CN212693409U - In-situ extraction instrument suitable for measuring moisture in flue gas - Google Patents

In-situ extraction instrument suitable for measuring moisture in flue gas Download PDF

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Publication number
CN212693409U
CN212693409U CN202020775795.4U CN202020775795U CN212693409U CN 212693409 U CN212693409 U CN 212693409U CN 202020775795 U CN202020775795 U CN 202020775795U CN 212693409 U CN212693409 U CN 212693409U
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extraction
pipeline
piston
flue gas
module
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姜兴益
林玉红
朱风鹏
常诚
李翔宇
张洪非
罗彦波
庞永强
慎龙舞
吕晓亮
闫瑞波
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National Tobacco Quality Supervision and Inspection Center
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National Tobacco Quality Supervision and Inspection Center
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Abstract

The utility model provides an normal position extraction appearance suitable for moisture determination in flue gas, including extraction unit and support (12), its characterized in that, the extraction unit is installed on support (12). The utility model discloses an normal position extraction appearance suitable for moisture determination in flue gas, its simple structure, convenient to use, be convenient for wash, through the reciprocating motion of two cavity pistons, realize extracting every extraction unit of circulation extraction through upper and lower two extraction intracavity pistons of thing are caught to the flue gas, make the extraction solution of extraction intracavity reciprocate to flow from top to bottom between two extraction chambeies, but the extraction of high efficiency is extracted to extractant circulation reciprocating flow catcher.

Description

In-situ extraction instrument suitable for measuring moisture in flue gas
Technical Field
The utility model belongs to the technical field of the tobacco detects and specifically relates to an normal position extraction appearance suitable for moisture determination in flue gas.
Background
The invention provides an in-situ extraction instrument suitable for measuring moisture in flue gas, aiming at the problems of capture of flue gas condensate of samples with too low (too high) moisture content in the flue gas of the prior ultra-low tar cigarettes, heated cigarettes, cigars and the like and large variability of moisture test. The invention has the advantages that: each extraction unit enables the extraction solution in the extraction cavity to flow up and down in a reciprocating manner between the two extraction cavities through the matched reciprocating motion of the pistons in the upper extraction cavity and the lower extraction cavity, and the extractant flows through the catcher in a circulating reciprocating manner, so that the extraction can be performed quickly and efficiently. The movement speed of the piston is accurate and adjustable, the reciprocating movement times can be set according to actual requirements, the extraction frequency and the extraction cycle times can be adjusted, and corresponding setting can be conveniently and flexibly carried out according to different test requirements. The instrument is composed of at least 10 test units, and can simultaneously perform multiple groups of tests, thereby improving the test efficiency and saving the time. The invention effectively solves the problems of overhigh moisture content of the flue gas of part of the samples and incomplete moisture capture of the samples at present, and realizes accurate determination of the moisture in the flue gas.
The moisture is one of active ingredients in the cigarette smoke and can be adjusted through manual control, and the inherent sensory quality of the cigarette is directly influenced by the moisture. Research has shown that the moisture in the cut tobacco can be effectively adjusted by controlling the process conditions. However, the generation mechanism and adjustment measures of the flue gas moisture are not deeply researched, which may be related to more influence factors of the flue gas moisture measurement. In view of the importance of moisture, in recent years, the accuracy requirement for moisture testing in cigarette smoke is becoming more and more strict. Meanwhile, the calculation of the tar level of the cigarettes relates to the moisture content in the total particulate matter, and the accurate numerical value of the tar amount in the total particulate matter can be obtained only after the moisture content and the nicotine content in the total particulate matter are accurately measured.
The heating cigarette is a novel tobacco product which heats a core substrate (below 300 ℃ or even lower) by utilizing a special heat source and only heats the core substrate without burning. The physical and chemical properties of the tobacco material (core base material) used by the heating cigarette are obviously different from those of tobacco leaves and traditional reconstituted tobacco leaves, particularly, the alcohol smoke agent with a high proportion is used, and the smoke agent has high hygroscopicity, so that the moisture content in the mainstream smoke of the heating cigarette is obviously higher than that of the traditional cigarette. When the cigarette which is not heated and burnt is smoked, condensate is found on the front cover and the rear cover of the catcher, and the traditional main stream smoke particle phase matter catching and extracting treatment mode is not suitable for catching and extracting treatment of smoke with high moisture content such as heated cigarette, thereby influencing the measurement result.
SUMMERY OF THE UTILITY MODEL
For overcoming current defect, the utility model provides an in situ extraction appearance suitable for moisture determination in the flue gas.
The in-situ extraction instrument suitable for measuring the moisture in the flue gas comprises an extraction unit and a support, wherein the extraction unit is arranged on the support.
The extraction unit comprises an upper linear sliding rail, an upper linear motor, a cylinder, an upper piston, an upper extraction cavity, a trap, a pipeline module, a lower extraction cavity, a lower piston, a lower linear motor and a lower linear sliding rail, wherein the upper linear motor, the upper piston and the upper extraction cavity are arranged on the cylinder and move together with the cylinder; the upper piston is arranged on a motor shaft of the upper linear motor, and is pushed by the motor shaft to reciprocate in the upper extraction cavity, and the upper end of the motor shaft is fixed on the upper linear slide rail and is limited at the upper part to do linear motion; the pipeline module is arranged on the lower extraction cavity, three pipelines are arranged in the pipeline module and respectively comprise a suction pipeline, an extraction pipeline and a release pipeline, a motor shaft of the lower linear motor pushes the lower piston to do reciprocating motion in the lower extraction cavity, the lower end of the motor shaft is fixed on the lower linear slide rail, and the lower piston is limited to do linear motion; the lower extraction chamber is fixed on the bracket, and the catcher is arranged between the pipeline module and the upper extraction chamber.
Wherein, the extraction unit is a plurality of, and is fixed for multiunit side by side.
Optionally, the extraction unit further comprises a cleaning module mounted between the piping module and the upper extraction chamber.
Preferably, the pipeline module is made of corrosion-resistant materials, and pipelines are automatically switched inside the pipeline module through electromagnetic valves.
Preferably, the upper extraction chamber and the lower extraction chamber are of transparent quartz glass.
The utility model discloses an normal position extraction appearance suitable for moisture determination in flue gas, its simple structure, convenient to use, be convenient for wash, through the reciprocating motion of two cavity pistons, realize extracting every extraction unit of circulation extraction through upper and lower two extraction intracavity pistons of thing are caught to the flue gas, make the extraction solution of extraction intracavity reciprocate to flow from top to bottom between two extraction chambeies, but the extraction of high efficiency is extracted to extractant circulation reciprocating flow catcher.
The movement speed of the piston is accurate and adjustable, the reciprocating movement times can be set according to actual requirements, the extraction frequency and the extraction cycle times can be adjusted, and corresponding setting can be conveniently and flexibly carried out according to different test requirements.
The instrument is composed of at least 10 test units, and can simultaneously perform multiple groups of tests, thereby improving the test efficiency and saving the time.
Drawings
FIG. 1 is a schematic diagram of an in-situ extractor suitable for measuring moisture in flue gas.
FIG. 2 is a schematic diagram of in situ extractor cleaning suitable for moisture determination in flue gas.
Detailed Description
The following describes in detail an in-situ extraction apparatus suitable for measuring moisture in flue gas, which is provided by the present invention, with reference to the accompanying drawings and specific embodiments.
Fig. 1 and 2 show an in-situ extractor suitable for moisture determination in flue gas, comprising an extraction unit and a support 12, the extraction unit being mounted on the support 12.
The extraction unit comprises an upper linear sliding rail 1, an upper linear motor 2, a cylinder 3, an upper piston 4, an upper extraction cavity 5, a catcher 6, a pipeline module 7, a lower extraction cavity 8, a lower piston 9, a lower linear motor 10 and a lower linear sliding rail 11, wherein the upper linear motor 2, the upper piston 4 and the upper extraction cavity 5 are arranged on the cylinder 3 and move together with the cylinder 3; the upper piston 4 is arranged on a motor shaft of the upper linear motor 2, and reciprocates in the upper extraction cavity 5 under the pushing of the motor shaft, and the upper end of the motor shaft is fixed on the upper linear slide rail 1 and limits the upper piston 4 to do linear motion; the pipeline module 7 is installed on the lower extraction cavity 8, three pipelines are arranged in the pipeline module 7 and respectively comprise a suction pipeline, an extraction pipeline and a release pipeline, a motor shaft of a lower linear motor 10 pushes a lower piston 9 to reciprocate in the lower extraction cavity 8, the lower end of the motor shaft is fixed on a lower linear slide rail 11, and the lower piston 4 is limited to do linear motion; the lower extraction chamber 8 is fixed on a support 12 and the trap 6 is mounted between the pipe module 7 and the upper extraction chamber 5.
The extraction units are multiple and are fixed in parallel.
The extraction unit further comprises a washing module 600, which washing module 600 is mounted between the pipe module 7 and the upper extraction chamber 5.
Before testing, the cylinder 3 is lifted to the highest position, the upper piston 4 is lowered to the lowest position in the upper extraction cavity 5, the lower piston 9 is lifted to the highest position in the lower extraction cavity 8, the catcher 6 is installed on the pipeline module 7, the cylinder 3 is lowered after the installation, the upper extraction cavity 5, the catcher 6, the management module 7 and the lower extraction cavity 8 are connected together to form a pipeline passage, the suction pipeline is selected through the switching of an electromagnetic valve in the pipeline module 7, the upper piston 4 moves upwards to suck the extractant into the upper extraction cavity 5, at the moment, the upper piston 4 is lifted to the highest position, the pipeline in the pipeline module 7 is switched to the extraction pipeline after the completion, the upper extraction cavity 5 and the lower extraction cavity 8 are connected into a passage, the upper piston 4 and the lower piston 8 reciprocate up and down simultaneously to push the extractant to circularly flow between the upper extraction cavity 5 and the lower extraction cavity 8, causing a cyclic flow back and forth through the trap 6.
After the test number is up, the upper piston 4 and the lower piston 8 both move to the highest position, the pipeline module 7 switches the pipeline to the release pipeline, the upper piston 4 moves downwards to release the extraction liquid in the upper extraction cavity 5, the rear cylinder 3 is lifted after the extraction liquid in the upper extraction cavity 5 is released, the catcher 6 is separated from the upper extraction cavity 5, and the catcher 6 is taken down. And finishing the extraction.
As shown in figure 2, the in-situ extraction instrument works in a cleaning state and comprises an upper linear slide rail 1, an upper linear motor 2, a cylinder 3, an upper piston 4, an upper extraction cavity 5, a cleaning module 60, a pipeline module 7, a lower extraction cavity 8, a lower piston 9, a lower linear motor 10, a lower linear slide rail 11 and a support 12. Upper portion extraction chamber 5, upper portion piston 4, upper portion linear electric motor 2 installs on cylinder 3, and follow cylinder 3 and move together, upper portion piston 4 installs on upper portion linear electric motor 2's motor shaft, be reciprocating motion in upper portion extraction chamber 5 under the promotion of motor shaft, pipeline module 7 installs on lower part extraction chamber 8, there is three pipeline inside pipeline module 7, be respectively the absorption pipeline, the extraction pipeline, release the pipeline, the upper end of motor shaft is fixed on upper portion linear slide rail 1, spacing upper portion piston 4 is linear motion, the motor shaft of lower part linear electric motor 10 promotes lower part piston 9 and is reciprocating motion in lower part extraction chamber 8, the lower extreme of motor shaft is fixed on lower part linear slide rail 11, spacing lower part piston 4 is linear motion.
Before cleaning, the cylinder 3 is firstly lifted to the highest position, the upper piston 4 is lowered to the lowest position in the upper extraction cavity 5, the lower piston 9 is lifted to the highest position in the lower extraction cavity 8, the cleaning module 60 is installed on the pipeline module 7, the cylinder 3 is lowered after the installation, the upper extraction cavity 5, the cleaning module 60, the management module 7 and the lower extraction cavity 8 are connected together to form a pipeline passage, the suction pipeline is selected through the switching of an electromagnetic valve in the pipeline module 7, the upper piston 4 moves upwards to suck cleaning liquid into the upper extraction cavity 5, the upper piston 4 is lifted to the highest position at the moment, the pipeline in the pipeline module 7 is switched to the extraction pipeline after the completion, the upper extraction cavity 5 and the lower extraction cavity 8 are connected into a passage, the upper piston 4 and the lower piston 8 reciprocate up and down simultaneously to push the cleaning liquid to circularly flow between the upper extraction cavity 5 and the lower extraction cavity 8, and cleaning the whole pipeline.
After the washing is accomplished, upper portion piston 4, lower part piston 8 all move to highest position, and pipeline module 7 switches the pipeline to releasing the pipeline, and upper portion piston 4 downstream releases the washing liquid in upper portion extraction chamber 5, and pipeline module 7 switches the pipeline again and to absorbing the pipeline, will wash in liquid absorbs upper portion extraction chamber 5, and pipeline module 7 switches the pipeline to the extraction pipeline, begins to wash.
And repeating the steps until the cleaning requirement is met, releasing the cleaning liquid in the upper extraction cavity 5, finishing the lifting of the rear cylinder 3, separating the cleaning module 60 from the upper extraction cavity 5, and taking down the capturing and cleaning module 60. And finishing the cleaning.
The working process of the invention when used for flue gas analysis is as follows:
the method comprises the steps of trapping particulate matters in smoke of the cigarettes by using a trap 6 provided with a Cambridge filter disc, installing the trap 6 on a pipeline module 7 on the premise of not opening the trap after trapping is completed, extracting by using isopropanol containing certain concentration internal standard ethanol or methanol as an extracting agent, and effectively trapping and extracting related components in the smoke of the cigarettes in the process.
Finally, it should be noted that the above embodiments are only intended to describe the technical solution of the present invention and not to limit the technical method, the present invention can be extended to other modifications, changes, applications and embodiments in application, and all such modifications, changes, applications, embodiments are therefore considered to be within the spirit and teaching scope of the present invention.

Claims (5)

1. The in-situ extraction instrument suitable for measuring moisture in flue gas comprises an extraction unit and a support (12), and is characterized in that the extraction unit is mounted on the support (12) and comprises an upper linear slide rail (1), an upper linear motor (2), a cylinder (3), an upper piston (4), an upper extraction cavity (5), a trap (6), a pipeline module (7), a lower extraction cavity (8), a lower piston (9), a lower linear motor (10) and a lower linear slide rail (11), wherein the upper linear motor (2), the upper piston (4) and the upper extraction cavity (5) are mounted on the cylinder (3) and move together with the cylinder (3); the upper piston (4) is arranged on a motor shaft of the upper linear motor (2) and reciprocates in the upper extraction cavity (5) under the pushing of the motor shaft, and the upper end of the motor shaft is fixed on the upper linear slide rail (1) and limits the upper piston (4) to do linear motion; the pipeline module (7) is arranged on the lower extraction cavity (8), three pipelines are arranged in the pipeline module (7) and respectively comprise a suction pipeline, an extraction pipeline and a release pipeline, a motor shaft of the lower linear motor (10) pushes the lower piston (9) to reciprocate in the lower extraction cavity (8), the lower end of the motor shaft is fixed on the lower linear slide rail (11), and the lower piston (9) is limited to do linear motion; the lower extraction chamber (8) is fixed on the bracket (12), and the catcher (6) is arranged between the pipeline module (7) and the upper extraction chamber (5).
2. The in-situ extractor suitable for measuring moisture in flue gas as claimed in claim 1, wherein the extraction unit is multiple and is fixed side by side in multiple groups.
3. The in-situ extractor for moisture determination in flue gases according to claim 1, wherein the extraction unit further comprises a cleaning module (60), the cleaning module (60) being installed between the piping module (7) and the upper extraction chamber (5).
4. The in-situ extraction instrument suitable for measuring moisture in flue gas according to claim 2, wherein the pipeline module (7) is made of corrosion-resistant material, and the pipeline is automatically switched inside through an electromagnetic valve.
5. The in-situ extractor for moisture determination in flue gases according to claim 1, wherein the upper extraction chamber (5) and the lower extraction chamber (8) are made of transparent quartz glass.
CN202020775795.4U 2020-05-12 2020-05-12 In-situ extraction instrument suitable for measuring moisture in flue gas Active CN212693409U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202020775795.4U CN212693409U (en) 2020-05-12 2020-05-12 In-situ extraction instrument suitable for measuring moisture in flue gas

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202020775795.4U CN212693409U (en) 2020-05-12 2020-05-12 In-situ extraction instrument suitable for measuring moisture in flue gas

Publications (1)

Publication Number Publication Date
CN212693409U true CN212693409U (en) 2021-03-12

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ID=74887064

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202020775795.4U Active CN212693409U (en) 2020-05-12 2020-05-12 In-situ extraction instrument suitable for measuring moisture in flue gas

Country Status (1)

Country Link
CN (1) CN212693409U (en)

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