CN211677692U - Eccentric stirrer for microemulsion system - Google Patents
Eccentric stirrer for microemulsion system Download PDFInfo
- Publication number
- CN211677692U CN211677692U CN201922043205.9U CN201922043205U CN211677692U CN 211677692 U CN211677692 U CN 211677692U CN 201922043205 U CN201922043205 U CN 201922043205U CN 211677692 U CN211677692 U CN 211677692U
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- Prior art keywords
- eccentric
- main journal
- bent axle
- motor
- microemulsion system
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Abstract
The utility model discloses an eccentric agitator is used to microemulsion system, including the motor, set up the motor pole in motor one end to and set up the bent axle stirring portion that just keeps away from motor one end at the motor pole, be provided with the connecting portion that is used for connecting bent axle stirring portion and motor pole between bent axle stirring portion and the motor pole, connecting portion and bent axle stirring portion and motor pole fixed connection, bent axle stirring portion includes main journal and eccentric portion, main journal and eccentric portion fixed connection. The utility model discloses as the main part of agitator with the bent axle stirring portion that has the eccentric part, utilize the characteristics of bent axle stirring portion decentraction, change the mode of current axle center stirring, can effectively avoid the microemulsion system to cause the concentration uneven distribution because of local overheat, influence the formation of nanoparticle and grow up.
Description
Technical Field
The utility model belongs to the technical field of experimental facilities, concretely relates to eccentric agitator is used to microemulsion system.
Background
The microemulsion method is a common method for synthesizing nano particles, and is characterized in that under the action of an amphiphilic molecular surfactant, two immiscible continuous media are fused to form emulsion microbubbles, each microbubble is used as an independent nano reactor, and the nano particles with controllable sizes are obtained through nucleation, coalescence, agglomeration and growth. Two mutually insoluble continuous media as reactants, wherein the micelle particles contained in the two continuous media collide with each other during the reaction, and exchange substances to initiate chemical reaction. Because the particle size of the water core in the microbubble is fixed, the water cores with different particle sizes can not exchange materials, and most of the energy absorbed by the water cores comes from the collision among the particles, the effective collision energy is obtained by controlling the effective collision times of the particles, and the method is an effective way for realizing the control of the morphology and the size of the nano particles.
Stirring is a common experimental means in a microemulsion method, the process of injecting energy into a microemulsion system by stirring is beneficial to breaking agglomeration among micelle particles, the current view is that the process of injecting energy into the microemulsion system by stirring is beneficial to generating nano particles with smaller sizes, which is mainly because the specific surface of small particles is larger and is easy to absorb the energy in the system, and the process of obtaining the nano particles with smaller particle sizes by improving the stirring speed is one of the common theories of the prior art, but the process of injecting energy by stirring is not only the generation of kinetic energy transfer, but also the exchange between another non-negligible energy, namely heat energy, exists, and in the process of injecting energy in the form of heat energy, the particles tend to aggregate and grow to form large particles.
The conventional stirring mode mostly adopts coaxial stirring, namely continuous stirring is carried out by taking the position of a stirring device or an extension line as an axis, and one view is that the stirring mode is favorable for forming a reaction system with uniform concentration in the emulsion and forming particles with uniform appearance. However, the stirring method still cannot control the generation of reaction heat, and in addition, the energy injected by stirring is too high to form nano wires or nano rods with stable and remarkable shapes by removing nano particles and other forms of nano particles such as nano wires or nano rods.
SUMMERY OF THE UTILITY MODEL
The technical problem to be solved by the utility model is to provide an eccentric stirrer for microemulsion system, which aims at the defects in the prior art. The device uses the bent axle stirring portion that has the eccentric part as the main part of agitator, utilizes the characteristics of bent axle stirring portion decentraction, changes the mode of current axle center stirring, can effectively avoid the microemulsion system to cause the concentration uneven distribution because of local overheat, influences the formation and the growth of nano-particle.
In order to solve the technical problem, the utility model discloses a technical scheme is: an eccentric agitator for a microemulsion system is characterized in that: including the motor, set up the motor shaft in motor one end to and set up the bent axle stirring portion that just keeps away from motor one end at the motor shaft, be provided with between bent axle stirring portion and the motor shaft and be used for connecting bent axle stirring portion and the connecting portion of motor shaft, connecting portion and bent axle stirring portion and motor shaft fixed connection, bent axle stirring portion includes main journal and eccentric portion, main journal and eccentric portion fixed connection.
The eccentric stirrer for the microemulsion system is characterized in that: the main journals comprise a first main journal and a second main journal, and the eccentric parts are multiple; the first main journal and the second main journal are not connected, the axial lead of the first main journal and the axial lead of the second main journal are collinear, one end of the first main journal is connected with the connecting portion, the other end of the first main journal is connected with the eccentric portion, and the second main journal is arranged between the two adjacent eccentric portions.
The eccentric stirrer for the microemulsion system is characterized in that: the first main journal is provided with threads, and the connecting part is internally provided with a threaded hole matched with the threads.
The eccentric stirrer for the microemulsion system is characterized in that: the eccentric portion includes left eccentric portion and right eccentric portion, left eccentric portion and right eccentric portion set up in turn.
The eccentric stirrer for the microemulsion system is characterized in that: the eccentric part and the main journal are integrally formed.
The eccentric stirrer for the microemulsion system is characterized in that: the number of the left eccentric parts is not equal to that of the right eccentric parts.
Compared with the prior art, the utility model has the following advantage:
1. the utility model discloses as the main part of agitator with the bent axle stirring portion that has the eccentric part, utilize the characteristics of bent axle stirring portion decentraction, change the mode of current axle center stirring, can effectively avoid the microemulsion system to cause the concentration uneven distribution because of local overheat, influence the formation of nanoparticle and grow up.
2. The utility model discloses bent axle stirring portion includes main shaft neck and eccentric portion, and direct and the different position contact of microemulsion system can in time disperse the heat that the stirring produced to other parts of system, make the microemulsion system can not cause the uneven distribution of concentration because of local heat accumulation, influence the controllable synthesis of nano-material.
3. The utility model discloses simple structure, reasonable in design does benefit to popularization and application.
The technical solution of the present invention will be described in further detail with reference to the accompanying drawings and embodiments.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a schematic view of a connection relationship between the first main journal and the connecting portion.
Description of reference numerals:
1, a motor; 2-motor shaft; 3-a connecting part;
4-1 — left eccentric portion; 4-2-right eccentric portion; 4-3 — a first main journal;
4-second main journal.
Detailed Description
Example 1
As shown in fig. 1 and 2, the eccentric stirrer for a microemulsion system of the present embodiment includes a motor 1, a motor rod 2 disposed at one end of the motor 1, and a crankshaft stirring portion disposed at the motor rod 2 and far away from one end of the motor 1, a connecting portion 3 disposed between the crankshaft stirring portion and the motor rod 2 and used for connecting the crankshaft stirring portion and the motor rod 2, the connecting portion 3 and the crankshaft stirring portion and the motor rod 2 are fixedly connected, the crankshaft stirring portion includes a main journal and an eccentric portion, and the main journal and the eccentric portion are fixedly connected. The device uses the bent axle stirring portion that has the eccentric part as the main part of agitator, utilizes the characteristics of bent axle stirring portion decentraction, changes the mode of current axle center stirring, can effectively avoid the microemulsion system to cause the concentration uneven distribution because of local overheat, influences the formation and the growth of nano-particle.
As shown in fig. 1 and 2, the eccentric stirrer for a microemulsion system of the present embodiment includes a first main journal 4-3 and a second main journal 4-4, and the number of the eccentric portions is plural; the first main journal 4-3 and the second main journal 4-4 are not connected, the axial lead of the first main journal 4-3 and the axial lead of the second main journal 4-4 are collinear, one end of the first main journal 4-3 is connected with the connecting portion 3, the other end of the first main journal 4-3 is connected with the eccentric portion, and the second main journal 4-4 is arranged between two adjacent eccentric portions. The main journal of the crankshaft stirring part and the eccentric part rotate to directly contact with different parts of the microemulsion system, and heat generated by stirring can be timely dispersed to other parts of the system, so that the microemulsion system cannot influence the controllable synthesis of the nano material due to uneven concentration distribution caused by local heat accumulation.
As shown in fig. 2, in the eccentric agitator for a microemulsion system of this embodiment, the first main journal 4-3 is provided with a thread, and the connecting portion 3 is provided with a threaded hole matching with the thread. The crankshaft stirring part is connected with the connecting part through threads, so that the crankshaft stirring part is convenient to disassemble and assemble.
As shown in FIG. 1, in the eccentric agitator for a microemulsion system according to the present embodiment, the eccentric portion includes a left eccentric portion 4-1 and a right eccentric portion 4-2, and the left eccentric portion 4-1 and the right eccentric portion 4-2 are alternately disposed. Through the left eccentric part and the right eccentric part which are alternately arranged, the contact area of the stirrer and a microemulsion system is increased, and meanwhile, the eccentric rotation of the stirrer is more favorably realized.
As shown in fig. 1, in the eccentric agitator for a microemulsion system of the present embodiment, the eccentric portion and the main journal are integrally formed. The eccentric part and the main journal are integrally formed, so that impurities are not introduced into the microemulsion system due to the contact of the connecting joint part and the microemulsion system, and the synthesis of the nano material is not influenced.
As shown in FIG. 1, in the eccentric agitator for a microemulsion system of the present embodiment, the number of the left eccentric portions 4-1 is not equal to the number of the right eccentric portions 4-2. The quantity of left eccentric portion is not equal with the quantity of right eccentric portion, is favorable to realizing the stability of agitator, improves stirring efficiency.
The installation and use method of the eccentric stirrer for the microemulsion system comprises the following steps: and (3) screwing one end with threads of the first main journal 4-3 into a threaded hole of the connecting part 3 to finish assembly, placing the assembled stirrer in the microemulsion reaction liquid, turning on a switch of the motor 1, rotating the motor rod 2 to drive a crankshaft stirring part to rotate, and simultaneously rotating the main journal of the crankshaft stirring part, the left eccentric part 4-1 and the right eccentric part 4-2 to realize the eccentric stirring of the microemulsion.
The above, only be the utility model discloses a preferred embodiment, it is not right the utility model discloses do any restriction, all according to the utility model discloses the technical entity all still belongs to any simple modification, change and the equivalent structure change of doing above embodiment the utility model discloses technical scheme's within the scope of protection.
Claims (6)
1. An eccentric agitator for a microemulsion system is characterized in that: including motor (1), set up motor rod (2) in motor (1) one end to and set up at motor rod (2) and keep away from bent axle stirring portion of motor (1) one end, be provided with connecting portion (3) that are used for connecting bent axle stirring portion and motor rod (2) between bent axle stirring portion and motor rod (2), connecting portion (3) and bent axle stirring portion and motor rod (2) fixed connection, bent axle stirring portion includes main journal and eccentric portion, main journal and eccentric portion fixed connection.
2. The eccentric agitator for a microemulsion system according to claim 1, wherein: the main journal comprises a first main journal (4-3) and a second main journal (4-4), and the eccentric part is multiple; the first main journal (4-3) and the second main journal (4-4) are not connected and the axial lead of the first main journal (4-3) and the axial lead of the second main journal (4-4) are collinear, one end of the first main journal (4-3) is connected with the connecting part (3), the other end of the first main journal (4-3) is connected with the eccentric part, and the second main journal (4-4) is arranged between two adjacent eccentric parts.
3. The eccentric agitator for a microemulsion system according to claim 2, wherein: the first main journal (4-3) is provided with threads, and the connecting part (3) is internally provided with a threaded hole matched with the threads.
4. The eccentric agitator for a microemulsion system according to claim 1 or 2, wherein: the eccentric part comprises a left eccentric part (4-1) and a right eccentric part (4-2), and the left eccentric part (4-1) and the right eccentric part (4-2) are alternately arranged.
5. The eccentric agitator for a microemulsion system according to claim 1, wherein: the eccentric part and the main journal are integrally formed.
6. The eccentric agitator for a microemulsion system according to claim 4, wherein: the number of the left eccentric parts (4-1) is not equal to the number of the right eccentric parts (4-2).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201922043205.9U CN211677692U (en) | 2019-11-22 | 2019-11-22 | Eccentric stirrer for microemulsion system |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201922043205.9U CN211677692U (en) | 2019-11-22 | 2019-11-22 | Eccentric stirrer for microemulsion system |
Publications (1)
Publication Number | Publication Date |
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CN211677692U true CN211677692U (en) | 2020-10-16 |
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CN201922043205.9U Expired - Fee Related CN211677692U (en) | 2019-11-22 | 2019-11-22 | Eccentric stirrer for microemulsion system |
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CN (1) | CN211677692U (en) |
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2019
- 2019-11-22 CN CN201922043205.9U patent/CN211677692U/en not_active Expired - Fee Related
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20201016 Termination date: 20211122 |
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CF01 | Termination of patent right due to non-payment of annual fee |