CN211752836U - Zirconium oxychloride crystal separation and suction filtration tank - Google Patents

Zirconium oxychloride crystal separation and suction filtration tank Download PDF

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Publication number
CN211752836U
CN211752836U CN201922295853.3U CN201922295853U CN211752836U CN 211752836 U CN211752836 U CN 211752836U CN 201922295853 U CN201922295853 U CN 201922295853U CN 211752836 U CN211752836 U CN 211752836U
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China
Prior art keywords
filter plate
jar
zirconium oxychloride
suction filtration
jar body
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Active
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CN201922295853.3U
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Chinese (zh)
Inventor
刘振明
刘福来
刘敬东
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Shandong Hongyuan New Material Technology Co ltd
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Shandong Hongyuan New Materials Co ltd
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Abstract

The utility model discloses a zirconium oxychloride crystal separation suction filtration jar, including a jar body, set up the internal filter plate in jar, the center department of filter plate lower, be the flute profile setting, the top of filter plate is equipped with the (mixing) shaft, is equipped with stirring vane on the (mixing) shaft, the (mixing) shaft is by the motion of motor reducer, the top of the jar body is equipped with leacheate import, feed inlet and extraction opening, the lower part of the jar body is equipped with the discharge gate, the discharge gate is at internal connection play material pipe of jar, the one end of play material pipe sees through the center department that the filter plate arrived the filter plate, the other end and the discharge gate intercommunication of play material pipe, the bottom of. The device can prevent the existence of volatile gas in production environment, and the stirring is more abundant, and the stirring in-process lotion flows fully and is convenient for remove and attaches impurity, makes things convenient for drip washing many times.

Description

Zirconium oxychloride crystal separation and suction filtration tank
Technical Field
The utility model relates to a separating device, in particular to a zirconium oxychloride crystal separation suction filtration tank.
Background
The application of high-purity zirconium oxychloride as an important chemical and metallurgical raw material is increasingly wide, and the process flow for industrially producing the high-purity zirconium oxychloride is as follows: alkali fusion → water transfer → acidification → water dissolving → concentration → acid washing → water dissolving concentration acid washing of high purity zirconium oxychloride.
In the prior art, pickling is usually carried out through a pickling tank, and stirring is carried out through a movable stirring vehicle.
The problems of the above process are:
(1) in the acid washing process, volatile acid gas exists in the production environment, and protection and recovery equipment is required to be equipped.
(2) In the acid process, for materials at a certain position, stirring is intermittent and insufficient.
(3) During the stirring process, the washing liquid has relatively poor fluidity, which is not beneficial to removing impurities.
(4) In the pickling process, repeated rinsing is inconvenient, and impurities are fully removed.
SUMMERY OF THE UTILITY MODEL
The to-be-solved technical problem of the utility model is to provide a zirconium oxychloride crystal separation suction filtration jar, the device can prevent the existence of volatile gas in the production environment, and the stirring is more abundant, and stirring in-process lotion flows and is fully convenient for remove and attaches impurity, convenient many times drip washing.
In order to solve the above technical problem, the utility model discloses a following technical means:
the utility model provides a zirconium oxychloride crystal separation suction filtration jar, includes a jar body, sets up the internal filter plate in jar, the center department of filter plate lower, be the flute profile setting, the top of filter plate is equipped with the (mixing) shaft, be equipped with stirring vane on the (mixing) shaft, the (mixing) shaft is by the motion of motor reducer, the top of jar body is equipped with leacheate import, feed inlet and extraction opening, the lower part of jar body is equipped with the discharge gate, the discharge gate is at the internal connecting discharging pipe of jar, discharging pipe's one end sees through the filter plate and arrives the center department of filter plate, discharging pipe's the other end and discharge gate intercommunication, the bottom.
Compared with the prior art, the outstanding characteristics are that:
through setting up the leakproofness jar body, get into the zirconium oxychloride crystal through the top feed inlet at the cylinder body, the center department of filter plate is lower, it makes the internal material of jar change and concentrates to be the flute profile setting, be convenient for the drip washing is accomplished and is derived the material through ejection of compact pipe, and be convenient for be equipped with stirring vane intensive mixing material through setting up in the top of filter plate and carry out the drip washing in order to detach impurity, the drip washing liquid flows to the filter plate below through mother liquor water outlet through the filter plate seepage, the aforesaid sets up and makes the existence of this device in production environment that can prevent volatile gas, the stirring is more abundant, the stirring in-process lotion flows and is fully convenient for remove and attaches impurity, convenient many times drip.
The further preferred technical scheme is as follows:
the filter plate is in a cone shape.
The conical filter plate is convenient for collecting materials, and stirring blades arranged above the filter plate can be fully utilized for stirring and leaching.
The bottom support frame is arranged below the bottom end of the filter plate, a support column is arranged on the bottom support frame, a support seat is arranged at the top end of the support column, and the support seat supports the filter plate.
Through setting up the bottom sprag frame, be convenient for form the support to the filter plate, improve the stability of this device, the bottom sprag frame sets up in filter plate bottom below, is convenient for improve the effective filter area of filter plate.
The top end below of filter plate be equipped with jar body mount, jar body mount is fixed along jar internal side wall and is set up.
Through setting up jar body mount, further improve the stability of the connection of filter plate, the filter plate mount can be the ring frame, also can be the arc bracket that the interval set up.
The leacheate inlet is arranged above the feeding hole.
By the arrangement, when the leacheate enters liquid, the leacheate can be directly washed to the materials entering the tank body, the leacheate and the materials flow down to the filter plate together, the falling process is mixed and washed, and the leaching effect is further improved.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Description of reference numerals: 1-an air extraction opening; 2-motor speed reducer; 3-eluent inlet; 4-a feed inlet; 5-stirring shaft; 6-discharging port; 7-mother liquor outlet; 8-a bottom support frame; 9-tank body fixing frame; 10-filter plate.
Detailed Description
Referring to fig. 1, the zirconium oxychloride crystal separation and filtration tank of the present invention comprises a tank body and a filter plate 10 disposed in the tank body; the center department of filter plate 10 is lower, is the flute profile setting, and the top of filter plate 10 is equipped with (mixing) shaft 5, (mixing) shaft 5 is last to be equipped with stirring vane, and (mixing) shaft 5 is moved by motor reducer 2, and the top of the jar body is equipped with leacheate import 3, feed inlet 4 and extraction opening 1, and the lower part of the jar body is equipped with discharge gate 6, and discharge gate 6 is internal at jar connection discharging pipe, and discharging pipe's one end sees through filter plate 10 and reaches the center department of filter plate 10, and discharging pipe's the other end and discharge gate 6 intercommunication, and the bottom of the jar.
Through setting up the leakproofness jar body, get into the zirconium oxychloride crystal through top feed inlet 4 at the cylinder body, the center department of filter plate 10 is lower, it is the flute profile setting and makes the internal material of jar more concentrate, be convenient for the drip washing is accomplished and is derived the material through ejection of compact pipe, and be convenient for be equipped with stirring vane intensive mixing material through setting up in the top of filter plate 10 and carry out the drip washing in order to detach impurity, the drip washing liquid flows to filter plate 10 below through filter plate 10 seepage and flows out through mother liquor water outlet 7, the aforesaid sets up and makes the existence of this device in production environment that can prevent volatile gas, the stirring is more abundant, the stirring in-process lotion flows and is fully convenient for remove attached impurity, convenient many times drip washing.
The filter plate 10 is in the shape of a cone.
The arrangement of the conical filter plate 10 is convenient for collecting materials, and meanwhile, the stirring blades arranged above the filter plate 10 can be fully utilized for stirring and leaching.
A bottom support frame 8 is arranged below the bottom end of the filter plate 10, a pillar is arranged on the bottom support frame 8, and a support seat is arranged at the top end of the pillar and supports the filter plate 10.
Through setting up bottom sprag 8, be convenient for form the support to filter plate 10, improve the stability of this device, bottom sprag 8 sets up in filter plate 10 bottom below, is convenient for improve the effective filter area of filter plate 10.
A tank body fixing frame 9 is arranged below the top end of the filter plate 10, and the tank body fixing frame 9 is fixedly arranged along the inner side wall of the tank body.
The connection stability of the filter plate 10 is further improved by arranging the tank body fixing frame 9, and the fixing frame of the filter plate 10 can be an annular frame or arc-shaped brackets arranged at intervals.
The eluent inlet 3 is arranged above the feed opening 4.
By the arrangement, when the leacheate enters liquid, the leacheate can directly wash the materials entering the tank body, the leacheate and the materials flow down onto the filter plate 10 together, and the flowing down process is mixed and washed, so that the leaching effect is further improved.
The above description is only a preferred and practical embodiment of the present invention, and not intended to limit the scope of the present invention, and all structural equivalents made by using the contents of the specification and drawings of the present invention are included in the scope of the present invention.

Claims (5)

1. The utility model provides a zirconium oxychloride crystal separation suction filtration jar, includes a jar body, sets up the internal filter plate in jar, its characterized in that: the center department of filter plate lower, be the flute profile setting, the top of filter plate is equipped with the (mixing) shaft, is equipped with stirring vane on the (mixing) shaft, the (mixing) shaft is moved by motor reducer, and the top of jar body is equipped with leacheate import, feed inlet and extraction opening, and the lower part of jar body is equipped with the discharge gate, and the discharge gate is at the internal material pipe that connects of jar, and the one end of material pipe sees through the filter plate and arrives the center department of filter plate, the other end and the discharge gate intercommunication of material pipe, and the bottom of jar.
2. The zirconium oxychloride crystal separation suction filtration tank of claim 1, wherein: the filter plate is in a cone shape.
3. The zirconium oxychloride crystal separation suction filtration tank of claim 2, wherein: the bottom support frame is arranged below the bottom end of the filter plate, a support column is arranged on the bottom support frame, a support seat is arranged at the top end of the support column, and the support seat supports the filter plate.
4. The zirconium oxychloride crystal separation suction filtration tank of claim 2, wherein: the top end below of filter plate be equipped with jar body mount, jar body mount is fixed along jar internal side wall and is set up.
5. The zirconium oxychloride crystal separation suction filtration tank of claim 1, wherein: the leacheate inlet is arranged above the feeding hole.
CN201922295853.3U 2019-12-19 2019-12-19 Zirconium oxychloride crystal separation and suction filtration tank Active CN211752836U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201922295853.3U CN211752836U (en) 2019-12-19 2019-12-19 Zirconium oxychloride crystal separation and suction filtration tank

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201922295853.3U CN211752836U (en) 2019-12-19 2019-12-19 Zirconium oxychloride crystal separation and suction filtration tank

Publications (1)

Publication Number Publication Date
CN211752836U true CN211752836U (en) 2020-10-27

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Application Number Title Priority Date Filing Date
CN201922295853.3U Active CN211752836U (en) 2019-12-19 2019-12-19 Zirconium oxychloride crystal separation and suction filtration tank

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115739809A (en) * 2022-11-18 2023-03-07 晨光生物科技集团股份有限公司 Crystal separation washer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115739809A (en) * 2022-11-18 2023-03-07 晨光生物科技集团股份有限公司 Crystal separation washer

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Address after: 251900 Xinhai Industrial Park, Wudi County, Binzhou City, Shandong Province

Patentee after: Shandong Hongyuan new material technology Co.,Ltd.

Address before: 251900 Xinhai Industrial Park, Wudi County, Binzhou City, Shandong Province

Patentee before: SHANDONG HONGYUAN NEW MATERIALS CO.,LTD.