CN209271468U - A kind of fermentation partial crystallization reaction kettle - Google Patents
A kind of fermentation partial crystallization reaction kettle Download PDFInfo
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- CN209271468U CN209271468U CN201822122341.2U CN201822122341U CN209271468U CN 209271468 U CN209271468 U CN 209271468U CN 201822122341 U CN201822122341 U CN 201822122341U CN 209271468 U CN209271468 U CN 209271468U
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Abstract
The utility model relates to chemical industry mixing plant technical fields, specifically a kind of fermentation partial crystallization reaction kettle, it includes autoclave body, stirring system, power drive system composition, the autoclave body includes end socket, inner cylinder and jacket cylinder, it is characterized in that the outer wall of the inner cylinder is equipped with deflector, one end of deflector is connected with the outer wall of inner cylinder, the other end of deflector is equipped with clay layer, the jacket cylinder is set as the collet arc plate of two and half tile-type, the inner wall of two collet arc plates mutually welds after connecting with deflector clay layer zero clearance, air guide distributor is equipped with above the inner cylinder, air guide distributor is set as tubular structure, one end of the air guide distributor of tubular structure stretches out inner cylinder and is connected with air supply system, the other end of air guide distributor spiral inner cylinder top and on tube wall be equipped with venthole, with knot The advantages that structure is simple, energy-efficient, quick heating, temperature control standard, good heat insulation, easy to operate, long service life.
Description
Technical field
The utility model relates to chemical industry mixing plant technical field, specifically a kind of structure is simple, it is energy-efficient, rise
Warm fast, temperature control standard, good heat insulation, fermentation partial crystallization reaction kettle easy to operate, with long service life.
Background technique
It is well known that partial crystallization reaction kettle generally comprises vapour-liquid contact reaction kettle, outside heat removing reaction kettle, interior takes heat both at home and abroad
Formula reaction kettle.Vapour-liquid contact reaction kettle is mainly characterized by: device without mixing, it is external match heat exchanger, energy consumption is small, reaction is uniform, but
Coordinative composition of equipments and subsequent purification are more complex, and outside heat removing reaction kettle is mainly characterized by: having blender, is external with heat exchanger, volume benefit
Big with rate, energy consumption is high, and hot type reaction kettle is inside taken to be mainly characterized by: having blender, inner coil pipe, energy consumption is small, reaction heat distribution is more equal
Even, capacity utilization is low, and partial crystallization slot can use batch production method and continuous producing method, batch production method disadvantage
It is that system temperature, viscosity are difficult to control, particle diameter distribution is relatively narrow, and system is unstable.The technique of batch process combinations analysis, is suitable for small rule
Mould, multi-item production, continuous producing method feature are that production scale is big, and energy consumption is low, and productivity is high, high degree of automation,
Quantity of three wastes is few, but product is relatively fixed, replaces more difficult.
At present, partial crystallization reaction kettle always has a short item to restrict the needs of present technique, and for example, energy consumption is small to be set
Standby, subsequent corollary equipment just needs very complicated, and capacity utilization is low；The high just needs of capacity utilization are outer to match heat exchanger to increase
Heat exchange；So with the continuous development of present technique, it is necessary to which a kind of new-type partial crystallization reaction kettle meets the needs of industry.
Summary of the invention
The purpose of this utility model is to solve above-mentioned the deficiencies in the prior art, provide a kind of structure it is simple, it is energy-efficient, rise
Warm fast, temperature control standard, good heat insulation, fermentation partial crystallization reaction kettle easy to operate, with long service life.
The technical scheme adopted by the utility model to solve the technical problem is as follows:
A kind of fermentation partial crystallization reaction kettle, including autoclave body, stirring system, power drive system form, the autoclave body packet
End socket, inner cylinder and jacket cylinder are included, the upper and lower ends of the inner cylinder are closed through end socket connect respectively, on the autoclave body
End seal head is equipped with power drive system, and the output shaft of power drive system is put in inner cylinder to be connected with stirring system, institute
The external package connection jacket cylinder for the inner cylinder stated, it is characterised in that the outer wall of the inner cylinder is equipped on vertical direction
The deflector being arranged successively, one end of deflector are connected with the outer wall of inner cylinder, and the other end of deflector is equipped with clay layer, institute
The jacket cylinder stated is set as the collet arc plate of two and half tile-type, the inner wall of two collet arc plates respectively with the clay layer on deflector
Zero clearance is mutually welded after contradicting connection, and air guide distributor is equipped with above the inner cylinder, and air guide distributor is set as tubulose knot
Structure, one end of the air guide distributor of tubular structure stretch out inner cylinder and are connected with air supply system, another end plate of air guide distributor
It is spun on the top of inner cylinder and is equipped with venthole on tube wall, effectively controlled by air guide distributor and rate and total amount is added.
Be equipped with two groups of dismountable baffle plate assemblies in inner cylinder described in the utility model, every group of baffle plate assembly by
Support tube closed at both ends, baffle, support bar group are at one end of the support rod is vertical with inner cylinder inner wall to be connect, support
Clamping boss is equipped with above the other end of bar, the lower end of the support tube is equipped with clamping groove, the clamping of the lower end of support tube
Groove is connected on the clamping boss of support rod, realizes being detachably connected between support tube and support rod, the support tube
Side wall be equipped with baffle, one end of baffle is connected with support tube side wall, and the other end makes object in system towards inner cylinder center
Material is uniformly dispersed, and not will form topical gel.
It is equipped in inner cylinder described in the utility model and cleans pipe, the clean pipe is set as five, and two of them are cleaned
It is realized at two feed openings that the outlet end of pipe is respectively provided on inner cylinder and feed opening is washed away, two other cleans going out for pipe
Baffle plate assembly is washed away in the upper side realization that mouth end puts in the support tube being located in baffle plate assembly in inner cylinder respectively, finally
The outlet section of one clean pipe put in inner cylinder respectively be located at stirring system upper side realization stirring system is washed away,
The input end of five clean pipes is connected with water system.
The utility model is equipped with the deflector being arranged successively on vertical direction, water conservancy diversion due to the outer wall of the inner cylinder
One end of plate is connected with the outer wall of inner cylinder, and the other end of deflector is equipped with clay layer, and the jacket cylinder is set as two
The collet arc plate of half tile-type, the inner wall of two collet arc plates mutually weld after contradicting connection with the clay layer zero clearance on deflector respectively
It connects, air guide distributor is equipped with above the inner cylinder, air guide distributor is set as tubular structure, the air guide distributor of tubular structure
One end stretch out inner cylinder be connected with air supply system, the other end of air guide distributor spiral inner cylinder top and in tube wall
It is equipped with venthole, is effectively controlled by air guide distributor and rate and total amount is added, it is removable equipped with two groups in the inner cylinder
The baffle plate assembly unloaded, every group of baffle plate assembly is by support tube closed at both ends, baffle, support bar group at the support
One end of bar is vertical with inner cylinder inner wall to be connect, and is equipped with above the other end of support rod and is clamped boss, under the support tube
End is equipped with clamping groove, and the clamping groove of the lower end of support tube is connected on the clamping boss of support rod, realizes support tube and branch
The side wall of being detachably connected between strut, the support tube is equipped with baffle, and one end of baffle is connected with support tube side wall
It connects, the other end keeps material dispersion in system uniform towards inner cylinder center, not will form topical gel, sets in the inner cylinder
There is clean pipe, the clean pipe is set as five, and two that the outlet end of the clean pipe of two of them is respectively provided on inner cylinder add
It is realized at material mouth and feed opening is washed away, the outlet end that two other cleans pipe is put in inner cylinder respectively to be located in baffle plate assembly
Support tube upper side realization baffle plate assembly is washed away, the last item clean pipe outlet section put in inner cylinder respectively
Stirring system is washed away in the upper side realization for being located at stirring system, and the input end of five clean pipes is connected with water system
It connects, has many advantages, such as simple structure, energy-efficient, quick heating, temperature control standard, good heat insulation, easy to operate, long service life.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Specific embodiment
The present invention will be further described with reference to the accompanying drawing:
As shown in the picture, a kind of fermentation partial crystallization reaction kettle, including autoclave body, stirring system 1, power drive system 2 form,
The autoclave body includes end socket 3, inner cylinder 4 and jacket cylinder, and the upper and lower ends of the inner cylinder 4 are closed through end socket 3 respectively
Connection, the autoclave body upper end head 3 are equipped with power drive system 2, and the output shaft of power drive system 2 puts in inner cylinder 4
It is interior to be connected with stirring system 1, the external package connection jacket cylinder of the inner cylinder 4, it is characterised in that the inner cylinder
The outer wall of body 4 is equipped with the deflector 5 being arranged successively on vertical direction, and one end of deflector 5 is connected with the outer wall of inner cylinder 4
It connects, the other end of deflector 5 is equipped with clay layer, and the jacket cylinder is set as the collet arc plate 6 of two and half tile-type, two collets
The inner wall of arc plate 6 mutually welds after contradicting connection with the clay layer zero clearance on deflector 5 respectively, sets above the inner cylinder 4
There is air guide distributor 7, air guide distributor 7 is set as tubular structure, and inner cylinder 4 is stretched out in one end of the air guide distributor 7 of tubular structure
Be connected with air supply system, the other end of air guide distributor 7 spiral inner cylinder 4 top and on tube wall be equipped with venthole,
Rate and total amount is added by the effectively control of air guide distributor 7, is equipped with two groups of dismountable baffle groups in the inner cylinder 4
Part, every group of baffle plate assembly are made of support tube 8 closed at both ends, baffle 9, support rod 10, the support rod 10
One end is vertical with 4 inner wall of inner cylinder to be connect, and clamping boss 11 is equipped with above the other end of support rod 10, the support tube 8
Lower end is equipped with clamping groove, and the clamping groove of the lower end of support tube 8 is connected on the clamping boss 11 of support rod 10, realizes support
The side wall of being detachably connected between pipe 8 and support rod 10, the support tube 8 is equipped with baffle 9, one end of baffle 9 and branch
8 side wall of stay tube is connected, and the other end keeps material dispersion in system uniform towards 4 center of inner cylinder, not will form topical gel, institute
It is equipped in the inner cylinder 4 stated and cleans pipe 12, the clean pipe 12 is set as five, and two of them clean the outlet end difference of pipe 12
It is realized at two feed openings being located on inner cylinder 4 and feed opening is washed away, the outlet end that two other cleans pipe 12 is stretched respectively
Baffle plate assembly is washed away in the upper side realization for the support tube 8 being located in baffle plate assembly in into inner cylinder 4, and the last item is cleaned
The outlet section of pipe 12 put in inner cylinder 4 respectively be located at stirring system 1 upper side realize washing away to stirring system 1, five
The input end that item cleans pipe 12 is connected with water system.
When the utility model is used, due to use " clay method " guarantee deflector 5 and 6 gap of collet arc plate for zero, and
And collet uses 6 structure of collet arc plate of two half-watts, to guarantee to be heated evenly in kettle, meets making for design pressure and design temperature
Use condition；Can effectively control by using 7 structure of air guide distributor and rate and total amount is added: partial crystallization reaction process is in kettle
Atmosphere requirements are extremely tight, influence that obtained partial crystallization average molecular weight, insatiable hunger be right, amount of by-products, and air guide distributor 7 can be effective
The addition rate and total amount for controlling oxyalkylene can make partial crystallization average molecular weight obtained and theory using air guide distributor 7
Molecular weight is close；By using dismountable block plate component, so that high performance fluids is stirred blender and be divided into the fluid in kettle
Systemic circulation above and below inside and outside can make fluid flowing in kettle sufficiently, exchange heat in time, reduce the temperature gradient in kettle, make object in system
Material is uniformly dispersed, and not will form topical gel, the uniform particle sizes of dispersion, and viscosity is low；By using five in kettle clean pipes 12
Structure, directly wash away to slotting feed opening, baffle plate assembly, stirring system 1: the internals after material reaction in kettle have extension
The phenomenon that wall, increased five clean pipes 12 by the control to angle and spacing, directly against slotting feed opening, baffle plate assembly,
Stirring system 1 reduces the loss to material；The utility model is equipped on vertical direction due to the outer wall of the inner cylinder 4
One end of the deflector 5 being arranged successively, deflector 5 is connected with the outer wall of inner cylinder 4, and the other end of deflector 5 is equipped with clay
Layer, the jacket cylinder are set as the collet arc plate 6 of two and half tile-type, and the inner wall of two collet arc plates 6 is respectively and on deflector 5
Clay layer zero clearance contradict connection after mutually weld, air guide distributor 7 is equipped with above the inner cylinder 4, air guide distributor 7 sets
For tubular structure, one end of the air guide distributor 7 of tubular structure stretches out inner cylinder 4 and is connected with air supply system, air guide distributor 7
The other end spiral inner cylinder 4 top and on tube wall be equipped with venthole, pass through air guide distributor 7 effectively control be added speed
Rate and total amount, the inner cylinder 4 is interior to be equipped with two groups of dismountable baffle plate assemblies, and every group of baffle plate assembly is by closed at both ends
Support tube 8, baffle 9, support rod 10 form, one end of the support rod 10 is vertical with 4 inner wall of inner cylinder to be connect, support rod
Clamping boss 11 is equipped with above 10 other end, the lower end of the support tube 8 is equipped with clamping groove, the lower end of support tube 8
Clamping groove is connected on the clamping boss 11 of support rod 10, realizes being detachably connected between support tube 8 and support rod 10, institute
The side wall for the support tube 8 stated is equipped with baffle 9, and one end of baffle 9 is connected with 8 side wall of support tube, and the other end is towards inner cylinder 4
Center keeps material dispersion in system uniform, not will form topical gel, is equipped in the inner cylinder 4 and cleans pipe 12, described
It cleans pipe 12 and is set as five, the outlet end that two of them clean pipe 12 is respectively provided at two feed openings on inner cylinder 4 and realizes
Feed opening is washed away, the outlet end that two other cleans pipe 12 puts in inner cylinder 4 support being located in baffle plate assembly respectively
Baffle plate assembly is washed away in the upper side realization of pipe 8, and the outlet section that the last item cleans pipe 12, which is put in respectively in inner cylinder 4, to be set
Washing away to stirring system 1 is realized in the upper side of stirring system 1, and the input end of five clean pipes 12 is connected with water system
It connects, has many advantages, such as simple structure, energy-efficient, quick heating, temperature control standard, good heat insulation, easy to operate, long service life.
The present invention is due to using the above structure, having the advantages that:
1. the stabilization of reaction temperature in reaction process is heated evenly in easily-controllable, kettle；
2. rate and total amount is added in effective control, keep partial crystallization average molecular weight and theoretical molecular weight obtained close；
4. material dispersion is uniform in system, topical gel not will form, the uniform particle sizes of dispersion, viscosity is low；
5. loss of material is few, increase capacity utilization.
Claims (3)
1. a kind of fermentation partial crystallization reaction kettle, including autoclave body, stirring system, power drive system form, the autoclave body includes
End socket, inner cylinder and jacket cylinder, the upper and lower ends of the inner cylinder are closed through end socket connect respectively, the autoclave body upper end
End socket is equipped with power drive system, and the output shaft of power drive system is put in inner cylinder to be connected with stirring system, described
Inner cylinder external package connection jacket cylinder, it is characterised in that the outer wall of the inner cylinder be equipped on vertical direction according to
The deflector of secondary arrangement, one end of deflector are connected with the outer wall of inner cylinder, and the other end of deflector is equipped with clay layer, described
Jacket cylinder be set as the collet arc plates of two and half tile-type, the inner wall of two collet arc plates respectively with the clay layer zero on deflector
Gap is mutually welded after contradicting connection, and air guide distributor is equipped with above the inner cylinder, and air guide distributor is set as tubular structure,
One end of the air guide distributor of tubular structure stretches out inner cylinder and is connected with air supply system, and the other end of air guide distributor spirals
The top of inner cylinder is simultaneously equipped with venthole on tube wall, is effectively controlled by air guide distributor and rate and total amount is added.
2. a kind of fermentation partial crystallization reaction kettle according to claim 1, it is characterised in that be equipped with two in the inner cylinder
The dismountable baffle plate assembly of group, every group of baffle plate assembly is by support tube closed at both ends, baffle, support bar group at described
Support rod one end it is vertical with inner cylinder inner wall connect, clamping boss, the support are equipped with above the other end of support rod
The lower end of pipe is equipped with clamping groove, and the clamping groove of the lower end of support tube is connected on the clamping boss of support rod, realizes support
Being detachably connected between pipe and support rod, the side wall of the support tube are equipped with baffle, one end and support tube side of baffle
Wall is connected, and the other end keeps material dispersion in system uniform towards inner cylinder center, not will form topical gel.
3. a kind of fermentation partial crystallization reaction kettle according to claim 1, it is characterised in that be equipped with and wash in the inner cylinder
Net pipe, the clean pipe are set as five, and the outlet end that two of them clean pipe is respectively provided at two feed openings on inner cylinder
Place, which realizes, washes away feed opening, and the outlet end that two other cleans pipe puts in inner cylinder the branch being located in baffle plate assembly respectively
Baffle plate assembly is washed away in the upper side realization of stay tube, and the outlet section that the last item cleans pipe is put in inner cylinder respectively to be located at
Stirring system is washed away in the upper side realization of stirring system, and the input end of five clean pipes is connected with water system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822122341.2U CN209271468U (en) | 2018-12-18 | 2018-12-18 | A kind of fermentation partial crystallization reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822122341.2U CN209271468U (en) | 2018-12-18 | 2018-12-18 | A kind of fermentation partial crystallization reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209271468U true CN209271468U (en) | 2019-08-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822122341.2U Active CN209271468U (en) | 2018-12-18 | 2018-12-18 | A kind of fermentation partial crystallization reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209271468U (en) |
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2018
- 2018-12-18 CN CN201822122341.2U patent/CN209271468U/en active Active
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