CN209497618U - Band coating graphite heater - Google Patents
Band coating graphite heater Download PDFInfo
- Publication number
- CN209497618U CN209497618U CN201821654938.5U CN201821654938U CN209497618U CN 209497618 U CN209497618 U CN 209497618U CN 201821654938 U CN201821654938 U CN 201821654938U CN 209497618 U CN209497618 U CN 209497618U
- Authority
- CN
- China
- Prior art keywords
- graphite heater
- coating
- graphite
- oxidation layer
- heater
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 229910002804 graphite Inorganic materials 0.000 title claims abstract description 37
- 239000010439 graphite Substances 0.000 title claims abstract description 37
- 239000011248 coating agent Substances 0.000 title claims abstract description 21
- 238000000576 coating method Methods 0.000 title claims abstract description 21
- 230000003064 anti-oxidating effect Effects 0.000 claims abstract description 14
- 229920005989 resin Polymers 0.000 claims abstract description 11
- 239000011347 resin Substances 0.000 claims abstract description 11
- 230000007704 transition Effects 0.000 claims abstract description 11
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000005011 phenolic resin Substances 0.000 claims abstract description 10
- 229920001568 phenolic resin Polymers 0.000 claims abstract description 10
- -1 aldehyde ketone Chemical class 0.000 claims abstract description 7
- 239000003822 epoxy resin Substances 0.000 claims abstract description 7
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 7
- 229910052580 B4C Inorganic materials 0.000 claims abstract description 6
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims abstract description 6
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000004952 Polyamide Substances 0.000 claims abstract description 5
- 229920002647 polyamide Polymers 0.000 claims abstract description 5
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000003963 antioxidant agent Substances 0.000 claims 1
- 230000003078 antioxidant effect Effects 0.000 claims 1
- 235000006708 antioxidants Nutrition 0.000 claims 1
- 230000003647 oxidation Effects 0.000 abstract description 3
- 238000007254 oxidation reaction Methods 0.000 abstract description 3
- 230000003026 anti-oxygenic effect Effects 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 4
- 229910052582 BN Inorganic materials 0.000 description 3
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910003978 SiClx Inorganic materials 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- LCDFWRDNEPDQBV-UHFFFAOYSA-N formaldehyde;phenol;urea Chemical compound O=C.NC(N)=O.OC1=CC=CC=C1 LCDFWRDNEPDQBV-UHFFFAOYSA-N 0.000 description 1
- 239000007770 graphite material Substances 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 239000012212 insulator Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 229920006122 polyamide resin Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Abstract
A kind of band coating graphite heater is characterized in that including graphite heater (1), the anti oxidation layer (3) being arranged on graphite heater (1): anti oxidation layer (3) is boron carbide and phenolic coating；Anti oxidation layer (3) is attached on graphite heater (1) by transition zone (2), and transition zone (2) is phenolic resin, epoxy resin, aldehyde ketone resin, furane resins, polyamide coating.It fundamentally solves the problems, such as graphite heater oxidation damage, has many advantages, such as that antioxygenic property is good, long service life.
Description
Technical field
The utility model relates to the component of graphitizing furnace, specifically a kind of band coating graphite heater.
Background technique
Graphite heater refers to that the electric furnace made of graphite material heats heater part.Graphite have excellent conduction,
Heating conduction is that graphite is commonly used in electric furnace as heater in special industrial furnace.Graphite electrode is selected to do in early days in industrial furnace
Heater, the oxidation rate and evaporation rate of graphite influence the service life of heater, when vacuum degree is 10-3~10-4mmHgWhen, make
It should be at 2300 DEG C or less with temperature.In protective atmosphere (logical H2、N2, Ar etc.) when, using temperature up to 3000 DEG C.Graphite cannot be
It is used in air, otherwise can occur to aoxidize and consume.
Boron nitride has a variety of excellent performances, is widely used in insulator, the automatic welding of high voltagehigh frequency electricity and plasma arc
Connect the coating of high temperature resistant frame, the material of high-frequency induction furnace, the solid phase admixture of semiconductor, atomic pile structural material,
Prevent the packaging material of neutron irradiation, the pass-through box of radar, the medium of radar antenna and constituent of rocket engine etc..Due to
With excellent greasy property, the release agent as high-temperature lubricant and a variety of models.The boron nitride of molding can manufacture high temperature resistant
Crucible and other products.
It in the prior art, is the inoxidizability and wearability that improve graphite body, if application publication number is CN 203024440
" a kind of solar energy hot-cast socket heating device " disclosed in the utility model patent of U, in the technical solution, by graphite, carbon
The setting of heater surface made of SiClx, refractory metal alloy etc. is using wrapping layer made of high-temperature resistant thermal insulating material.But simultaneously
Not specifically disclose the specific composition of the wrapping layer.
Utility model content
The purpose of the utility model is to provide a kind of band coating graphite heaters, fundamentally solve graphite heater
The problem of oxidation damage, has many advantages, such as that antioxygenic property is good, long service life.
To achieve the above object, the utility model provides following technical solution: the band coating graphite heater includes
Graphite heater, the anti oxidation layer being arranged on graphite heater, are characterized in that: anti oxidation layer is boron carbide and phenolic aldehyde tree
Rouge coating；Anti oxidation layer is attached on graphite heater by transition zone, and transition zone is phenolic resin, epoxy resin, aldehyde ketone tree
Rouge, furane resins, polyamide coating.
Although the utility model has the beneficial effects that graphite, silicon carbide, phenolic resin and epoxy resin etc. belong to it is common
Material, but be incorporated into the service life for extending graphite heater, the prior art there is no similar technical solution.?
Boron carbide and phenolic resin are uniformly dispersed by coating material, when in use, transition zone by organic solvent in anti oxidation layer
Organic material is dispersed in organic solvent (ethyl alcohol or acetoacetic ester), and phenolic resin in anti oxidation layer can have with transition zone
Machine material (phenolic resin, epoxy resin, aldehyde ketone resin, furane resins, polyamide) combines, to ensure that boron carbide
Evenly dispersed and stable coating.To finally improve the inoxidizability of graphite heater, and prolong its service life.
Detailed description of the invention
Fig. 1 is the using state structure diagram of the utility model.
Fig. 2 is the structural schematic diagram of the utility model.
Specific embodiment
Below in conjunction with Fig. 1 ~ 2, the content of the utility model is described in detail by specific embodiment.The band coating graphite hair
Hot body includes graphite heater 1, the anti oxidation layer being arranged on graphite heater 13.Wherein, anti oxidation layer 3 is boron carbide and phenol
Urea formaldehyde coating；Anti oxidation layer 3 is attached on graphite heater 1 by transition zone 2, and transition zone 2 is phenolic resin, asphalt mixtures modified by epoxy resin
Rouge, aldehyde ketone resin, furane resins, polyamide coating.
The utility model the preparation method is as follows:
Step 1, boron nitride, phenolic resin, alcohol are mixed and stirs evenly obtained coating paste, it is spare；
Step 2, by graphite heater surface phenolic resin, epoxy resin, aldehyde ketone resin, furane resins, polyamide resin
The uniform brushing naturally dry of the organic solvents mixed solution such as at least one of rouge etc. and ethyl alcohol or acetoacetic ester；
Step 3, coating naturally dry made from uniform squeegeeing step 1 after the graphite heater made from step 2 dries；
Step 4, will brush the graphite heater that finishes install to be passed through at 950 ~ 1000 DEG C of graphitizing furnace inert gas every
Carbonization treatment is carried out in the retort of exhausted air to get finished product.
Description of symbols:
1 graphite heater
2 transition zones
3 anti oxidation layers
4 graphitizing furnaces.
Claims (1)
1. a kind of band coating graphite heater, anti-oxidant on graphite heater (1) including graphite heater (1), setting
Layer (3), it is characterised in that: anti oxidation layer (3) is boron carbide and phenolic coating；Anti oxidation layer (3) is attached by transition zone (2)
On graphite heater (1), transition zone (2) be phenolic resin, epoxy resin, aldehyde ketone resin, furane resins, polyamide
Coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821654938.5U CN209497618U (en) | 2018-10-12 | 2018-10-12 | Band coating graphite heater |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821654938.5U CN209497618U (en) | 2018-10-12 | 2018-10-12 | Band coating graphite heater |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209497618U true CN209497618U (en) | 2019-10-15 |
Family
ID=68141604
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821654938.5U Active CN209497618U (en) | 2018-10-12 | 2018-10-12 | Band coating graphite heater |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209497618U (en) |
-
2018
- 2018-10-12 CN CN201821654938.5U patent/CN209497618U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Coated graphite heating element Granted publication date: 20191015 Pledgee: China Construction Bank Corporation Liaoyang Branch Pledgor: LIAONING JINGU CARBON MATERIAL CO.,LTD. Registration number: Y2024210000034 |