduction method to remove dolomite [ magnesium carbonate calcium CaMg (C0)3)2]Magnesium oxide produced through a step such as calcination is thermally reduced to produce magnesium metal, and hence the method is also called a silicothermic method. The production process of the silicothermic process comprises the steps of crushing dolomite, heating and calcining by coal gas to obtain calcined dolomite (called calcined dolomite, the main components of which are magnesium oxide and calcium oxide), grinding by a ball mill, preparing and pressing balls by the calcined dolomite, fluorite powder and crushed and ball-milled ferrosilicon powder according to a proportion, then putting the balls into a reduction tank with a water jacket at the opening end, placing the reduction tank into a coal gas heating reduction furnace, putting the reduction tank into a crystallization device, vacuumizing and heating the interior of the reduction tank for reduction. Because the temperature of the water jacket is lower under the action of circulating water, magnesium steam reduced from the tank is crystallized in a crystallization barrel in the water jacket to form crystallized magnesium (crude magnesium), after the crystallization is finished, the crystallization barrel in the water jacket is taken out, the crystallized magnesium is taken out by a magnesium pressing machine, the crystallized magnesium is put into a refining furnace for refining, and the crystallized magnesium is cast into magnesium metal ingots (refined magnesium) with different specifications through a continuous casting machine.
The short joint (short joint) part of the water jacket is welded with the opening end of the reduction pot by using M407 welding materials, the water jacket is cooled by circulating water, a crystallization device in the water jacket consists of a crystallization barrel, a fire baffle plate and a magnesium pressing plate, and the reduction pot can be horizontally placed (called as a transverse pot) or vertically placed (called as a vertical pot) in the reduction furnace.
At present, an inner sleeve and a short-circuit part of a water jacket are made into straight sections by using a seamless steel pipe, the inner sleeve is also made into a cone with the inclination of 1 degree, a wet straw rope is filled between the large opening end of a crystallization barrel and the inner sleeve of the water jacket to prevent magnesium steam from crystallizing to the outside of the crystallization barrel and the inner sleeve, even if the crystallization barrel is not easy to take out due to crystallization outside the barrel caused by poor sealing performance, the crystallization barrel is commonly called as a clamping tank, so that the water jacket cannot be normally used, the short-circuit part of the water jacket is frequently replaced in the production process to ensure the normal use of the water jacket and prolong the service cycle of the water jacket, and when a large cover of the water jacket is opened to take out the crystallization barrel, air enters the inner sleeve to enable the straw rope to be instantly; in addition, the vacuum tube on the water jacket passes through the cooling water chamber, and in the production practice, the cooling water enters the reduction tank to cause explosion and injury accidents due to leakage at the joint of the vacuum tube and the inner sleeve. The inner sleeve and the outer sleeve are welded with the water jacket flange to form the structure of the cooling water chamber, and when the flange deforms and the water jacket large cover is not tightly sealed in use, the flange is difficult to replace, and the cost is high.
SUMMERY OF THE UTILITY MODEL
The utility model overcomes prior art's is not enough, provides a magnesium metal crystallization water jacket and crystallization device, and the device simple structure need not to use the straw rope, avoids pressing from both sides the jar, reduces safe risk, improves the life of device.
In order to achieve the purpose, the utility model discloses a realize through following technical scheme:
a magnesium metal crystallization device comprises a water jacket, a reduction tank, a crystallization barrel and a vacuum tube, wherein the water jacket is arranged outside the crystallization barrel and is connected with the vacuum tube and the reduction tank; a crystallization barrel is arranged in the inner sleeve, a short joint is arranged on one side of the inner sleeve, and the inner sleeve is connected with a reduction tank through the short joint; the short joint can also be written as a short joint.
The crystallization barrel is conical and comprises a large-diameter end and a small-diameter end, the outer wall of the large-diameter end of the crystallization barrel is in close contact with the short joint, and a crystallization barrel support ring and a radial positioning piece are arranged outside the small-diameter end;
the water jacket big cover is connected with the water jacket through a water jacket flange, and the water jacket flange is arranged on the inner sleeve.
A fire baffle is arranged between the short joint and the reduction tank, the fire baffle comprises an inner plate and an outer plate, the outer plate is circular, a through hole is formed in the center of the outer plate, the inner plate is hexagonal, and the outer plate and the inner plate are connected through a connecting plate;
the crystallization barrel support ring comprises an inner ring and an outer ring, the diameter of the outer ring is smaller than that of the inner ring, a rib plate is arranged between the inner ring and the outer ring, a radial positioning piece is detachably arranged between the crystallization barrel support ring and the inner sleeve, and the radial positioning piece is in a semi-circular shape;
a sealing gasket is arranged between the water jacket large cover and the water jacket flange, the sealing gasket is annular, and an annular groove is formed in the water jacket large cover.
The inner sleeve is in a straight cylinder shape, the short joint is in a conical shape, the conical degree is 6-20 degrees, and the conical large end of the short joint is connected with the inner sleeve.
The inner sleeve and the short joint are arranged into an integral conical structure, the large-diameter end of the conical structure is connected with the water jacket flange, the small-diameter end of the conical structure is connected with the reduction tank, and the direction of the inner sleeve of the conical structure is opposite to that of the conical crystallization barrel.
A magnesium pressing plate is arranged in the small-diameter end of the crystallization barrel, and an airflow groove is formed in the edge of the magnesium pressing plate.
An arc-shaped gap is arranged between the arc-shaped concave part and the outer wall of the vacuum tube, and the width of the arc-shaped gap is more than 10 mm.
A magnesium metal crystal water jacket, one end of the water jacket is connected with a reduction tank, the other end of the water jacket is connected with a water jacket big cover, the water jacket comprises an inner jacket and an outer jacket, the outer jacket is connected with a water inlet pipe and a water outlet pipe, a water-stop plate is arranged between the water inlet pipe and the water outlet pipe along the axial direction, the outer jacket is provided with an arc-shaped concave part, a vacuum pipe is arranged on the inner side of the arc-shaped concave part and does not contact; a crystallization barrel is arranged in the inner sleeve, a short joint is arranged on one side of the inner sleeve, and the inner sleeve is connected with a reduction tank through the short joint; a fire baffle is arranged between the short joint and the reduction tank, the fire baffle comprises an inner plate and an outer plate, the outer plate is circular, a through hole is formed in the center of the outer plate, the inner plate is hexagonal, and the outer plate and the inner plate are connected through a connecting plate; a sealing gasket is arranged between the water jacket large cover and the water jacket flange, the sealing gasket is annular, and an annular groove is formed in the water jacket large cover. The inner sleeve is in a straight cylinder shape, the short joint is in a conical shape, the conical degree is 6-20 degrees, and the conical large end of the short joint is connected with the inner sleeve. The inner sleeve and the short joint are arranged into an integrated conical structure, the large-diameter end of the conical structure is connected with the large water jacket cover, the small-diameter end of the conical structure is connected with the reduction tank, and the direction of the inner sleeve of the conical structure is opposite to that of the conical crystallization barrel. An arc-shaped gap is arranged between the arc-shaped concave part and the outer wall of the vacuum tube, and the width of the arc-shaped gap is more than 10 mm.
The utility model discloses produced beneficial effect for prior art does:
the problem that a crystallization barrel is easy to generate magnesium vapor in a water jacket and is crystallized outside the barrel to cause tank clamping in the existing production process is solved;
secondly, the generation of pollutants caused by the use of straw ropes is avoided, and good economic benefits and environmental protection benefits are achieved;
thirdly, the risk that in the prior art, because the vacuum tube passes through the circulating water chamber, the leakage of the welding seam can cause the circulating water to enter the reduction tank to cause safety accidents is thoroughly eliminated;
fourthly, the water jacket flange can be conveniently replaced, and welding is simple and convenient;
fifthly, the usability and the durability of the crystallization barrel are improved, the replacement period of the crystallization barrel is prolonged, the cost is reduced, and the benefit is improved.
Drawings
Fig. 1 is a schematic structural diagram of an apparatus according to embodiment 1 of the present invention.
Fig. 2 is a view from a-a of fig. 1.
Fig. 3 is a schematic view of the position of a water-stop sheet according to embodiment 1 of the present invention.
Fig. 4 is a schematic structural view of a supporting ring and a radial positioning member of a crystallization barrel in embodiment 1 of the present invention.
Fig. 5 is a schematic structural view of a fire damper of embodiment 1 of the present invention.
Fig. 6 is a schematic structural view of an inner plate and an outer plate according to embodiment 1 of the present invention.
Fig. 7 is a schematic structural view of a magnesium pressing plate according to embodiment 1 of the present invention.
Fig. 8 is a schematic structural view of an apparatus according to embodiment 2 of the present invention.
The device comprises an inner sleeve 1, an outer sleeve 2, a reduction tank 3, a crystallization barrel 4, a vacuum tube 5, a water inlet tube 6, a water outlet tube 7, a water-stop plate 8, an arc-shaped concave part 9, a short joint 10, a crystallization barrel support ring 11, a radial positioning piece 12, a water jacket large cover 13, a water jacket flange 14, a fire-stop plate 15, a sealing gasket 16, an arc-shaped gap 17, a magnesium pressing plate 18, an airflow groove 19, an inner ring 111, an outer ring 112, a rib plate 113, an inner plate 151, an outer plate 152, a through hole 153 and a connecting.
Detailed Description
In order to make the technical problem, technical scheme and beneficial effect that the utility model will solve more clearly understand, combine embodiment and attached drawing, it is right to go on further detailed description the utility model discloses. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention. The technical solution of the present invention is described in detail below with reference to the embodiments and the drawings, but the scope of protection is not limited thereto.
Example 1
As shown in the figures 1-7 of the drawings,
a magnesium metal crystallization device comprises a water jacket, a reduction tank 3, a crystallization barrel 4 and a vacuum tube 5, wherein the water jacket is arranged outside the crystallization barrel and is connected with the vacuum tube and the reduction tank.
One end of the water jacket is connected with a reduction tank 3, the other end of the water jacket is connected with a water jacket big cover 13, the water jacket comprises an inner sleeve 1 and an outer sleeve 2, the outer sleeve 2 is connected with a water inlet pipe 6 and a water outlet pipe 7, a water stop plate 8 is arranged between the water inlet pipe 6 and the water outlet pipe 7, the outer sleeve is provided with an arc-shaped concave part 9, the vacuum pipe 5 is connected with the inner sleeve 1, the vacuum pipe 5 is arranged on the inner side of the arc-shaped concave part 9 and is not in contact with the arc-shaped concave part, an arc-shaped gap 17 is.
A crystallization barrel 4 is arranged in the inner sleeve, a short joint (short joint) 10 is arranged on one side of the inner sleeve, and the inner sleeve is connected with a reduction tank 3 through the short joint (short joint);
the inner sleeve 1 is in a straight cylinder shape, the short joint (short joint) 10 is in a conical shape, the conical degree is 6-20 degrees, and the conical large end of the short joint (short joint) is connected with the inner sleeve.
The water jacket big cover 13 is connected with the water jacket through a water jacket flange 14, and the water jacket flange is arranged on the inner sleeve 1. And a sealing gasket 16 is arranged between the water jacket large cover 13 and the water jacket flange 14, the sealing gasket is annular, and an annular groove is formed in the water jacket large cover.
A fire baffle plate 15 is arranged between the short joint 10 and the reduction tank, the fire baffle plate comprises an inner plate 151 and an outer plate 152, the outer plate is circular, the center of the outer plate is provided with a through hole 153, the inner plate is hexagonal, and the outer plate and the inner plate are connected through a connecting plate 154;
the crystallization barrel 4 is conical and comprises a large-diameter end and a small-diameter end, the outer wall of the large-diameter end of the crystallization barrel is in close contact with the short joint 10, and a crystallization barrel support ring 11 and a radial positioning piece 12 are arranged on the outer side of the small-diameter end;
the crystallization barrel support ring 11 comprises an inner ring 111 and an outer ring 112, the diameter of the outer ring 112 is smaller than that of the inner ring 111, a rib plate 113 is arranged between the inner ring and the outer ring, a radial positioning piece 12 can be detachably arranged between the crystallization barrel support ring 11 and the inner sleeve, and the radial positioning piece 12 is in a semicircular shape; the inner part of the small-diameter end of the crystallization barrel is provided with a magnesium pressing plate 18, the edge of the magnesium pressing plate is provided with an airflow groove 19, and the airflow groove enables airflow to be formed during vacuum pumping.
Example 2
In the device of embodiment 1, the inner sleeve 1 and the short joint 10 can also be arranged into an integral conical structure, the large diameter end of the conical structure is connected with the large water jacket cover 13, the small diameter end is connected with the reduction tank 3, and the direction of the inner sleeve of the conical structure is opposite to that of the conical crystallization barrel. As shown in fig. 8.
In actual production, the short-circuit part of the water jacket is welded with the opening end of the reduction pot by using M407 welding materials, the water jacket is cooled by circulating water, a crystallization device in the water jacket consists of a crystallization barrel, a fire baffle plate and a magnesium pressing plate, the reduction pot can be horizontally placed (called a transverse pot) or vertically placed (called a vertical pot) in the reduction furnace, and a radial positioning piece is not used when the reduction pot is vertically placed.
A water-stop plate is arranged between the outer sleeve and the inner sleeve along the axial direction and is positioned between the water inlet pipe and the water outlet pipe.
1. The short joint (short joint) part is conical, and the conicity is 6-20 degrees according to the specifications of the water jacket and the reduction tank.
2. The vacuum tube is connected with the inner sleeve and does not pass through the cooling water chamber, so that the safety is good.
3. The flange of the water jacket is only connected with the inner sleeve but not connected with the outer sleeve, and the flange is convenient to replace after being deformed in the using process.
4. The water-stop sheet is axially arranged in the cooling water chamber, the water inlet pipe and the water outlet pipe are respectively arranged on two sides of the water-stop sheet, circulating water short circuit is avoided, the cooling effect is good, and the blockage of circulation caused by scaling is not easy to occur.
5. The crystallization barrel is of a large-small-head conical structure, a column part is not arranged (the column part causes that crystallized magnesium is not easy to be extruded out of the crystallization barrel), and a support ring, also called a crystallization ring, is arranged outside the small head end and is used for placing the crystallization barrel on a magnesium pressing machine. Install in the tip and press the magnesium board, its effect: firstly, prevent that magnesium vapour from passing through little head toward outer crystallization, secondly lay the crystallization bucket that contains crystal magnesium on pressing the magnesium machine, hydro-cylinder pressure acts on and presses the magnesium board, extrudes crystal magnesium from the crystallization bucket.
6. The crystallization bucket lock ring can be made into a single-layer ring reinforced structure, and also can be made into a double-layer ring reinforced structure.
7. A semicircular annular radial positioning is arranged between the position of the support ring of the crystallization barrel and the inner sleeve of the water jacket, so that the radial positioning is ensured, and the assembly and disassembly are convenient; the single-layer support ring can be welded with a plurality of radial positioning columns on the outer circle of the single-layer support ring, so that the axis of the crystallization barrel and the axis of the inner sleeve are concentric and sealed.
8. The fire baffle plate is arranged in the big end of the crystallization barrel and is used for preventing high-temperature heat in the reduction tank from entering the crystallization barrel, so that magnesium steam is crystallized in the crystallization barrel.
9. The big end of the crystallization barrel is connected with the taper at the short joint (short joint) part of the water jacket to form sealing, thereby avoiding crystallization outside the barrel.
The above description is for further details of the present invention with reference to specific preferred embodiments, and it should not be understood that the embodiments of the present invention are limited thereto, and it will be apparent to those skilled in the art that the present invention can be implemented in a plurality of simple deductions or substitutions without departing from the scope of the present invention, and all such alterations and substitutions should be considered as belonging to the present invention, which is defined by the appended claims.
In the description of the present invention, it is to be understood that the terms "center", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise" and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, and do not indicate or imply that the designated device or element must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.

Claims (9)

1. A magnesium metal crystallization device comprises a water jacket, a reduction tank (3), a crystallization barrel (4) and a vacuum tube (5), the water jacket is arranged outside the crystallization barrel and is connected with the vacuum tube and the reduction tank,
one end of the water jacket is connected with a reduction tank (3), the other end of the water jacket is connected with a water jacket big cover (13), the water jacket comprises an inner sleeve (1) and an outer sleeve (2), the outer sleeve (2) is connected with a water inlet pipe (6) and a water outlet pipe (7), a water-stop plate (8) is arranged between the water inlet pipe (6) and the water outlet pipe (7) along the axial direction, the outer sleeve is provided with an arc-shaped concave part (9), the vacuum pipe (5) is arranged on the inner side of the arc-shaped concave part (9) and does not contact with the arc; a crystallization barrel (4) is arranged in the inner sleeve, a short joint (10) is arranged at one side of the inner sleeve, and the inner sleeve is connected with a reduction tank (3) through the short joint;
the crystallization barrel (4) is conical and comprises a large-diameter end and a small-diameter end, the outer wall of the large-diameter end of the crystallization barrel is in close contact with the short joint (10), and a crystallization barrel support ring (11) and a radial positioning piece (12) are arranged on the outer side of the small-diameter end;
the water jacket big cover (13) is connected with the water jacket through a water jacket flange (14), and the water jacket flange is arranged on the inner sleeve (1).
2. The magnesium metal crystallization device according to claim 1, wherein the inner sleeve (1) is straight cylindrical, the short joint (10) is conical, the conicity is 6-20 degrees, and the large end of the short joint is connected with the inner sleeve.
3. The magnesium metal crystallization device according to claim 1, characterized in that the inner sleeve (1) and the short joint (10) are arranged into an integral conical structure, the large diameter end of the conical structure is connected with the water jacket flange (14), and the small diameter end is connected with the reduction tank (3).
4. The magnesium metal crystallization device according to claim 1, wherein the crystallization barrel support ring (11) comprises an inner ring (111) and an outer ring (112), the diameter of the outer ring (112) is smaller than that of the inner ring (111), a rib plate (113) is arranged between the inner ring and the outer ring, and a radial positioning element (12) is detachably arranged between the crystallization barrel support ring (11) and the inner sleeve.
5. The magnesium metal crystallization device is characterized in that a sealing gasket (16) is arranged between the water jacket big cover (13) and the water jacket flange (14), the sealing gasket is annular, and an annular groove is formed in the water jacket big cover; a fire baffle (15) is arranged between the short joint (10) and the reduction tank, the fire baffle comprises an inner plate (151) and an outer plate (152), the outer plate is circular, a through hole (153) is formed in the center of the outer plate, the inner plate is hexagonal, and the outer plate and the inner plate are connected through a connecting plate (154); a magnesium pressing plate (18) is arranged in the small-diameter end of the crystallization barrel, and an airflow groove (19) is arranged at the edge of the magnesium pressing plate.
6. The magnesium metal crystallization device according to claim 1, wherein an arc gap (17) is provided between the arc-shaped concave portion (9) and the outer wall of the vacuum tube (5), and the width of the arc gap is 10mm or more.
7. The water jacket for the magnesium metal crystallization is characterized in that one end of the water jacket is connected with a reduction tank (3), the other end of the water jacket is connected with a water jacket big cover (13), the water jacket comprises an inner sleeve (1) and an outer sleeve (2), the outer sleeve (2) is connected with a water inlet pipe (6) and a water outlet pipe (7), a water-stop plate (8) is arranged between the water inlet pipe (6) and the water outlet pipe (7) along the axial direction, the outer sleeve is provided with an arc-shaped concave part (9), a vacuum pipe (5) is arranged on the inner side of the arc-shaped concave part (9) and does not contact with the arc; a crystallization barrel (4) is arranged in the inner sleeve, a short joint (10) is arranged at one side of the inner sleeve, and the inner sleeve is connected with a reduction tank (3) through the short joint;
a fire baffle (15) is arranged between the inner part of the short joint (10) and the reduction tank, the fire baffle comprises an inner plate (151) and an outer plate (152), the outer plate is circular, a through hole (153) is arranged in the center of the outer plate, the inner plate is hexagonal, and the outer plate and the inner plate are connected through a connecting plate (154);
a sealing gasket (16) is arranged between the water jacket large cover (13) and the water jacket flange (14), the sealing gasket is annular, and an annular groove is formed in the water jacket large cover.
8. The water jacket for magnesium metal crystallization as claimed in claim 7, wherein the inner sleeve (1) is straight cylindrical, the short joint (10) is tapered, the taper is 6-20 degrees, and the tapered large end of the short joint is connected with the inner sleeve.
9. The water jacket for magnesium metal crystallization according to claim 7, characterized in that the inner sleeve (1) and the short joint (10) are arranged into an integral conical structure, the large diameter end of the conical structure is connected with the water jacket flange (14), and the small diameter end is connected with the reduction tank (3).
CN202021198762.4U 2020-06-24 2020-06-24 Water jacket for magnesium metal crystallization and crystallization device Active CN212983030U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202021198762.4U CN212983030U (en) 2020-06-24 2020-06-24 Water jacket for magnesium metal crystallization and crystallization device

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Application Number Priority Date Filing Date Title
CN202021198762.4U CN212983030U (en) 2020-06-24 2020-06-24 Water jacket for magnesium metal crystallization and crystallization device

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CN212983030U true CN212983030U (en) 2021-04-16

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CN202021198762.4U Active CN212983030U (en) 2020-06-24 2020-06-24 Water jacket for magnesium metal crystallization and crystallization device

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023245794A1 (en) * 2022-06-21 2023-12-28 李勇 Magnesium vacuum crystallization tank having electromagnetic induction heating and cooling functions

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023245794A1 (en) * 2022-06-21 2023-12-28 李勇 Magnesium vacuum crystallization tank having electromagnetic induction heating and cooling functions

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