CN210385826U - Reaction device for producing silica sol - Google Patents
Reaction device for producing silica sol Download PDFInfo
- Publication number
- CN210385826U CN210385826U CN201920652176.3U CN201920652176U CN210385826U CN 210385826 U CN210385826 U CN 210385826U CN 201920652176 U CN201920652176 U CN 201920652176U CN 210385826 U CN210385826 U CN 210385826U
- Authority
- CN
- China
- Prior art keywords
- mixing drum
- silica sol
- mixing
- blanking plate
- churn
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 39
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 238000002156 mixing Methods 0.000 claims abstract description 44
- 238000003756 stirring Methods 0.000 claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 8
- 239000007788 liquid Substances 0.000 abstract description 22
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract description 21
- 239000011863 silicon-based powder Substances 0.000 abstract description 21
- 238000007667 floating Methods 0.000 abstract description 10
- 238000000034 method Methods 0.000 description 8
- 239000000843 powder Substances 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 229910052739 hydrogen Inorganic materials 0.000 description 6
- 239000001257 hydrogen Substances 0.000 description 6
- 238000007670 refining Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000003513 alkali Substances 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000013590 bulk material Substances 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 235000013312 flour Nutrition 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005495 investment casting Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 239000011819 refractory material Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
Images
Landscapes
- Silicon Compounds (AREA)
Abstract
The utility model provides a reaction unit for silica sol production, including the churn that the level set up, the churn bottom is equipped with the supporting leg, is equipped with the (mixing) shaft in the churn, is equipped with a plurality of stirring vane on the (mixing) shaft, and the (mixing) shaft passes through agitator motor drive, and the churn upside is equipped with the loading hopper, is equipped with blanking plate in the loading hopper, is equipped with blanking hole on the blanking plate, and the churn top is equipped with filling tube and blast pipe, and churn one end bottom is equipped with the bin outlet, is equipped with the valve on the bin outlet, and the. The device can reduce the floating amount of the silicon powder on the liquid surface and improve the reaction rate.
Description
Technical Field
The utility model belongs to silica sol production facility field, in particular to a reaction unit for silica sol production.
Background
The silica sol is a dispersion of nano-silica with the particle size of 1-100 nanometers in water or other organic solvents, and is widely applied to the fields of precision casting, refractory materials, coatings, spinning, precision polishing and the like.
The domestic silica sol production technology mainly comprises an ion exchange method and a silica powder hydrolysis method. In the production process of the silicon powder hydrolysis method, the reaction is carried out in a reaction kettle with mechanical stirring, a common reaction kettle is vertically arranged, and laminar flow is easily generated in the stirring process; the silicon powder can generate hydrogen in the reaction process, and part of the hydrogen can be attached to the fine silicon powder in the reaction process, so that the fine silicon powder floats to the liquid level to form a thick layer of floating objects. Because the silicon powder can be well hydrolyzed only by fully mixing and contacting with the alkali liquor, the silicon powder floating on the liquid surface can not be fully contacted with the liquid, and the reaction speed is reduced. For example, in the conventional solution, CN206008722U adopts a water pump to circularly convey the liquid at the bottom of the reaction kettle to the upper end of the reaction kettle, so as to improve the contact with the silicon powder floating on the liquid surface, but as the reaction proceeds, the liquid at the bottom of the reaction kettle is sticky and easily blocks the water pump; moreover, the liquid to be conveyed cannot be uniformly sprinkled on the silicon powder, and a part of the silicon powder still cannot be in good contact with the liquid.
The existing reaction device generally adds the needed silicon powder and alkali liquor into the reaction device at one time, a large amount of hydrogen is generated by reaction, a pump pot, namely a reaction kettle, is easy to boil, and a large amount of raw material liquid overflows along with a guide pipe. In order to prevent the pan pumping phenomenon, the silicon powder can only be added manually in batches, the participation of operators is high, the feeding time needs to be controlled, and the operation is complicated.
Disclosure of Invention
The utility model aims to solve the technical problem that a reaction unit for silica sol production is provided, reduces the showy volume of liquid level silica flour, improves reaction rate.
In order to solve the technical problem, the utility model discloses the technical scheme who adopts is: the utility model provides a reaction unit for silica sol production, the churn that sets up including the level, the churn bottom is equipped with the supporting leg, is equipped with the (mixing) shaft in the churn, is equipped with a plurality of stirring vane on the (mixing) shaft, and the (mixing) shaft passes through agitator motor drive, and the churn upside is equipped with the loading hopper, is equipped with blanking plate in the loading hopper, is equipped with blanking hole on the blanking plate, and the churn top is equipped with liquid feeding pipe and blast pipe, and churn one end bottom is equipped with the bin outlet, is equipped with the valve on the.
In the preferred scheme, the inner wall of the charging hopper is provided with a supporting seat for supporting the blanking plate, a spring is arranged between the supporting seat and the blanking plate, the bottom of the blanking plate is provided with an eccentric wheel which is sleeved on a rotating shaft, and the rotating shaft is driven by a motor arranged at the top of the mixing drum.
In the preferred scheme, the charging hopper is communicated with a refining cavity arranged in the mixing drum, the middle of the bottom of the refining cavity is high, the two ends of the refining cavity are low, and the bottom of the refining cavity is provided with a material dispersing hole.
In the preferred scheme, the supporting leg lower extreme that is close to bin outlet one end is equipped with the mount pad, and the supporting leg passes through the pin to be installed on the mount pad, and the one end bottom that the bin outlet was kept away from to the churn is equipped with the telescoping device.
In a further scheme, the telescopic device is an electric push rod or a hydraulic cylinder.
In a further aspect, the mounting base is anchored to the ground by an anchor bolt.
According to the reaction device for producing the silica sol, the stirring blades rotate to stir reaction materials, so that solid-liquid mixing is facilitated, and the reaction efficiency is improved; meanwhile, for the powder floating on the liquid surface due to the attachment of hydrogen, the liquid surface is flapped in the rotation process of the stirring blade, which is beneficial to pressing the floating powder below the liquid surface, thereby preventing the powder from floating to influence the reaction efficiency; the feeding hopper is internally provided with the blanking plate, so that silicon powder can uniformly fall into the mixing drum, the probability of producing a pan due to one-time large-amount addition of the silicon powder is reduced, manual batch feeding is not needed, and the labor intensity is reduced.
Drawings
The invention will be further explained with reference to the following figures and examples:
fig. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a cross-sectional view taken along plane A-A of FIG. 1;
FIG. 3 is an enlarged view at B of FIG. 1;
in the figure: the stirring device comprises a stirring drum 1, supporting legs 2, a stirring shaft 3, stirring blades 4, a stirring motor 5, a charging hopper 6, a blanking plate 7, a liquid adding pipe 8, an exhaust pipe 9, a discharge outlet 10, a supporting seat 11, a spring 12, an eccentric wheel 13, a rotating shaft 14, a motor 15, a material homogenizing cavity 16, a mounting seat 17, a telescopic device 18, a heating coil 19, a blanking hole 701 and a bulk material hole 1601.
Detailed Description
As shown in figures 1-3, a reaction device for silica sol production comprises a mixing drum 1 horizontally arranged, the mixing drum 1 can be arranged to be a cylinder at the bottom, the upper side is a rectangle, the bottom of the mixing drum 1 is provided with supporting legs 2, a mixing shaft 3 is arranged in the mixing drum 1, the mixing shaft 3 is horizontally arranged, two ends of the mixing shaft 3 are rotatably arranged on the mixing drum 1 through bearings, the mixing shaft 3 is provided with a plurality of mixing blades 4, the mixing shaft 3 is driven by a mixing motor 5, the mixing motor 5 is arranged on a supporting plate at the end part of the mixing drum 1, the output end of the mixing motor 5 is connected with the input end of a speed reducer, the output end of the speed reducer is connected with the mixing shaft 3, the upper side of the mixing drum 1 is provided with a feeding hopper 6, a blanking plate 7 is arranged in the feeding hopper 6, a blanking hole 701 is arranged on the blanking plate 7, be equipped with the valve on the bin outlet 10, 1 outer wall of churn is equipped with heating coil 19, and heating coil 19 encircles at 1 outer wall of churn, carries heating medium to heating coil 19 inner loop through the water pump, and heating medium can be hot water.
When this reaction unit specifically uses, at first add alkali lye in to churn 1 through liquid feeding pipe 8, through to carrying hot water in the heating coil 19, preheat alkali lye, open agitator motor 5 and stir alkali lye, then add silica flour in to churn 1 through loading hopper 6, the hydrogen that the reaction produced is discharged from blast pipe 9.
The stirring motor 5 drives the stirring shaft 3 to rotate, and the stirring blades 4 rotate to stir the reaction materials, so that solid-liquid mixing is facilitated, and the reaction efficiency is improved; meanwhile, for the powder floating on the liquid surface due to the attachment of hydrogen, the liquid surface is flapped in the rotation process of the stirring blade 4, which is beneficial to pressing the floating powder below the liquid surface, thereby preventing the powder from floating to influence the reaction efficiency; the feeding hopper 6 is internally provided with the blanking plate 7, so that silicon powder can uniformly fall into the stirring cylinder 1, the probability of producing a pan due to one-time large-amount addition of the silicon powder is reduced, manual batch feeding is not needed, and the labor intensity is reduced.
Preferably, a supporting seat 11 for supporting the blanking plate 7 is arranged on the inner wall of the charging hopper 6, a spring 12 is arranged between the supporting seat 11 and the blanking plate 7, an eccentric wheel 13 is arranged at the bottom of the blanking plate 7, the eccentric wheel 13 is sleeved on a rotating shaft 14, two ends of the rotating shaft 14 are rotatably installed in the charging hopper 6 through bearings, and the rotating shaft 14 is driven by a motor 15 arranged at the top of the mixing drum 1.
The blanking plate 7 is extruded in the rotating process of the eccentric wheel 13, and the blanking plate 7 vibrates up and down under the action of the spring 12, so that silicon powder falls off, and the blanking hole 701 is prevented from being blocked.
Preferably, the charging hopper 6 is communicated with a homogenizing chamber 16 arranged in the mixing drum 1, the middle of the bottom of the homogenizing chamber 16 is high, and the two ends of the bottom of the homogenizing chamber 16 are low, and a material dispersing hole 1601 is arranged at the bottom of the homogenizing chamber 16.
Silicon powder falling from the charging hopper 6 falls into the refining cavity 16, the silicon powder slides along the bottom of the refining cavity 16, and the silicon powder falls into the mixing drum 1 from the bulk material hole 1601 in the sliding process, so that the uniformity of silicon powder falling is improved, and the reaction rate is improved.
The lower extreme of supporting leg 2 that is close to bin outlet 10 one end is equipped with mount pad 17, and supporting leg 2 installs on mount pad 17 through the pin, and the one end bottom that the bin outlet 10 was kept away from to churn 1 is equipped with telescoping device 18, and for the support stability who improves mount pad 17, mount pad 17 passes through the anchor bolt anchor subaerial.
The telescoping device 18 is an electric push rod or a hydraulic cylinder.
After the reaction is completed, the valve on the discharge hole 10 is opened to discharge materials, and in order to prevent incomplete discharge, the telescopic device 18 is started to lift one end of the mixing drum 1, which is far away from the discharge hole 10, so that the emptying degree of the materials is improved.
The above-mentioned embodiments are merely preferred embodiments of the present invention, and should not be considered as limitations of the present invention, and the protection scope of the present invention should be defined by the technical solutions described in the claims, and includes equivalent alternatives of technical features in the technical solutions described in the claims. Namely, equivalent alterations and modifications within the scope of the invention are also within the scope of the invention.
Claims (6)
1. A reaction unit for silica sol production, characterized in that: mixing drum (1) that sets up including the level, mixing drum (1) bottom is equipped with supporting leg (2), be equipped with (mixing) shaft (3) in mixing drum (1), be equipped with a plurality of stirring vane (4) on (mixing) shaft (3), stirring shaft (3) are through agitator motor (5) drive, mixing drum (1) upside is equipped with loading hopper (6), be equipped with blanking plate (7) in loading hopper (6), be equipped with blanking hole (701) on blanking plate (7), mixing drum (1) top is equipped with filling tube (8) and blast pipe (9), mixing drum (1) one end bottom is equipped with bin outlet (10), be equipped with the valve on bin outlet (10), mixing drum (1) outer wall is equipped with heating coil (19).
2. A reaction device for silica sol production according to claim 1, characterized in that: the inner wall of the charging hopper (6) is provided with a supporting seat (11) for supporting the blanking plate (7), a spring (12) is arranged between the supporting seat (11) and the blanking plate (7), the bottom of the blanking plate (7) is provided with an eccentric wheel (13), the eccentric wheel (13) is sleeved on a rotating shaft (14), and the rotating shaft (14) is driven by a motor (15) arranged at the top of the mixing drum (1).
3. A reaction device for silica sol production according to claim 1, characterized in that: the feed hopper (6) is communicated with a material homogenizing cavity (16) arranged in the mixing drum (1), the middle of the bottom of the material homogenizing cavity (16) is high, the two ends of the bottom of the material homogenizing cavity are low, and a material dispersing hole (1601) is formed in the bottom of the material homogenizing cavity (16).
4. A reaction device for silica sol production according to claim 1, characterized in that: the lower end of the supporting leg (2) close to one end of the discharge hole (10) is provided with a mounting seat (17), the supporting leg (2) is installed on the mounting seat (17) through a pin, and the bottom of the end, far away from the discharge hole (10), of the stirring cylinder (1) is provided with a telescopic device (18).
5. A reaction device for silica sol production according to claim 4, characterized in that: the telescopic device (18) is an electric push rod or a hydraulic cylinder.
6. A reaction device for silica sol production according to claim 4, characterized in that: the mounting seat (17) is anchored on the ground through an anchor bolt.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920652176.3U CN210385826U (en) | 2019-05-08 | 2019-05-08 | Reaction device for producing silica sol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920652176.3U CN210385826U (en) | 2019-05-08 | 2019-05-08 | Reaction device for producing silica sol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210385826U true CN210385826U (en) | 2020-04-24 |
Family
ID=70346002
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920652176.3U Expired - Fee Related CN210385826U (en) | 2019-05-08 | 2019-05-08 | Reaction device for producing silica sol |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210385826U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112844256A (en) * | 2020-12-29 | 2021-05-28 | 山东东珩胶体材料有限公司 | Aluminum powder batch feeding method and automatic feeding equipment in aluminum sol production process |
| CN114288963A (en) * | 2020-10-08 | 2022-04-08 | 张家港清澄纳米科技有限公司 | High-efficient low pressure reation kettle |
-
2019
- 2019-05-08 CN CN201920652176.3U patent/CN210385826U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114288963A (en) * | 2020-10-08 | 2022-04-08 | 张家港清澄纳米科技有限公司 | High-efficient low pressure reation kettle |
| CN112844256A (en) * | 2020-12-29 | 2021-05-28 | 山东东珩胶体材料有限公司 | Aluminum powder batch feeding method and automatic feeding equipment in aluminum sol production process |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN202087264U (en) | Slurry stirring tank | |
| CN210385826U (en) | Reaction device for producing silica sol | |
| CN109603628B (en) | Multi-stage stirring device for chemical material mixing processing | |
| CN208512345U (en) | A kind of powder particle speed-adjustable stir mixing arrangement | |
| CN215749979U (en) | Fixed pouring agitating unit is used in aerated concrete block production | |
| CN214210217U (en) | Polishing solution preparation device | |
| CN212578876U (en) | Aerated concrete pouring agitating unit | |
| CN211025857U (en) | High-efficient mixing dissolving device of hydrophilicity macromolecular material | |
| CN216442805U (en) | Lightweight wallboard concrete mixing device | |
| CN212651693U (en) | A raw materials proportioning machine for preparing carborundum | |
| CN113829504A (en) | Dosing unit is used in concrete processing that permeates water | |
| CN209302572U (en) | A kind of cosmetics batch mixer | |
| CN219003049U (en) | Grinding aid apparatus for producing | |
| CN220824720U (en) | Micro powder mixing and stirring device | |
| CN2486202Y (en) | Vacuum emulsifying machine | |
| CN219580532U (en) | Water-based polyurethane reaction kettle capable of feeding materials uniformly | |
| CN219922886U (en) | Reation kettle is used in detergent production | |
| CN217527181U (en) | Agitating unit is used in antiseptic solution production of misce bene | |
| CN221161095U (en) | High-speed dispersion mixer for color master batch | |
| CN212915480U (en) | Production equipment of SMA esterified substance for high-pigment-ratio ink | |
| CN216171611U (en) | Compound production equipment for liquid chemical products | |
| CN220194674U (en) | Strong dispersing machine for platinum catalyst production | |
| CN215540348U (en) | Integrated equipment for preparing wear-resistant ramming material | |
| CN218795393U (en) | Safe and environment-friendly pigment stirring dispersion kettle | |
| CN215996299U (en) | High performance water-reducing agent agitating unit |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200424 |