CN209584428U - Portable melt device built in a kind of high-field electrode - Google Patents

Portable melt device built in a kind of high-field electrode Download PDF

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Publication number
CN209584428U
CN209584428U CN201920294512.1U CN201920294512U CN209584428U CN 209584428 U CN209584428 U CN 209584428U CN 201920294512 U CN201920294512 U CN 201920294512U CN 209584428 U CN209584428 U CN 209584428U
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China
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shell
spinning nozzle
spinning
electrode
blocking sleeve
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陈宏波
汪传生
韩雯雯
杨卫民
刘海超
焦冬梅
田晓龙
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Qingdao University of Science and Technology
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Qingdao University of Science and Technology
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Abstract

The utility model belongs to melt electrostatic spinning equipment technical field, it is related to Portable melt device built in a kind of high-field electrode, it is made of spinneret part and fan section, the main structure of spinneret part includes spinning nozzle, electrode holder, electrode, insulation blocking sleeve, heat transfer cylinder, Electrothermal ring, jackscrew, high-voltage conducting wires, roller groove, idler wheel, high-pressure electrostatic module, power module, shell, power supply line, regulating switch and No.1 contact point, the main structure of fan section includes shell, motor, bracket, flabellum, heater strip, venthole and No. two contact points, using tubulose charge bar as spinning material, accurate temperature control heating is carried out to tubulose charge bar using Electrothermal ring and becomes melt, tubulose charge bar slowly moves under idler wheel drive to spinning end, squeeze melt after spinning nozzle tip annular is uniformly distributed Tens of jet streams are formed under electric field action, are formed fiber after stretched, solidification and cooling, are realized that real-time mass prepares superfine fibre.

Description

Portable melt device built in a kind of high-field electrode
Technical field:
The utility model belongs to melt electrostatic spinning equipment technical field, and in particular to portable built in a kind of high-field electrode Melt electrostatic spinning device can be realized the portable real-time continuous mass preparation of superfine fibre.
Background technique:
Electrostatic spinning is the technique that polymer melt or solution are prepared into superfine fibre using high-pressure electrostatic, has and sets Feature standby simple and that operation is easy, has received widespread attention, and is that prepare polymer continuous nano-fibre at present most important One of method.With the continuous development of nano material technology, electrostatic spinning simple and effective produces nanofiber as a kind of New Processing, played in terms of bio-medical material, filtering and protection, catalysis, the energy, photoelectricity and food engineering huge Big effect.Electrostatic spinning technique is quickly grown, and researcher opens around the directions such as fibre diameter, increase fiber output efficiency are reduced A variety of electrostatic spinning apparatus to have been sent out, but have mostly rested on laboratory stage, volume is larger, and it is not readily portable, and can not accomplish Being used while making limits the application of electrostatic spinning technique.In recent years, portable electrostatic device for spinning is surrounded, researcher carries out Some technological improvements.A kind of hand-held portable electrostatic spinning equipment of air-flow auxiliary disclosed in Chinese patent 201810373378.4 It is opened including insulation crust, large capacity secondary cell, charging jacks, high-voltage conducting wires, high voltage electrostatic generation unit, high-pressure electrostatic Pass, the fixed bracket of airflow duct connector, airflow duct, syringe, disposable syringe, syringe needle fixed bracket, stainless pin Head, air-flow orientation cover;The handle portion of the insulation crust is equipped with dismountable insulating cover;Large capacity secondary cell passes through high pressure Conducting wire is connect with high voltage electrostatic generation unit and charging jacks;High voltage electrostatic generation unit and high-pressure electrostatic occur switch and pass through height Conducting wire is pressed to be connected;High-pressure electrostatic occurs switch and is located on the inside of the handle of insulation crust;Airflow duct is located inside insulation crust Middle position is equipped with airflow duct connector among insulation crust handle bottom end;Insulation crust top is set there are two syringe Fixed bracket, is fixed on insulation crust top for disposable syringe;The stainless steel syringe needle of syringe passes through the fixed bracket of syringe needle It is fixed on the axis line position of insulation crust front end, the fixed bracket of syringe needle passes through high-voltage conducting wires and high voltage electrostatic generation unit phase Even;Insulation crust leading portion opening is equipped with cylindrical air-flow orientation cover;And disclosed in Chinese patent 201720057770.9 A kind of novel portable electrostatic spinning apparatus includes host and pistol, and the host includes host housing, in host housing It is provided with power supply, gas generator and high voltage power supply mechanism, the pistol includes gun body shell, spinning head and is spinneret Head provides the liquid supplying device of spinning precursor liquid, and air inlet and air outlet, the air inlet connection are provided on the gun body shell The gas-guide tube of gas generator, the spinning head stretch out gun body shell, the injection tip of spinning head and gas outlet from gas outlet Central axis coincide;Power electric connection high voltage power supply mechanism, gas generator and liquid supplying device, high voltage power supply machine The anode of the voltage output end of structure connects spinning head by conducting wire;One kind disclosed in Chinese patent 201510214221.3 is portable Electrospinning device includes dry battery power, high-voltage electrostatic generator, charging gear, gas generating unit, spinning injection dress It sets and insulation crust;The dry battery power electrical connection high-voltage electrostatic generator, charging gear and gas generating unit;It is described High-voltage electrostatic generator includes DC- high pressure DC inverter and voltage regulating and controlling circuit, the voltage input end of DC- high pressure DC inverter It is electrically connected dry battery power, the voltage output end connection control high-voltage electrostatic generator output voltage of DC- high pressure DC inverter The voltage regulating and controlling circuit of size;The voltage output end of voltage regulating and controlling circuit is the voltage output end of high-voltage electrostatic generator, The cathode of the voltage output end of high-voltage electrostatic generator is grounded, the metal capillary spray head of anode connection spinning injection apparatus, The metal capillary spray head is connected to charging gear;The spinning injection apparatus further includes the gas coaxial with metal capillary spray head Conductance pipe, the airflow duct are placed on outside metal capillary spray head, and the airflow duct connects gas generating unit;It is described dry Battery supply, high-voltage electrostatic generator, gas generating unit are placed in insulation crust, are provided on insulation crust and are led with air-flow The opening that pipe port bore matches, airflow duct be aligned with the injection tip of metal capillary spray head insulation crust opening or It is stretched out from opening;A kind of Portable low-voltage near field electrostatic spinning presentation device disclosed in Chinese patent 201020156420.6, Main structure includes experiment instrument shell, voltage drainage area, control panel, univalve door, portable handle, attaching plug, spinning dials, connects Ground wire, high-voltage DC power supply, metal spinning needle, scale support rod, connecting rod, dielectric base face, aluminium foil, coverslip, taylor cone And spinning jet, it is characterised in that be formed with portable handle, experiment instrument at the experiment instrument shell upper side center of cuboid box structure Shell leading flank right-half plane is formed with control panel, and left demifacet is made the univalve door of single open-type, connects on the trailing flank of experiment instrument shell Power supply line is electrically connected with attaching plug out;Experiment instrument body interior structure, intracavity bottom system are provided in experiment instrument housing cavity There is the dielectric base face with experiment instrument housing bottom surface correspondingly-sized, dielectric base left side of face middle vertical type is provided with scale branch Strut, the scale support rod upper half are laterally formed with connecting rod, are formed with spinning dials at connecting rod end point, upright in spinning dials Formula is provided with 1-10 root metal spinning needle, and metal spinning needle top connects high-voltage DC power supply anode, and metal spinning needle is made on bottom end There is taylor cone, Taylor's cone tip part ejects spinning jet;Side to the right lays aluminium foil at the center of dielectric base face, places lid on aluminium foil Slide;Aluminium foil connect and is grounded with high-voltage DC power supply cathode;A kind of reality disclosed in Chinese patent 201120097470.6 Testing room dedicated portable miniature integration electrostatic spinning machine includes insulation box, transparent plastic door, compression screw, liquid feeding bottle cap, row Gas hose, burp valve, filament lamp switch, locking knob, pressurised cylinder, breather valve, connector sleeve, hose, fixed ring, direct current High voltage power supply, adjusting pressuring knob, liquid feeding bottle, liquid outlet valve, conducting wire, liquid storage pipe, taylor cone, controllable turning point, incandescent lamp, dirt support Disk collects device, support rod, fastening screw, support frame, and whole equipment is equipped with ground line, and each section device is centered on liquid storage pipe It is integrated in small-sized insulation box, and is connected using handle screw with clip, is readily disassembled;Above-mentioned patented product spinning medium is equal It is solution, does not can be carried out melt electrostatic spinning, can not realizes that the mass portability of superfine fibre is continuously prepared in real time.Cause This, a kind of Portable melt device of R & D design, by the miniaturization of internal high-voltage electrode realization device, portable Change, and the mass that can be realized fiber is continuously prepared.
Summary of the invention:
The purpose of the utility model is to overcome defect of the existing technology, research and develop portable built in a kind of high-field electrode Melt electrostatic spinning device realizes the fiber coating in arbitrary surfaces any direction, deposition and continuous preparation in real time.
To achieve the goals above, the utility model relates to high-field electrode built in Portable melt device by Spinneret part and fan section composition;The main structure of spinneret part includes spinning nozzle, electrode holder, electrode, isolation guarantor Sheath, heat transfer cylinder, Electrothermal ring, jackscrew, high-voltage conducting wires, roller groove, idler wheel, high-pressure electrostatic module, power module, shell, Power supply line, regulating switch and No.1 contact point;The spinning nozzle of hollow type cylindrical structure is internally provided with electrode holder, The top of spinning nozzle is outer circle taper, and the tail end of electrode holder is cone, and one end of electrode holder is provided with ball The electrode of shape structure, the periphery of spinning nozzle are provided with the insulation blocking sleeve of tubular structure, spinning nozzle and insulation blocking sleeve it Between front end be provided with the heat transfer cylinder and Electrothermal ring of tubular structure, the fixed front end for being set in heat transfer cylinder of Electrothermal ring lacks On the inside of mouthful, the top of heat transfer cylinder is the cone being adapted with spinning nozzle top, and the jackscrew of three equidistant formulas settings will Spinning nozzle, electrode holder and heat transfer cylinder are fastenedly connected, and one of jackscrew is hollow structure, and high-voltage conducting wires are by electric heating Circle draw, connect after hollow jackscrew and electrode holder with electrode, the inside of insulation blocking sleeve open up there are two mirror image The roller groove of symmetrical structure is provided with idler wheel in roller groove, is provided with high-pressure electrostatic module below the rear end of insulation blocking sleeve, Power module is provided with below high-pressure electrostatic module, the outside of insulation blocking sleeve, high-pressure electrostatic module and power module, which is enclosed, to be set There is shell, power supply line extendes back out shell from power module extraction, and the shell at high-pressure electrostatic module is provided with regulating switch, shell Outside be provided with No.1 contact point;The main structure of fan section includes shell, motor, bracket, flabellum, heater strip, ventilation Hole and No. two contact points;The shell of hollow type structure is internally provided with motor, and motor is fixed on shell by two brackets Inside, motor are connect with flabellum, and flabellum is located between two brackets, and heater strip, the rear end of shell are provided between two brackets Venthole is offered, the side of shell is provided with No. two contact points, and motor and heater strip are connect with No. two contact points respectively;Spinning Gap between spray head and electrode holder is No.1 annular chamber, and the gap between spinning nozzle and insulation blocking sleeve is No. two rings Shape chamber, shell are inserted into spinneret part and fan section realization connection after No. two annular chambers, and No.1 contact point is led with No. two contact points Logical, power module is fan section power supply.
The utility model is convenient for storage, carrying and the tubulose charge bar installed compared with prior art, using what is prepared in advance As spinning material, using Electrothermal ring to material a part of near tubulose charge bar end carry out accurate temperature control heating make its at For melt, tubulose charge bar is slowly moved under idler wheel drive to spinning end, squeezes melt in the spinning nozzle point of conical structure End ring shape is uniformly distributed, and under electric field action, tens of jet streams of the melt composition of annular spread, motor drives flabellum rotation to generate High-speed flow drive jet stream to blow to reception device after heater strip heats up, jet stream is stretched, solidification and it is cooling after formed Superfine fibre, to realize the real-time mass preparation of superfine fibre, electrode is built in spinning nozzle center, applies voltage from normal The 50-80kV of rule is reduced within 10kV, and the volume of high-pressure electrostatic module is reduced while improving safety coefficient, is conducive to Realize portability purpose of design, meanwhile, the limitation that conventional electrostatic spinning reception device connects electricity is relieved, can be realized expectation in office The real-time continuous spraying of the superfine fibre mass of face any direction, deposition and preparation, extend electrostatic spinning and prepare micro-nano fiber Application direction;Its structure is simple, easy to operate, compact, easy to carry and hand-held, and spinning efficiency is high, heating speed and Wire vent speed is fast, and temperature control is accurate, is conducive to the refinement of fiber, can be widely applied for experimental demonstration, medical and military etc. fields.
Detailed description of the invention:
Fig. 1 is the main structure schematic illustration of the utility model.
Fig. 2 be the utility model relates to tubulose charge bar main structure schematic illustration.
Fig. 3 be the utility model relates to tubulose charge bar and idler wheel connection relationship diagram.
Specific embodiment:
It is described in further detail with reference to the accompanying drawing and by embodiment to the utility model.
Embodiment 1:
Portable melt device is by spinneret part 1 and fan section built in the high-field electrode that the present embodiment is related to 3 compositions;The main structure of spinneret part 1 includes spinning nozzle 10, electrode holder 11, electrode 12, insulation blocking sleeve 13, heat biography Guide tube 14, Electrothermal ring 15, jackscrew 16, high-voltage conducting wires 17, roller groove 18, idler wheel 19, high-pressure electrostatic module 20, power module 21, shell 22, power supply line 23, regulating switch 24 and No.1 contact point 25;The spinning nozzle 10 of hollow type cylindrical structure it is interior Portion is provided with electrode holder 11, and the top of spinning nozzle 10 is outer circle taper, and the tail end of electrode holder 11 is cone, electricity One end of pole retainer 11 is provided with the electrode 12 of spheroidal structure, and the periphery of spinning nozzle 10 is provided with the isolation of tubular structure Protective case 13, the front end between spinning nozzle 10 and insulation blocking sleeve 13 are provided with heat transfer cylinder 14 and the electric heating of tubular structure Circle 15, the fixed front end inner side for being set in heat transfer cylinder 14 of Electrothermal ring 15, the top of heat transfer cylinder 14 is to spray with spinning The adaptable cone in first 10 top, the jackscrew 16 that three equidistant formulas are arranged is by spinning nozzle 10, electrode holder 11 and warm Conduction cylinder 14 is fastenedly connected, and one of jackscrew 16 is hollow structure, and high-voltage conducting wires 17 are drawn by Electrothermal ring 15, is passed through hollow Jackscrew 16 and electrode holder 11 after connect with electrode 12, the inside of insulation blocking sleeve 13 is opened up there are two mirror symmetry formula knot The roller groove 18 of structure is provided with idler wheel 19 in roller groove 18, is provided with high-pressure electrostatic module below the rear end of insulation blocking sleeve 13 20, the lower section of high-pressure electrostatic module 20 is provided with power module 21, insulation blocking sleeve 13, high-pressure electrostatic module 20 and power module 21 outside is enclosed equipped with shell 22, and power supply line 23 draws from power module 21 and extendes back out shell 22, at high-pressure electrostatic module 20 Shell 22 is provided with regulating switch 24, and the outside of shell 22 is provided with No.1 contact point 25;The main structure of fan section 3 includes Shell 30, motor 31, bracket 32, flabellum 33, heater strip 34, venthole 35 and No. two contact points 36;The shell of hollow type structure 30 are internally provided with motor 31, and motor 31 is fixed on the inside of shell 30 by two brackets 32, motor 31 and flabellum 33 connect It connects, flabellum 33 is located between two brackets 32, heater strip 34 is provided between two brackets 32, the rear end of shell 30 offers logical Stomata 35, the side of shell 30 are provided with No. two contact points 36, and motor 31 and heater strip 34 are connect with No. two contact points 36 respectively; Gap between spinning nozzle 10 and electrode holder 11 is No.1 annular chamber 41, between spinning nozzle 10 and insulation blocking sleeve 13 Gap be No. two annular chambers 42, shell 30, which is inserted into spinneret part 1 and fan section 3 after No. two annular chambers 42, to be realized and connects, one Number contact point 25 and No. two contact points 36 are connected, and power module 21 is that fan section 3 is powered.
The electrode holder 11 and insulation blocking sleeve 13 that the present embodiment is related to are partiting thermal insulation material, including ceramic, poly- Tetrafluoroethene and polyether-ether-ketone;Insulation blocking sleeve 13 has heat-insulated and insulating effect, being capable of protection staff and equipment safety;Idler wheel 19 be concave wheel;Power module 21 carries out AC-DC conversion to alternating current and decompression is handled;The high-pressure electrostatic module 20 and electricity of shell 22 21 exterior portion of source module is handgrip part;Power supply line 23 can be connect with alternating current or lithium battery;Regulating switch 24 can be adjusted The flow velocity and temperature of air-flow, electrostatic potential, the revolving speed of idler wheel 19, the temperature of Electrothermal ring 15 and the temperature of heater strip 34;Shell Body 30 has positioning action to spinning nozzle 10;Motor 31 is high-speed motor;Heater strip 34 is thermal resistance heater strip;Venthole 35 It is the channel that air enters shell 30.
Portable melt device built in the high-field electrode that the present embodiment is related in use, remove fan section 3, It will be sent between the concave surface of idler wheel 19 convenient for what is stored and carry by polymer raw material extrusion or injection molding tubulose charge bar, pipe The internal diameter and outer diameter of shape charge bar are identical as the internal diameter of No. two annular chambers 42 and outer diameter, then fan section 3 is inserted into No. two annular chambers In 42;Power supply line 23 is electrically connected with city, motor 31 drives 33 high speed rotation of flabellum, generates air-flow to the right, air-flow is by adding Become thermal current after the heating of heated filament 34 to adjust by regulating switch 24 according to the spinning parameter of setting and control thermal current Temperature and speed, thermal current enter No.1 annular chamber 41 via the cavity of spinning nozzle 10, after annular spread outside electrode 12 Side spray goes out;Meanwhile tubulose charge bar is clamped in No. two annular chambers 42 by the concave surface of idler wheel 19 and conveys to the right, passes through regulating switch 24 The revolving speed of idler wheel 19 is adjusted to adjust the speed that tubulose charge bar conveys in No. two annular chambers 42, tubulose charge bar right end reaches heat and passes At guide tube 14, before this, Electrothermal ring 15 has been powered and has heated to heat transfer cylinder 14, reaches the pipe at heat transfer cylinder 14 Shape charge bar, which is heated, is melt into melt, and the tubulose charge bar that melt is constantly conveyed to the right is squeezed to the conical surface tip of spinning nozzle 10 Place, and be uniformly distributed in a ring;Band high-pressure electrostatic under the action of high-pressure electrostatic module 20 of electrode 12, passes through regulating switch 24 Electrostatic potential is adjusted to 10kV, electrode 12 charges, 10 conical surface tip induction charging of spinning nozzle, the conical surface tip of spinning nozzle 10 The melt self-organizing at place forms dozens of and is uniformly distributed jet stream, under thermal current drive, sprays forward to reception device, jet stream warp Overstretching solidifies and is cooled into superfine fibre.

Claims (1)

1. Portable melt device built in a kind of high-field electrode, it is characterised in that main structure is by spinneret part and wind Fan part forms;The main structure of spinneret part includes spinning nozzle, electrode holder, electrode, insulation blocking sleeve, heat transfer Cylinder, Electrothermal ring, jackscrew, high-voltage conducting wires, roller groove, idler wheel, high-pressure electrostatic module, power module, shell, power supply line, adjusting Switch and No.1 contact point;The spinning nozzle of hollow type cylindrical structure is internally provided with electrode holder, spinning nozzle Top is outer circle taper, and the tail end of electrode holder is cone, and one end of electrode holder is provided with the electricity of spheroidal structure The periphery of pole, spinning nozzle is provided with the insulation blocking sleeve of tubular structure, and the front end between spinning nozzle and insulation blocking sleeve is set It is equipped with the heat transfer cylinder and Electrothermal ring of tubular structure, the fixed front end inner side for being set in heat transfer cylinder of Electrothermal ring, heat The top for conducting cylinder is the cone being adapted with spinning nozzle top, the jackscrew that three equidistant formulas are arranged by spinning nozzle, Electrode holder and heat transfer cylinder are fastenedly connected, and one of jackscrew is hollow structure, and high-voltage conducting wires are drawn by Electrothermal ring, worn It is connect after crossing hollow jackscrew and electrode holder with electrode, the inside of insulation blocking sleeve is opened up there are two mirror symmetry formula structure Roller groove, idler wheel is provided in roller groove, is provided with high-pressure electrostatic module, high-pressure electrostatic mould below the rear end of insulation blocking sleeve Power module is provided with below block, the outside of insulation blocking sleeve, high-pressure electrostatic module and power module is enclosed equipped with shell, power supply Line extendes back out shell from power module extraction, and the shell at high-pressure electrostatic module is provided with regulating switch, the outside setting of shell There is No.1 contact point;The main structure of fan section includes that shell, motor, bracket, flabellum, heater strip, venthole and No. two connect Contact;The shell of hollow type structure is internally provided with motor, and motor is fixed on the inside of shell by two brackets, motor with Flabellum connection, flabellum are located between two brackets, heater strip are provided between two brackets, the rear end of shell offers ventilation Hole, the side of shell are provided with No. two contact points, and motor and heater strip are connect with No. two contact points respectively;Spinning nozzle and electrode Gap between retainer is No.1 annular chamber, and the gap between spinning nozzle and insulation blocking sleeve is No. two annular chambers, shell Spinneret part is connected with fan section realization after being inserted into No. two annular chambers, and No.1 contact point is connected with No. two contact points, power supply mould Block is fan section power supply.
CN201920294512.1U 2019-03-08 2019-03-08 Portable melt device built in a kind of high-field electrode Active CN209584428U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109797444A (en) * 2019-03-08 2019-05-24 青岛科技大学 Portable melt device built in a kind of high-field electrode
WO2020172207A1 (en) * 2019-02-20 2020-08-27 Board Of Regents, University Of Texas System Handheld/portable apparatus for the production of microfibers, submicron fibers and nanofibers
US11408096B2 (en) 2017-09-08 2022-08-09 The Board Of Regents Of The University Of Texas System Method of producing mechanoluminescent fibers

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11408096B2 (en) 2017-09-08 2022-08-09 The Board Of Regents Of The University Of Texas System Method of producing mechanoluminescent fibers
WO2020172207A1 (en) * 2019-02-20 2020-08-27 Board Of Regents, University Of Texas System Handheld/portable apparatus for the production of microfibers, submicron fibers and nanofibers
US11427937B2 (en) 2019-02-20 2022-08-30 The Board Of Regents Of The University Of Texas System Handheld/portable apparatus for the production of microfibers, submicron fibers and nanofibers
CN109797444A (en) * 2019-03-08 2019-05-24 青岛科技大学 Portable melt device built in a kind of high-field electrode
CN109797444B (en) * 2019-03-08 2024-04-09 青岛科技大学 High-voltage electrode built-in portable melt electrostatic spinning device

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