CN209378978U - A kind of organic intermediate hydrogenation reaction equipment - Google Patents
A kind of organic intermediate hydrogenation reaction equipment Download PDFInfo
- Publication number
- CN209378978U CN209378978U CN201821364042.3U CN201821364042U CN209378978U CN 209378978 U CN209378978 U CN 209378978U CN 201821364042 U CN201821364042 U CN 201821364042U CN 209378978 U CN209378978 U CN 209378978U
- Authority
- CN
- China
- Prior art keywords
- reaction warehouse
- reaction
- outside
- water
- organic intermediate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Abstract
A kind of organic intermediate hydrogenation reaction equipment, including pedestal, reaction warehouse is provided with above pedestal, the inside of pedestal is equipped with motor, the output end of motor is provided with the rotary shaft extended to inside reaction warehouse, and multiple groups mixing component is provided on the outside of rotary shaft, the side of reaction warehouse is provided with cold water storage cistern, and water pump is installed above cold water storage cistern, the pump mouth of water pump is equipped with the second water pipe for extending to cold water storage cistern inner bottom, cooling tube is provided on the outside of reaction warehouse, reaction warehouse is equipped with gas-guide tube above water pump side, and valve is provided on gas-guide tube.The utility model is stirred inside reaction warehouse by mixing component, react organic intermediate sufficiently with hydrogen, and pass through the graduation mark registration of observation air guide pipe surface, the reaction dosage of controllable hydrogen, it is allowed to accurately react with organic intermediate, and water cooling is carried out to reaction warehouse by being provided with cooling tube on the outside of reaction warehouse, it avoids heat from influencing reaction result, improves the purity of product.
Description
Technical field
The utility model relates to intermediate reaction technical field, specially a kind of organic intermediate hydrogenation reaction equipment.
Background technique
Intermediate initially refers to coal tar or oil product is Material synthesis fragrance, dyestuff, resin, drug, plasticizer, rubber
During the chemical products such as promotor, the intermediate product produced now refers to various centres obtained in organic synthesis process
Product, catalytic hydrogenation is the important technology of organic intermediate synthesis, instead of past iron powder reducing technology, for containing insatiable hunger
With the organic intermediate reduction reaction of gene, more clean and effective.
But existing organic intermediate hydrogenation reaction equipment can not be such that organic intermediate mixes with hydrogen sufficiently, and then make two
Person is not sufficiently reacted, and reduces reaction rate, and reacts closely bound up with temperature, and hydrogenation reaction heat release, heat cannot be timely
Processing, impacts to reaction result, the purity of product is made to be lower.
Utility model content
The purpose of this utility model is to provide a kind of organic intermediate hydrogenation reaction equipment, to solve above-mentioned background technique
The problem of middle proposition.
To achieve the above object, the utility model provides the following technical solutions: a kind of organic intermediate hydrogenation reaction equipment,
Including pedestal, reaction warehouse is provided with above the pedestal, the inside of the pedestal is equipped with motor, the output end of the motor
It is provided with the rotary shaft extended to inside reaction warehouse, and is provided with multiple groups mixing component on the outside of rotary shaft, the mixing component
Number be four groups, and mixing component includes casing and stirring blade, and stirring blade is provided on the outside of described sleeve pipe, described to stir
The number for mixing blade is three groups, and the stirring blade tilts down in the horizontal direction, and the angle of stirring blade and casing is
60 °, the side of the reaction warehouse is provided with cold water storage cistern, and water pump is equipped with above cold water storage cistern, the pump mouth peace of the water pump
Equipped with the second water pipe for extending to cold water storage cistern inner bottom, cooling tube is provided on the outside of the reaction warehouse, the cooling tube is in
Spiral distribution, and the water outlet of the cooling tube is connected with the first water pipe for extending to cold water storage cistern inner bottom, the water pump
Water outlet is connected with third water pipe, and the end of third water pipe is connected to the water inlet of cooling tube, and the reaction warehouse is close to water pump
Gas-guide tube is installed above side, and is provided with valve on gas-guide tube.
Preferably, feed inlet is provided at the top of the reaction warehouse, and the outside screw of feed inlet is connected with sealing cover.
Preferably, mechanical seal is provided on the outside of the rotary shaft, and mechanical seal is located at the bottom and bottom of reaction warehouse
The top of seat.
Compared with prior art, the utility model has the beneficial effects that this kind of organic intermediate hydrogenation reaction equipment passes through
Motor drives rotary shaft rotation, and then stirs mixing component inside reaction warehouse, keeps organic intermediate abundant with hydrogen
Reaction uniformly mixes, improves reaction rate, and by the graduation mark registration of observation air guide pipe surface, controllable hydrogen it is anti-
Application amount is allowed to accurately react with organic intermediate, and by being provided with cooling tube on the outside of reaction warehouse, water pump twitches cold water storage cistern
Internal cold water carries out water cooling to reaction warehouse, and the heat released to reaction is handled, and heat is avoided to influence reaction result, improves
The purity of product.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the main view of the utility model；
Fig. 3 is the structural schematic diagram of the mixing component of the utility model.
In figure: 1, pedestal；2, reaction warehouse；3, motor；4, rotary shaft；5, mixing component；5a, casing；5b, stirring blade；
6, feed inlet；7, sealing cover；8, mechanical seal；9, gas-guide tube；10, valve；11, the second water pipe；12, third water pipe；13, cooling
Pipe；14, cold water storage cistern；15, the first water pipe；16, water pump.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3 is please referred to, a kind of embodiment provided by the utility model: a kind of organic intermediate hydrogenation reaction equipment, packet
Pedestal 1 is included, the top of pedestal 1 is provided with reaction warehouse 2, and the inside of pedestal 1 is equipped with motor 3, and the output end of motor 3 is provided with
The rotary shaft 4 inside reaction warehouse 2 is extended to, and the outside of rotary shaft 4 is provided with multiple groups mixing component 5, the side of reaction warehouse 2 is set
It is equipped with cold water storage cistern 14, and the top of cold water storage cistern 14 is equipped with water pump 16, the pump mouth of water pump 16, which is equipped with, extends to cold water storage cistern 14
Second water pipe 11 of inner bottom, the outside of reaction warehouse 2 is provided with cooling tube 13, and the water outlet of cooling tube 13 is connected with extension
To the first water pipe 15 of 14 inner bottom of cold water storage cistern, the water outlet of water pump 16 is connected with third water pipe 12, and third water pipe 12
End is connected to the water inlet of cooling tube 13, and reaction warehouse 2 is equipped with gas-guide tube 9, and gas-guide tube above 16 side of water pump
It is provided with valve 10 on 9, controls the disengaging of hydrogen, cooling tube 13 is in spiral distribution, increases film-cooled heat, makes cooling effect more
It is good.
In this embodiment: water pump 16 twitches the cold water inside cold water storage cistern 14, and is back to cold water after the circulation of cooling tube 13
Case 14, cooling tube 13 can carry out water cooling to reaction warehouse 2, the heat for avoiding reaction from releasing is to reaction result in the outside of reaction warehouse 2
It impacts, ensure that the purity of product.
Attached drawing 1 and Fig. 3 are please referred to, the number of mixing component 5 is four groups, and mixing component 5 includes casing 5a and stirring blade
Stirring blade 5b is provided on the outside of 5b, casing 5a, the number of stirring blade 5b is three groups, and stirring blade 5b and casing 5a
Angle is 60 °, and stirring blade 5b is tilted down in the horizontal direction.
In the present invention, it is rotated, is stirred in the inside of reaction warehouse 2, and stirring blade by stirring blade 5b
5b is tilted with casing 5a, it is made to increase agitation amplitude in the vertical direction, and the contact area of organic intermediate and hydrogen becomes larger,
Promote the two reaction, improves the reaction rate of hydrogenation reaction.
Attached drawing 1 is please referred to, the top of reaction warehouse 2 is provided with feed inlet 6, and the outside screw of feed inlet 6 is connected with sealing
Lid 7；The outside of rotary shaft 4 is provided with mechanical seal 8, and mechanical seal 8 is located at the bottom of reaction warehouse 2 and the top of pedestal 1.
In the present invention, sealing cover 7 is unscrewed, reactant is added, then tighten sealing cover, keeps the leakproofness of equipment,
It avoids air from entering to impact reaction result, causes the purity of product not high, mechanical seal 8 can guarantee the sealing of equipment
Property, it avoids reactant from leaking out to the inside of pedestal 1, the normal work of motor 3 is impacted.
Working principle: unscrewing sealing cover 7, and organic intermediate and catalyst be put into the inside of reaction warehouse 2, gas-guide tube 9 with
Hydrogen-storing device is connected, and valve 10 is opened, and hydrogen enters the inside of reaction warehouse 2 from gas-guide tube 9, powers on, and motor 3 drives
Rotary shaft 4 rotates, and then stirs mixing component 5 in the inside of reaction warehouse 2, contacts organic intermediate with hydrogen, instead
It should mix, and react and release heat, water pump 16 can be made to work, the cold water inside cold water storage cistern 14 be extracted out, by spiral helicine cold
But pipe 13 is back to the inside of cold water storage cistern 13, and water resource, the inside cold water flow of cooling tube 13, to reaction are saved in recycling
Storehouse 2 carries out water cooling, reduces the temperature of charge inside reaction warehouse 2, avoids because the heat that reaction is released makes reaction result
At influence, the purity of reactant ensure that.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting
Related claim.
Claims (3)
1. a kind of organic intermediate hydrogenation reaction equipment, including pedestal (1), it is characterised in that: the top of the pedestal (1) is arranged
Have reaction warehouse (2), the inside of the pedestal (1) is equipped with motor (3), and the output end of the motor (3), which is provided with, to be extended to instead
The rotary shaft (4) for answering storehouse (2) internal, and multiple groups mixing component (5) are provided on the outside of rotary shaft (4), the mixing component (5)
Number be four groups, and mixing component (5) includes casing (5a) and stirring blade (5b), is provided on the outside of described sleeve pipe (5a)
Stirring blade (5b), the number of the stirring blade (5b) are three groups, and the stirring blade (5b) tilts down in the horizontal direction,
And the angle of stirring blade (5b) and casing (5a) are 60 °, the side of the reaction warehouse (2) is provided with cold water storage cistern (14), and cold
It is equipped with above water tank (14) water pump (16), the pump mouth of the water pump (16), which is equipped with, extends to cold water storage cistern (14) inner bottom
Second water pipe (11) at end is provided with cooling tube (13) on the outside of the reaction warehouse (2), and the cooling tube (13) is helically divided
Cloth, and the water outlet of the cooling tube (13) is connected with the first water pipe (15) for extending to cold water storage cistern (14) inner bottom, it is described
The water outlet of water pump (16) is connected with third water pipe (12), and the water inlet of the end of third water pipe (12) and cooling tube (13) connects
Logical, the reaction warehouse (2) is equipped with gas-guide tube (9) above water pump (16) side, and is provided with valve on gas-guide tube (9)
(10)。
2. a kind of organic intermediate hydrogenation reaction equipment according to claim 1, it is characterised in that: the reaction warehouse (2)
Top be provided with feed inlet (6), and the outside screw of feed inlet (6) is connected with sealing cover (7).
3. a kind of organic intermediate hydrogenation reaction equipment according to claim 1, it is characterised in that: the rotary shaft (4)
Outside be provided with mechanical seal (8), and mechanical seal (8) is located at the bottom of reaction warehouse (2) and the top of pedestal (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821364042.3U CN209378978U (en) | 2018-08-23 | 2018-08-23 | A kind of organic intermediate hydrogenation reaction equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821364042.3U CN209378978U (en) | 2018-08-23 | 2018-08-23 | A kind of organic intermediate hydrogenation reaction equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209378978U true CN209378978U (en) | 2019-09-13 |
Family
ID=67869286
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821364042.3U Active CN209378978U (en) | 2018-08-23 | 2018-08-23 | A kind of organic intermediate hydrogenation reaction equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209378978U (en) |
-
2018
- 2018-08-23 CN CN201821364042.3U patent/CN209378978U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206343183U (en) | A kind of chemical reaction kettle with heat insulation function | |
| CN201848251U (en) | Agitated reactor with stirring and liquid feeding device | |
| CN209378978U (en) | A kind of organic intermediate hydrogenation reaction equipment | |
| CN105771869B (en) | Chemical industry high efficiency solid-liquid reaction kettle | |
| CN207413248U (en) | A kind of synthesis device of alcohol-based fuel | |
| CN106669560A (en) | Use method of combined reactor | |
| CN206355974U (en) | A kind of reactor with liquid feeding buffer structure | |
| CN202778444U (en) | Steam heating and stirring reaction kettle | |
| CN208553865U (en) | A kind of industrial chemicals is pre-mixed device | |
| CN207287442U (en) | A kind of calcium hydroxide production retort | |
| CN206404772U (en) | A kind of synthesizing isocyanate reactor | |
| CN208346099U (en) | Waste plastic oil-refining equipment | |
| CN202011850U (en) | Multilayer stirring-type fixed bed reactor | |
| CN206751728U (en) | A kind of safe charging device of organic waste | |
| CN204914392U (en) | A material jar for high -pressure foaming machine | |
| CN205361325U (en) | Resin reaction kettle | |
| CN215389308U (en) | Synthetic cauldron of thiodicarb convenient to maintain | |
| CN206014774U (en) | A kind of full-mixing type catalytic cracking reaction device | |
| CN205667833U (en) | A kind of reactor | |
| CN205308247U (en) | Agitating unit ventilates | |
| CN216400085U (en) | Utensil dustproof concrete reation kettle | |
| CN205007949U (en) | Reaction kettle | |
| CN211837918U (en) | Sodium cromoglicate filter-pressing waste liquid recycle device | |
| CN216093466U (en) | Stirring device for storage battery separator slurry tank | |
| CN206424959U (en) | A kind of reactor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |