CN209612984U - For extending the water washing device of MTBE catalyst life - Google Patents
For extending the water washing device of MTBE catalyst life Download PDFInfo
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- CN209612984U CN209612984U CN201920138910.4U CN201920138910U CN209612984U CN 209612984 U CN209612984 U CN 209612984U CN 201920138910 U CN201920138910 U CN 201920138910U CN 209612984 U CN209612984 U CN 209612984U
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- water washing
- washing tank
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- horizontal water
- water
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Abstract
The utility model provides a kind of for extending the water washing device of MTBE catalyst life, including mixer is adjusted, the front end of the adjustable mixer is provided with water inlet pipe and oil liquefied gas feed pipe, it further include quartz filter, horizontal water washing tank, the adjustable mixer is connect in its outlet with the quartz filter pipeline, and the quartz filter is connect through feed pipe with the horizontal water washing tank pipeline；The horizontal water washing tank is additionally provided with water supply pipe, is used for horizontal water washing tank make-up water source；It is additionally provided with discharge nozzle on the horizontal water washing tank, for conveying material to MTBE process units.The utility model can carry out water washing cleaning to liquefied petroleum gas, extend catalyst service life in subsequent technique, reduce production cost, reduce safe and environment-friendly risk.
Description
Technical field
The utility model relates to oil liquefied gas water process units, and in particular to a kind of oil liquefied gas water washing cleaning dress
It sets.
Background technique
MTBE is the trade name of methyl tertiary butyl ether(MTBE), is the production that isobutene and methanol react under strongly acidic catalyst effect
Object, it is mainly used for substitution lead tetraethide as dopes for gasoline, and strong acidic ion resin catalysis
Agent is to generate methyl tertiary butyl ether(MTBE) (MTBE) catalyst carrier.Requirement of the catalyst for raw material is very harsh, due to upstream
Partial vulcanization object could be removed by having to pass through alkali cleaning when the oil liquefied gas factory of device production, also have micro alkali in alkaline cleaning procedure
Property substance exist wherein, and the basic species in raw material directly affect activity and the service life of strongly acidic catalyst.The catalyst is just
Often activity without filtering with washing in the case where, most two months activity completely without, it is necessary to replace.Practical life has been significantly greatly increased
Safe and environment-friendly risk in production, while also increasing the production cost of enterprise.
Summary of the invention
The technical problem to be solved by the utility model is to provide a kind of for extending the washing of MTBE catalyst life
Device overcomes the above technological deficiency, extends catalyst service life, reduces production cost, reduces safe and environment-friendly risk.
In order to solve the above technical problems, the water washing device for extending MTBE catalyst life of the utility model includes can
The front end of adjusting mixer, the adjustable mixer is provided with water inlet pipe and oil liquefied gas feed pipe, further includes quartz
Sand filter, horizontal water washing tank, the adjustable mixer are connect in its outlet with the quartz filter pipeline, the stone
Sand filter is connect through feed pipe with the horizontal water washing tank pipeline；The horizontal water washing tank is additionally provided with water supply pipe, is used for
To horizontal water washing tank make-up water source；It is additionally provided with discharge nozzle on the horizontal water washing tank, for conveying object to MTBE process units
Material.
The lower end of the horizontal water washing tank is provided with circulation water pot, and the circulation water pot is through centrifugal pump and the water inlet pipe
It is connected by pipeline.
The circulation water pot is also parallel with auxiliary centrifugal pump between the water inlet pipe.
The horizontal water washing tank is horizontally disposed, and the feed pipe, discharge nozzle are respectively arranged at horizontal water washing tank both ends, described
Discharge nozzle accesses horizontal water washing tank from upper surface.
Cross-line is also parallel between the adjustable mixer and the feed pipe.
Sample tap and row's leaching mouth are additionally provided on the horizontal water washing tank；Liquid level is additionally provided on the horizontal water washing tank certainly
Dynamic detection instrument and pressure instrumentation etc..The ratio between swept volume of the quartz filter and horizontal water washing tank for 1:5~
7。
After adopting the above technical scheme, raw material liquefied gas obtains before contacting highly acidic resin catalyst by the present apparatus
Purification, to extend the service life of catalyst, reduces production cost；The replacement cycle of catalyst has also obtained obviously prolonging
It is long, reduce safety and environmentally friendly risk.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the water washing device for extending MTBE catalyst life of the utility model.
Specific embodiment
It is described further below in conjunction with specific operation mode of the attached drawing to the utility model.
As shown in Figure 1, the water washing device for extending MTBE catalyst life of the utility model includes adjustable mixing
The front end of device 1, the adjustable mixer 1 is provided with water inlet pipe 10 and oil liquefied gas feed pipe 11, further includes quartz sand
Filter 2, horizontal water washing tank 3, the adjustable mixer 1 is connect in its outlet with 2 pipeline of quartz filter, described
Quartz filter 2 is connect through feed pipe 30 with horizontal 3 pipeline of water washing tank；The horizontal water washing tank 3 is additionally provided with moisturizing
Pipe 31 is used for horizontal 3 make-up water source of water washing tank；It is additionally provided with discharge nozzle 32 on the horizontal water washing tank 3, for raw to MTBE
It produces device and conveys material.
The lower end of the horizontal water washing tank 3 be provided with circulation water pot 33, the circulation water pot 33 through centrifugal pump 40 with it is described
Water inlet pipe 10 be connected by pipeline.
The circulation water pot 33 passes through and is also parallel with auxiliary centrifugal pump 41 between the water inlet pipe 10.
The horizontal water washing tank 3 is horizontally disposed, and the feed pipe 30, discharge nozzle 32 are respectively arranged at 3 liang of horizontal water washing tank
End, the discharge nozzle 32 access horizontal water washing tank 3 from upper surface.
Cross-line 5 is also parallel between the adjustable mixer 1 and the feed pipe 30.
Sample tap and row's leaching mouth are additionally provided on the horizontal water washing tank 3；Liquid level is additionally provided on the horizontal water washing tank 3
Automatic Measuring Instruments and pressure instrumentation etc..The ratio between the quartz filter 2 and the swept volume of horizontal water washing tank 3 are 1:
5~7, in the present embodiment, the swept volume of quartz filter 2 and horizontal water washing tank 3 is respectively 50 cubes of 10 sum of cubes.
The workflow of the water washing device for extending MTBE catalyst life includes:
Liquefied petroleum gas is pressurized to 1Mpa from storage tank delivery pump, is delivered to through oil liquefied gas feed pipe 11 adjustable
Mixer 1, water inlet pipe 10 are intake simultaneously, carry out being sufficiently mixed for water and liquefied gas by mixer 1 is adjusted；Then using
Quartz filter 2 is filtered, and some mechanical impurity in raw material, alkaline residues are removed, guarantee the clean of raw material.Through
It crosses filtered raw material to enter from horizontal 3 one upper side of water washing tank, axially flow to the other side along water washing tank, flowed over axially
The separation of liquefied gas and water is carried out in journey, liquefied gas is gone out to enter next process by the discharge nozzle 32 above the other side.Operation
In the process, washing amount is controlled, the water level of horizontal water washing tank is controlled, to guarantee that raw material liquefied gas being capable of abundant water in tank
It washes.Assay is irregularly carried out to the water quality in tank by sample tap simultaneously, the measurement of pH value is periodically carried out to the tank water quality,
The case where according to result of laboratory test and pH value, regularly replaces water in tank, the water source softened water of this tank.
According to inspection result, the water in horizontal water washing tank 3 is recycled through circulation water pot 33 and pipeline, or through row leaching mouth row
Out other than the present apparatus.
Before entering highly acidic resin catalyst, quality is greatly improved raw material liquefied gas after the system, into
One step meets requirement of the catalyst to raw material, and the service life of the catalyst will be greatly prolonged, by original every
The catalyst of replacement in two months extends to 6 months or more.The catalyst is per ton to press 2.3 ten thousand calculating, can save every year large quantities of
Cost, economic benefit is clearly.It has been greatly reduced the workload of employee simultaneously, has reduced the frequency of more catalyst changeout, also
It is reduction of risk during disassemblerassembler, realizes that benefit and safety get bumper harvests.
Specific embodiment of the present utility model includes but is not limited to above-described embodiment, without departing substantially from the utility model essence
In the case where mind and its essence, those skilled in the art can make various corresponding changes and change according to the utility model
Shape, but still fall into the protection scope of the utility model.
Claims (4)
1. it is a kind of for extending the water washing device of MTBE catalyst life, including adjustable mixer (1), the adjustable mixing
The front end of device (1) is provided with water inlet pipe (10) and oil liquefied gas feed pipe (11), it is characterised in that: further includes quartz sand mistake
Filter (2), horizontal water washing tank (3), the adjustable mixer (1) connect in its outlet with the quartz filter (2) pipeline
It connects, the quartz filter (2) connect through feed pipe (30) with horizontal water washing tank (3) pipeline；The horizontal water washing tank
(3) water supply pipe (31) are additionally provided with, are used for horizontal water washing tank (3) make-up water source；It is additionally provided on the horizontal water washing tank (3)
Discharge nozzle (32), for conveying material to MTBE process units.
2. as described in claim 1 for extending the water washing device of MTBE catalyst life, it is characterised in that: the horizontal water
The lower end of cleaning of evaporator (3) is provided with circulation water pot (33), and the circulation water pot (33) is through centrifugal pump (40) and the water inlet pipe
(10) it is connected by pipeline.
3. as claimed in claim 2 for extending the water washing device of MTBE catalyst life, it is characterised in that: the recirculated water
Tank (33) passes through and is also parallel with auxiliary centrifugal pump (41) between the water inlet pipe (10).
4. as described in claim 1 for extending the water washing device of MTBE catalyst life, it is characterised in that: the horizontal water
Cleaning of evaporator (3) is horizontally disposed, and the feed pipe (30), discharge nozzle (32) are respectively arranged at horizontal water washing tank (3) both ends, the discharging
It manages (32) and accesses horizontal water washing tank (3) from upper surface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920138910.4U CN209612984U (en) | 2019-01-28 | 2019-01-28 | For extending the water washing device of MTBE catalyst life |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920138910.4U CN209612984U (en) | 2019-01-28 | 2019-01-28 | For extending the water washing device of MTBE catalyst life |
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| Publication Number | Publication Date |
|---|---|
| CN209612984U true CN209612984U (en) | 2019-11-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201920138910.4U Active CN209612984U (en) | 2019-01-28 | 2019-01-28 | For extending the water washing device of MTBE catalyst life |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109663616A (en) * | 2019-01-28 | 2019-04-23 | 安庆市泰发能源科技有限公司 | For extending the water washing device of MTBE catalyst life |
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2019
- 2019-01-28 CN CN201920138910.4U patent/CN209612984U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109663616A (en) * | 2019-01-28 | 2019-04-23 | 安庆市泰发能源科技有限公司 | For extending the water washing device of MTBE catalyst life |
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