CN212818272U - Liquid-liquid extractor - Google Patents
Liquid-liquid extractor Download PDFInfo
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- CN212818272U CN212818272U CN202021411499.2U CN202021411499U CN212818272U CN 212818272 U CN212818272 U CN 212818272U CN 202021411499 U CN202021411499 U CN 202021411499U CN 212818272 U CN212818272 U CN 212818272U
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Abstract
The utility model discloses a liquid-liquid extractor, which comprises a tank body, the left bottom intercommunication of the jar body has the purge valve, the bottom fixedly connected with motor of the jar body, the output fixedly connected with pivot of motor, the inner chamber to the jar body is run through at the top of pivot, the surface of pivot is overlapped respectively and is equipped with puddler and connecting rod, the equal fixedly connected with scraper blade in both sides of connecting rod, the top of scraper blade is provided with annular water pipe, the bottom intercommunication of annular water pipe has the washing nozzle. The utility model discloses a set up jar body, connecting rod, motor, puddler, solvent valve, connecting pipe, washing nozzle, annular water pipe, liquid valve, scraper blade, pivot, feed liquor valve, light looks go out liquid pump, heavy phase go out liquid pump, wash water tank, water injection valve, extraction box, observation window, casing, washing water pump and the cooperation of purge valve and use, possess the convenience and wash jar internal portion, do not influence the advantage of other liquid extraction experiments next time.
Description
Technical Field
The utility model relates to an extraction technical field specifically is a liquid-liquid extractor.
Background
Extraction, also known as solvent extraction or liquid-liquid extraction, also known as extraction, is a unit operation that separates mixtures by utilizing the different solubilities of components in the system in a solvent. That is, the method is a method of transferring a solute substance from one solvent to another solvent by utilizing the difference in solubility or partition coefficient of the substance in two solvents which are not soluble (or slightly soluble) with each other.
The wide application is in chemistry, metallurgy, industries such as food, and is general in the petroleum refining industry, also often is used in the chemistry experiment, need use liquid-liquid extractor to extract in the chemistry experiment, and the extraction in-process solvent need be at jar internal and liquid mixing, and current extractor is inconvenient to be washd mixing tank internal portion, causes the pollution to another kind of liquid when can leading to the experiment next time like this, influences the precision of experiment.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a liquid-liquid extraction ware possesses the convenience and washs jar internal portion, does not influence the advantage of other liquid extraction experiments next time, has solved the inside inconvenient washing that washs of current extractor hybrid tank to influence the problem of experiment precision next time.
In order to achieve the above object, the utility model provides a following technical scheme: a liquid-liquid extractor comprises a tank body, wherein a cleaning valve is communicated with the left bottom of the tank body, a motor is fixedly connected with the bottom of the tank body, a rotating shaft is fixedly connected with the output end of the motor, the top of the rotating shaft penetrates through an inner cavity of the tank body, a stirring rod and a connecting rod are respectively sleeved on the surface of the rotating shaft, scraping plates are fixedly connected with the two sides of the connecting rod, an annular water pipe is arranged at the top of each scraping plate, a cleaning nozzle is communicated with the bottom of the annular water pipe, a solvent valve and a liquid valve are respectively communicated with the tops of the two sides of the tank body, a cleaning water tank is arranged at the bottom of the motor, a shell is fixedly connected with the left side of the inner cavity of the cleaning water tank, a cleaning water pump is fixedly connected with the inner cavity of the shell, a water, the one side that the washing water pump was kept away from to the connecting pipe runs through in proper order and washs the water tank and jar body and communicate with annular water pipe, the bottom intercommunication on jar body right side has the feed liquor valve, the right side intercommunication of feed liquor valve has the extraction box, the top of extraction box is fixedly connected with light looks liquid pump and heavy phase liquid pump respectively, the feed liquor end that the light looks goes out the liquid pump runs through to the top of extraction box inner chamber, the feed liquor end that the heavy phase goes out the liquid pump runs through to the bottom on extraction box inner chamber right side.
Preferably, the four corners of the bottom of the tank body are fixedly connected with supporting columns, and the joint of the surface of the rotating shaft and the tank body is movably connected through a sealing bearing.
Preferably, the inner cavity of the tank body is movably connected with the scraper which is made of hard rubber.
Preferably, the inner cavity of the tank body is fixedly connected with the annular water pipe, and the top on the right side of the cleaning water tank is communicated with a water injection valve.
Preferably, the front side of the cleaning water tank is fixedly connected with a glass plate in a penetrating manner, and the number of the cleaning nozzles is several.
Preferably, the front side of extraction box runs through fixedly connected with observation window, the quantity of puddler is a plurality of.
Compared with the prior art, the beneficial effects of the utility model are as follows:
1. the utility model discloses a set up jar body, connecting rod, motor, puddler, solvent valve, connecting pipe, washing nozzle, annular water pipe, liquid valve, scraper blade, pivot, feed liquor valve, light looks go out liquid pump, heavy phase goes out liquid pump, washs water tank, water injection valve, extraction box, observation window, casing, washing water pump and the cooperation of purge valve and use, possess the convenience and wash jar internal portion, do not influence the advantage of other liquid extraction experiments next time, be worth promoting.
2. The utility model can avoid the tank body from directly contacting with the ground by arranging the support columns;
by arranging the sealing bearing, the leakage of the mixed liquid in the tank body can be avoided;
by arranging the water injection valve, cleaning liquid can be conveniently injected into the cleaning water tank;
by arranging the glass plate, the stock of the cleaning liquid in the cleaning water tank can be conveniently observed;
through setting up the observation window, can conveniently observe the layering effect of extraction incasement mixture.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a front sectional view of the cleaning water tank of the present invention;
fig. 3 is a bottom view of the annular water pipe of the present invention.
In the figure: 1 tank body, 2 connecting rods, 3 motors, 4 stirring rods, 5 solvent valves, 6 connecting pipes, 7 cleaning nozzles, 8 annular water pipes, 9 liquid valves, 10 scraping plates, 11 rotating shafts, 12 liquid inlet valves, 13 light-phase liquid outlet pumps, 14 heavy-phase liquid outlet pumps, 15 cleaning water tanks, 16 water injection valves, 17 extraction tanks, 18 observation windows, 19 shells, 20 cleaning water pumps and 21 cleaning valves.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front end", "rear end", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element to be referred must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted", "provided", "connected", and the like are to be construed broadly, such as "connected", which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.
The utility model provides a jar body 1, connecting rod 2, motor 3, puddler 4, solvent valve 5, connecting pipe 6, washing nozzle 7, annular water pipe 8, liquid valve 9, scraper blade 10, pivot 11, feed liquor valve 12, light phase goes out liquid pump 13, heavy phase goes out liquid pump 14, wash water tank 15, water injection valve 16, extraction box 17, observation window 18, casing 19, parts such as washing water pump 20 and purge valve 21 are general standard or the part that technical staff in the field knows, its structure and principle all can learn through the technical manual or learn through conventional experimental method for technical staff in the field.
Referring to fig. 1-3, a liquid-liquid extractor comprises a tank body 1, a cleaning valve 21 is communicated with the bottom of the left side of the tank body 1, a motor 3 is fixedly connected with the bottom of the tank body 1, a rotating shaft 11 is fixedly connected with the output end of the motor 3, the top of the rotating shaft 11 penetrates into the inner cavity of the tank body 1, a stirring rod 4 and a connecting rod 2 are respectively sleeved on the surface of the rotating shaft 11, scrapers 10 are fixedly connected with the two sides of the connecting rod 2, an annular water pipe 8 is arranged at the top of each scraper 10, a cleaning nozzle 7 is communicated with the bottom of the annular water pipe 8, a solvent valve 5 and a liquid valve 9 are respectively communicated with the top of the two sides of the tank body 1, a cleaning water tank 15 is arranged at the bottom of the motor 3, a shell 19 is fixedly connected with the left side of the bottom of the inner cavity of the cleaning water tank 15, a cleaning water pump, one side of the connecting pipe 6, which is far away from the cleaning water pump 20, sequentially penetrates through the cleaning water tank 15 and the tank body 1 and is communicated with the annular water pipe 8, the bottom of the right side of the tank body 1 is communicated with a liquid inlet valve 12, the right side of the liquid inlet valve 12 is communicated with an extraction tank 17, the top of the extraction tank 17 is fixedly connected with a light phase liquid outlet pump 13 and a heavy phase liquid outlet pump 14 respectively, the liquid inlet end of the light phase liquid outlet pump 13 penetrates through the top of the inner cavity of the extraction tank 17, and the liquid inlet end of the heavy phase liquid outlet pump 14 penetrates through the;
the four corners of the bottom of the tank body 1 are fixedly connected with support columns, and the joint of the surface of the rotating shaft 11 and the tank body 1 is movably connected through a sealing bearing;
the inner cavity of the tank body 1 is movably connected with a scraper 10, and the scraper 10 is made of hard rubber;
the inner cavity of the tank body 1 is fixedly connected with the annular water pipe 8, and the top of the right side of the cleaning water tank 15 is communicated with a water injection valve 16;
the front side of the cleaning water tank 15 is fixedly connected with a glass plate in a penetrating way, and the number of the cleaning nozzles 7 is a plurality;
the front side of the extraction box 17 is fixedly connected with an observation window 18 in a penetrating way, and the number of the stirring rods 4 is a plurality;
the tank body 1 can be prevented from being directly contacted with the ground by arranging the supporting columns;
by arranging the sealing bearing, the leakage of the mixed liquid in the tank body 1 can be avoided;
by arranging the water injection valve 16, cleaning liquid can be conveniently injected into the cleaning water tank 15;
by arranging the glass plate, the stock of the cleaning liquid in the cleaning water tank 15 can be conveniently observed;
through setting up observation window 18, can conveniently observe the layering effect of the interior mixed liquid of extraction box 17.
When the device is used, a solvent and liquid are respectively injected from a solvent valve 5 and a liquid valve 9, then a motor 3 is electrified to work to drive a rotating shaft 11 to rotate, a stirring rod 4 and a scraper 10 on the surface of the rotating shaft 11 rotate along with the rotating shaft to stir and mix the solvent and the liquid, the motor 3 stops rotating after the mixing is finished, a liquid inlet valve 12 is opened, mixed liquid in a tank body 1 flows into an extraction tank 17, a light phase liquid outlet pump 13 and a heavy phase liquid outlet pump 14 work after the mixed liquid is layered in the extraction tank 17, light phase liquid in the upper layer and heavy phase liquid in the lower layer are respectively pumped out of the extraction tank 17, after the extraction is finished, the liquid inlet valve 12 is closed, a cleaning water pump 20 is electrified to work to convey cleaning liquid in a cleaning water tank 15 into an annular water pipe 8 through a connecting pipe 6, then the cleaning liquid is sprayed out through a cleaning nozzle 7 to wash the inner wall of the tank body 1, at the moment, the, the inside abluent more thorough of jar body 1 can be opened the purge valve 21 to pivoted scraper blade 10 cooperation washing liquid this moment, and the washing liquid flows out from purge valve 21, conveniently washs jar internal portion like this, does not influence other liquid extraction experiments next time.
In summary, the following steps: this liquid-liquid extractor, through a jar body 1, connecting rod 2, motor 3, puddler 4, solvent valve 5, connecting pipe 6, wash nozzle 7, annular water pipe 8, liquid valve 9, scraper blade 10, pivot 11, feed liquor valve 12, light phase goes out liquid pump 13, heavy phase goes out liquid pump 14, wash water tank 15, water injection valve 16, extraction box 17, observation window 18, casing 19, wash water pump 20 and washing valve 21's cooperation is used, the inside inconvenient washing that washs of current extractor hybrid tank has been solved, thereby influence the problem of experiment precision next time.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides a liquid-liquid extractor, includes jar body (1), its characterized in that: the cleaning tank is characterized in that a cleaning valve (21) is communicated with the left bottom of the tank body (1), a motor (3) is fixedly connected with the bottom of the tank body (1), a rotating shaft (11) is fixedly connected with the output end of the motor (3), the top of the rotating shaft (11) penetrates through the inner cavity of the tank body (1), a stirring rod (4) and a connecting rod (2) are respectively sleeved on the surface of the rotating shaft (11), scraping plates (10) are fixedly connected with the two sides of the connecting rod (2), an annular water pipe (8) is arranged at the top of each scraping plate (10), a cleaning nozzle (7) is communicated with the bottom of each annular water pipe (8), a solvent valve (5) and a liquid valve (9) are respectively communicated with the tops of the two sides of the tank body (1), a cleaning water tank (15) is arranged at the bottom of the motor (3), and a shell (19, the inner cavity of the shell (19) is fixedly connected with a cleaning water pump (20), a water inlet pipe of the cleaning water pump (20) penetrates through the inner cavity of the cleaning water tank (15), the water outlet end of the cleaning water pump (20) is communicated with a connecting pipe (6), one side of the connecting pipe (6) far away from the cleaning water pump (20) sequentially penetrates through the cleaning water tank (15) and the tank body (1) and is communicated with the annular water pipe (8), the bottom of the right side of the tank body (1) is communicated with a liquid inlet valve (12), the right side of the liquid inlet valve (12) is communicated with an extraction box (17), the top of the extraction box (17) is respectively and fixedly connected with a light phase liquid outlet pump (13) and a heavy phase liquid outlet pump (14), the liquid inlet end of the light phase liquid outlet pump (13) penetrates to the top of the inner cavity of the extraction box (17), the liquid inlet end of the heavy phase liquid outlet pump (14) penetrates through the bottom of the right side of the inner cavity of the extraction box (17).
2. The liquid-liquid extractor of claim 1, wherein: the equal fixedly connected with support column in four corners of jar body (1) bottom, the junction through sealed bearing swing joint of the surface of pivot (11) and jar body (1).
3. The liquid-liquid extractor of claim 1, wherein: the inner cavity of the tank body (1) is movably connected with the scraper (10), and the scraper (10) is made of hard rubber.
4. The liquid-liquid extractor of claim 1, wherein: the inner cavity of the tank body (1) is fixedly connected with the annular water pipe (8), and the top on the right side of the cleaning water tank (15) is communicated with a water injection valve (16).
5. The liquid-liquid extractor of claim 1, wherein: the front side of the cleaning water tank (15) penetrates through the glass plate and is fixedly connected with the glass plate, and the number of the cleaning nozzles (7) is a plurality.
6. The liquid-liquid extractor of claim 1, wherein: the front side of extraction box (17) runs through fixedly connected with observation window (18), the quantity of puddler (4) is a plurality of.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021411499.2U CN212818272U (en) | 2020-07-17 | 2020-07-17 | Liquid-liquid extractor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021411499.2U CN212818272U (en) | 2020-07-17 | 2020-07-17 | Liquid-liquid extractor |
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| Publication Number | Publication Date |
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| CN212818272U true CN212818272U (en) | 2021-03-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202021411499.2U Active CN212818272U (en) | 2020-07-17 | 2020-07-17 | Liquid-liquid extractor |
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| CN (1) | CN212818272U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113750568A (en) * | 2021-09-26 | 2021-12-07 | 臻顺(南京)工业设备有限公司 | Extraction barrel convenient to clean and cleaning method thereof |
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2020
- 2020-07-17 CN CN202021411499.2U patent/CN212818272U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113750568A (en) * | 2021-09-26 | 2021-12-07 | 臻顺(南京)工业设备有限公司 | Extraction barrel convenient to clean and cleaning method thereof |
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