CN212328304U - Boric acid monoester preparation check out test set - Google Patents

Boric acid monoester preparation check out test set Download PDF

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Publication number
CN212328304U
CN212328304U CN202020903084.0U CN202020903084U CN212328304U CN 212328304 U CN212328304 U CN 212328304U CN 202020903084 U CN202020903084 U CN 202020903084U CN 212328304 U CN212328304 U CN 212328304U
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pipe
kettle body
connecting piece
sealing cover
fixing
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CN202020903084.0U
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Chinese (zh)
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韩军
潘永清
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Boxing County Shasuo New Materials Co ltd
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Boxing County Shasuo New Materials Co ltd
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Abstract

A device for preparing and detecting boric acid monoester comprises a fixed seat, a connecting piece, a feeding pipe, a first sealing cover, a fixed piece, a press-out pipe, a first cleaning pipe, a second cleaning pipe, a stirring shaft, a heating piece, a fixed ring and a kettle body; the kettle body is arranged on the fixed seat in a sliding manner; the fixed seat is provided with a heat-insulating layer, and the heating element is arranged on the fixed seat and positioned between the kettle body and the heat-insulating layer; the bolt penetrates through the fixed block and is in threaded connection with the fixed seat; the connecting piece is provided with a second sealing cover, the stirring shaft is arranged at the output end of the motor and penetrates through the second sealing cover to extend into the kettle body, the fixing sleeve is provided with a blind hole and is in sliding connection with the stirring shaft, and the locking piece penetrates through the fixing sleeve and is in threaded connection with the stirring shaft; the water spray pipe is communicated with the annular groove on the connecting piece; one end of the first cleaning pipe in the kettle body is connected with the connecting piece and communicated with the annular groove. The utility model discloses reaction rate is faster, and preparation back reation kettle washs convenient more totally, need not unpack apart the manual cleaning, safe and reliable, and efficient.

Description

Boric acid monoester preparation check out test set
Technical Field
The utility model relates to a boric acid monoester makes equipment technical field, especially relates to a boric acid monoester preparation check out test set.
Background
The boric acid monoester is a product obtained by esterifying boric acid according to different ingredients, and the product has various excellent characteristics; when the boric acid monoester is manufactured, raw materials are required to be mixed and stirred to be subjected to a partial reaction, and a required product is obtained after distillation; the existing boric acid monoester reaction kettle only has a stirring function and is slow in reaction, and the reaction kettle needs to be manually disassembled after the reaction is finished, and residues in the reaction kettle are cleaned, so that the reaction kettle does not have an automatic cleaning function; some reactants are corrosive and hazardous, so that the method is not beneficial to human bodies and has high risk; in order to solve the problems, the application provides a device for preparing and detecting the boric acid monoester.
SUMMERY OF THE UTILITY MODEL
Objects of the invention
For solving the technical problem who exists among the background art, the utility model provides a boric acid monoester preparation check out test set, reaction rate is faster, and reation kettle washs convenient more totally after the preparation, need not unpack apart the manual cleaning, safe and reliable, and efficient.
(II) technical scheme
The utility model provides a boric acid monoester preparation detection equipment, which comprises a fixed seat, a connecting piece, a fixed block, a bolt, a feeding pipe, a first sealing cover, a fixed piece, a press-out pipe, a first connecting head, a first cleaning pipe, a second connecting head, a second cleaning pipe, a stirring shaft, a fixed sleeve, a locking piece, a heating piece, a fixed ring and a kettle body; the fixed seat is provided with a groove, and the kettle body is arranged on the fixed seat in a sliding manner and is positioned in the groove; the fixed seat is provided with a heat-insulating layer, and the heating element is arranged on the fixed seat and positioned between the kettle body and the heat-insulating layer; the fixing block is arranged on the connecting piece, a through hole is formed in the fixing block, a threaded hole is correspondingly formed in the fixing seat, and the bolt penetrates through the fixing block and is in threaded connection with the fixing seat; the connecting piece is provided with a second sealing cover, and the feeding pipe is arranged on the second sealing cover and is connected with the first sealing cover; the fixing piece is arranged on the second sealing cover, and a motor is arranged on the fixing piece; the stirring shaft is arranged at the output end of the motor and penetrates through the second sealing cover to extend into the kettle body, the fixing sleeve is provided with a blind hole and is in sliding connection with one end of the stirring shaft away from the motor, and the fixing sleeve is provided with a stirrer; one end of the stirring shaft, which is far away from the motor, is provided with a threaded hole, and the locking part passes through the fixed sleeve and is in threaded connection with the stirring shaft; the pressure outlet pipe is arranged on the second sealing cover and extends into the kettle body, and the fixing ring is arranged on the pressure outlet pipe and is connected with the kettle body; the first connecting joint is arranged on the extrusion pipe and is connected with the air pipe; the connecting piece is provided with an annular groove and a water spraying pipe, and the water spraying pipe is communicated with the annular groove on the connecting piece; the first cleaning pipe is arranged on the second sealing cover, and one end of the first cleaning pipe, which is positioned in the kettle body, is connected with the connecting piece and communicated with the annular groove; the second connector is arranged on the first cleaning pipe and communicated with the second cleaning pipe; the liquid outlet pipe is arranged on the kettle body and communicated with the outside.
Preferably, an anti-corrosion sealing ring is arranged between the connecting piece and the fixed seat.
Preferably, the number of the fixing blocks and the bolts is two, and the fixing blocks and the bolts are distributed on the connecting piece in an aligned mode.
Preferably, the number of the stirrers is four, and the stirrers are distributed on the fixed sleeve in an aligned manner.
Preferably, the number of the water spray pipes is multiple groups, and the water spray pipes are distributed on the connecting piece in an aligned mode.
Preferably, the spray pipe is provided with a nozzle, and the spraying direction of the nozzle faces the inner circumferential surface of the kettle body.
Preferably, a control valve is arranged on the liquid outlet pipe.
The above technical scheme of the utility model has following profitable technological effect: when the stirring device works, the first sealing cover is firstly opened, then boric acid and materials to be reacted are poured into the kettle body through the feeding pipe, then the heating element and the motor are started, the motor works and drives the stirring shaft rotating shaft through the rotating shaft, and the stirrer is arranged on the fixing sleeve which is locked with the stirring shaft through the locking element, so that the stirrer is convenient to disassemble; the stirrer rotates to stir the materials, and meanwhile, the heating element heats the kettle body, so that the reaction is more sufficient and faster; the heat preservation layer on the kettle body reduces heat loss, a control valve on the liquid outlet pipe is opened after the reaction for reducing energy consumption is finished, and the gas pump is started to convey gas into the kettle body through the extrusion pipe to extrude liquid; finally, cleaning fluid enters the annular groove of the connecting piece through the second cleaning pipe and the first cleaning pipe and is sprayed into the kettle body through the water spraying pipe and the spray head to be cleaned; the reaction kettle is more convenient and clean to clean, does not need to be disassembled for manual cleaning, and is safe, reliable and high in efficiency.
Drawings
Fig. 1 is the utility model provides a structural schematic diagram of boric acid monoester preparation check out test set.
Fig. 2 is the utility model provides a schematic diagram of a section of boric acid monoester preparation check out test set.
Fig. 3 is the utility model provides a structural schematic diagram of connecting piece in boric acid monoester preparation check out test set.
Reference numerals: 1. a fixed seat; 2. a connecting member; 3. a fixed block; 4. a bolt; 5. a feed pipe; 6. a first sealing cover; 7. a second sealing cover; 8. a fixing member; 9. a motor; 10. pressing a pipe out; 11. a first connector; 12. a first cleaning pipe; 13. a second connector; 14. a second cleaning pipe; 15. a heat-insulating layer; 16. an annular groove; 17. a stirring shaft; 18. a stirrer; 19. fixing a sleeve; 20. a locking member; 21. a heating member; 22. a fixing ring; 23. a water spray pipe; 24. a kettle body; 25. a liquid outlet pipe.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in detail with reference to the accompanying drawings. It should be understood that the description is intended to be illustrative only and is not intended to limit the scope of the present invention. Moreover, in the following description, descriptions of well-known structures and techniques are omitted so as to not unnecessarily obscure the concepts of the present invention.
As shown in fig. 1-3, the utility model provides a device for detecting the preparation of boric acid monoester, which comprises a fixed seat 1, a connecting piece 2, a fixed block 3, a bolt 4, a feeding pipe 5, a first sealing cover 6, a fixed piece 8, a press-out pipe 10, a first connecting head 11, a first cleaning pipe 12, a second connecting head 13, a second cleaning pipe 14, a stirring shaft 17, a fixed sleeve 19, a locking piece 20, a heating piece 21, a fixed ring 22 and a kettle body 24; a groove is arranged on the fixed seat 1, and the kettle body 24 is arranged on the fixed seat 1 in a sliding manner and is positioned in the groove; the fixed seat 1 is provided with a heat-insulating layer 15, and the heating element 21 is arranged on the fixed seat 1 and positioned between the kettle body 24 and the heat-insulating layer 15; the fixing block 3 is arranged on the connecting piece 2, a through hole is formed in the fixing block 3, a threaded hole is correspondingly formed in the fixing seat 1, and the bolt 4 penetrates through the fixing block 3 and is in threaded connection with the fixing seat 1; a second sealing cover 7 is arranged on the connecting piece 2, and the feeding pipe 5 is arranged on the second sealing cover 7 and connected with the first sealing cover 6; the fixing piece 8 is arranged on the second sealing cover 7, and the fixing piece 8 is provided with a motor 9; the stirring shaft 17 is arranged at the output end of the motor 9 and penetrates through the second sealing cover 7 to extend into the kettle body 24, the fixing sleeve 19 is provided with a blind hole and is in sliding connection with one end of the stirring shaft 17 far away from the motor 9, and the fixing sleeve 19 is provided with a stirrer 18; a threaded hole is formed in one end, far away from the motor 9, of the stirring shaft 17, and the locking piece 20 penetrates through the fixing sleeve 19 and is in threaded connection with the stirring shaft 17; the press-out pipe 10 is arranged on the second sealing cover 7 and extends into the kettle body 24, and the fixing ring 22 is arranged on the press-out pipe 10 and is connected with the kettle body 24; the first connecting head 11 is arranged on the extrusion pipe 10 and is connected with the air pipe; the connecting piece 2 is provided with an annular groove 16 and a spray pipe 23, and the spray pipe 23 is communicated with the annular groove 16 on the connecting piece 2; the first cleaning pipe 12 is arranged on the second sealing cover 7, and one end of the first cleaning pipe 12, which is positioned in the kettle body 24, is connected with the connecting piece 2 and communicated with the annular groove 16; the second connector 13 is arranged on the first cleaning pipe 12 and communicated with the second cleaning pipe 14; the liquid outlet pipe 25 is arranged on the kettle body 24 and communicated with the outside.
In an alternative embodiment, an anti-corrosion sealing ring is arranged between the connecting piece 2 and the fixed seat 1, so that the sealing performance is improved.
In an alternative embodiment, the number of the fixing blocks 3 and the bolts 4 is two, and the fixing blocks and the bolts are distributed on the connecting member 2 in an aligned manner.
In an alternative embodiment, the stirrers 18 are four in number and are distributed in a row on the jacket 19.
In an alternative embodiment, the number of spray pipes 23 is multiple and they are distributed in a row on the connector 2.
In an alternative embodiment, the spray pipes 23 are provided with spray heads, and the spray direction of the spray heads faces the inner circumferential surface of the kettle body 24, so that the spray is more comprehensive and the cleaning is cleaner.
In an alternative embodiment, drain 25 is provided with a control valve.
In the utility model, when in work, the first sealing cover 6 is firstly opened, then the boric acid and the material to be reacted are poured into the kettle body 24 through the feeding pipe 5, then the heating element 21 and the motor 9 are started, the motor 9 works and drives the rotating shaft 17 through the rotating shaft, as the stirrer 18 is arranged on the fixing sleeve 19, and the fixing sleeve 19 is locked with the stirring shaft 17 through the locking element 20, the stirrer is convenient to be detached; the stirrer 18 rotates to stir the materials, and meanwhile, the heating element 21 heats the kettle body 24, so that the reaction is more sufficient and faster; the heat preservation layer 15 on the kettle body 24 reduces heat loss, a control valve on the liquid outlet pipe 25 is opened after the reaction for reducing energy consumption is finished, and the gas pump is started to convey gas into the kettle body 24 through the pressure outlet pipe 10 to press out liquid; finally, cleaning liquid enters the annular groove 16 of the connecting piece 2 through the second cleaning pipe 14 and the first cleaning pipe 12 and is sprayed into the kettle body 24 through the water spraying pipe 23 and the spray head for cleaning; the reaction kettle is more convenient and clean to clean, does not need to be disassembled for manual cleaning, and is safe, reliable and high in efficiency.
It is to be understood that the above-described embodiments of the present invention are merely illustrative of or explaining the principles of the invention and are not to be construed as limiting the invention. Therefore, any modification, equivalent replacement, improvement and the like made without departing from the spirit and scope of the present invention should be included in the protection scope of the present invention. Further, it is intended that the appended claims cover all such variations and modifications as fall within the scope and boundaries of the appended claims or the equivalents of such scope and boundaries.

Claims (7)

1. The equipment for preparing and detecting the boric acid monoester is characterized by comprising a fixed seat (1), a connecting piece (2), a fixed block (3), a bolt (4), a feeding pipe (5), a first sealing cover (6), a fixed piece (8), a press-out pipe (10), a first connecting head (11), a first cleaning pipe (12), a second connecting head (13), a second cleaning pipe (14), a stirring shaft (17), a fixed sleeve (19), a locking piece (20), a heating piece (21), a fixed ring (22) and a kettle body (24); a groove is arranged on the fixed seat (1), and the kettle body (24) is arranged on the fixed seat (1) in a sliding manner and is positioned in the groove; the fixed seat (1) is provided with a heat-insulating layer (15), and the heating element (21) is arranged on the fixed seat (1) and positioned between the kettle body (24) and the heat-insulating layer (15); the fixing block (3) is arranged on the connecting piece (2), a through hole is formed in the fixing block (3), a threaded hole is correspondingly formed in the fixing seat (1), and the bolt (4) penetrates through the fixing block (3) and is in threaded connection with the fixing seat (1); a second sealing cover (7) is arranged on the connecting piece (2), and the feeding pipe (5) is arranged on the second sealing cover (7) and is connected with the first sealing cover (6); the fixing piece (8) is arranged on the second sealing cover (7), and the fixing piece (8) is provided with a motor (9); the stirring shaft (17) is arranged at the output end of the motor (9) and extends into the kettle body (24) through the second sealing cover (7), the fixing sleeve (19) is provided with a blind hole and is in sliding connection with one end of the stirring shaft (17) far away from the motor (9), and the fixing sleeve (19) is provided with a stirrer (18); a threaded hole is formed in one end, far away from the motor (9), of the stirring shaft (17), and the locking piece (20) penetrates through the fixing sleeve (19) and is in threaded connection with the stirring shaft (17); the press-out pipe (10) is arranged on the second sealing cover (7) and extends into the kettle body (24), and the fixing ring (22) is arranged on the press-out pipe (10) and is connected with the kettle body (24); the first connecting head (11) is arranged on the extrusion pipe (10) and is connected with the air pipe; the connecting piece (2) is provided with an annular groove (16) and a water spray pipe (23), and the water spray pipe (23) is communicated with the annular groove (16) on the connecting piece (2); the first cleaning pipe (12) is arranged on the second sealing cover (7), and one end of the first cleaning pipe (12) positioned in the kettle body (24) is connected with the connecting piece (2) and communicated with the annular groove (16); the second connector (13) is arranged on the first cleaning pipe (12) and communicated with the second cleaning pipe (14); the liquid outlet pipe (25) is arranged on the kettle body (24) and is communicated with the outside.
2. The equipment for preparing and detecting the boric acid monoester according to claim 1, wherein an anti-corrosion sealing ring is arranged between the connecting piece (2) and the fixed seat (1).
3. The apparatus for preparing and detecting the boric acid monoester according to claim 1, wherein the number of the fixing blocks (3) and the bolts (4) is two groups, and the fixing blocks and the bolts are distributed on the connecting piece (2) in an aligned manner.
4. The apparatus for detecting the preparation of a boronic acid monoester according to claim 1, wherein the number of the stirrers (18) is four, and the stirrers are distributed in a row on the fixing sleeve (19).
5. The apparatus for preparing and detecting the boric acid monoester according to claim 1, wherein the number of the water spraying pipes (23) is multiple, and the water spraying pipes are distributed on the connecting piece (2) in an aligned manner.
6. The apparatus for preparing and detecting the boric acid monoester according to claim 1, wherein the spray nozzle is arranged on the spray pipe (23), and the spraying direction of the spray nozzle faces to the inner circumferential surface of the kettle body (24).
7. The apparatus for preparing and detecting the boric acid monoester according to claim 1, wherein the liquid outlet pipe (25) is provided with a control valve.
CN202020903084.0U 2020-05-25 2020-05-25 Boric acid monoester preparation check out test set Active CN212328304U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202020903084.0U CN212328304U (en) 2020-05-25 2020-05-25 Boric acid monoester preparation check out test set

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202020903084.0U CN212328304U (en) 2020-05-25 2020-05-25 Boric acid monoester preparation check out test set

Publications (1)

Publication Number Publication Date
CN212328304U true CN212328304U (en) 2021-01-12

Family

ID=74084340

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202020903084.0U Active CN212328304U (en) 2020-05-25 2020-05-25 Boric acid monoester preparation check out test set

Country Status (1)

Country Link
CN (1) CN212328304U (en)

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