CN209138033U - A kind of dibazol refining crystallization kettle - Google Patents

A kind of dibazol refining crystallization kettle Download PDF

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Publication number
CN209138033U
CN209138033U CN201821641884.9U CN201821641884U CN209138033U CN 209138033 U CN209138033 U CN 209138033U CN 201821641884 U CN201821641884 U CN 201821641884U CN 209138033 U CN209138033 U CN 209138033U
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China
Prior art keywords
crystallization
crystallization kettle
main body
storehouse
dibazol
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CN201821641884.9U
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Chinese (zh)
Inventor
韦建国
顾玉仅
朱凤
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Shanghai Qing Ping Pharmaceutical Co Ltd
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Shanghai Qing Ping Pharmaceutical Co Ltd
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Abstract

The utility model discloses a kind of dibazol refining crystallization kettles, including crystallization kettle main body, the middle position of the crystallization kettle body top is socketed with fixed disk, and the bottom of fixed disk is connected with filtering cabin, middle position at the top of the fixed disk is equipped with rotating electric machine, and the output end of rotating electric machine is connected with the first rotating shaft being through to inside filtering cabin, and the first paddle is evenly arranged on the outside of the first rotating shaft.The variable-frequency motor of the utility model setting drives crank rotation by the second shaft, crank drives the second paddle to move in a circle by agitating shaft, so that the mixture inside crystallization storehouse is constantly in vibrating state, so that the finished product that crystallization is completed is not in that the excessive phenomenon of conglomeration makes feeding more convenient, not only reduce the working strength for smashing process, and variable-frequency motor adjusts mixing speed so that crystallization effect improves, to improve the quality of crystalline product.

Description

A kind of dibazol refining crystallization kettle
Technical field
The utility model relates to medicine pharmaceutical field, specially a kind of dibazol refining crystallization kettle.
Background technique
With the development of science and technology more and more people are in default of movement and take exercise, many people are suffering from slight height Blood pressure, and Bendazol Tablets are the medicals for treating mild hypertension, so many pharmaceutical factories have all introduced dibazol purification knot Brilliant kettle processes Bendazol Tablets, but present dibazol refining crystallization kettle because crystallization so that a part of drug with Steam be lost, lead to wastage of material, so that production cost increases, and cause to take because conglomeration is excessive after the completion of crystallizing Material is difficult, and excessive velocities cause crystalline quality to reduce when increasing working strength to process is smashed, while crystallizing stirring.
Utility model content
The purpose of this utility model is to provide a kind of dibazol refining crystallization kettles, to solve to propose in above-mentioned background technique The problem of.
To achieve the above object, the utility model provides the following technical solutions: a kind of dibazol refining crystallization kettle, including knot Brilliant kettle main body, the middle position of the crystallization kettle body top is socketed with fixed disk, and the bottom of fixed disk is connected with filtering Storehouse, the middle position at the top of the fixed disk is equipped with rotating electric machine, and the output end of rotating electric machine is connected with and was through to First rotating shaft inside filter position is evenly arranged with the first paddle on the outside of the first rotating shaft, is located at the top of the fixed disk The side of rotating electric machine is provided with feed inlet, and the top of crystallization kettle main body two sides is all provided with reflux storehouse, and flows back in storehouse Portion is provided with the coiled pipe for being through to crystallization kettle body interior, and the middle position of crystallization kettle body interior bottom end is provided with Storehouse being crystallized, and having heaters is all installed in the bottom end of crystallization kettle body interior two sides, the bottom in the reflux storehouse is connected with tee tube, And the output end of tee tube has two groups, wherein tee tube output end described in one group is through crystallization kettle main body and extends to crystallization storehouse Inside, the bottom end of the crystallization kettle body side is equipped with variable-frequency motor, and the output end of variable-frequency motor is connected with through crystallization Kettle main body simultaneously extends to the second shaft inside crystallization storehouse, and the middle position of the crystallization storehouse two sides inner wall is all turned by bearing It is dynamic to be connected with crank, agitating shaft is provided between crank described in two groups, and the second paddle is evenly arranged on the outside of agitating shaft, The bottom end of the crystallization kettle main body front surface is provided with hermatic door.
Preferably, the surface of the filtering cabin is evenly arranged with through-hole, and filter screen is equipped between through-hole.
Preferably, second shaft is rotatablely connected with wherein crank described in one group, and the second shaft passes through crank handle turns Agitating shaft moves in a circle.
Preferably, two groups of output ends of the tee tube are all provided with valve.
Preferably, the first section of the coiled pipe is inverted funnel-form.
Preferably, sealing ring is provided at the position that the crystallization kettle main body is contacted with fixed disk.
Compared with prior art, the utility model has the beneficial effects that the variable-frequency motor of the utility model setting passes through the Two shafts drive crank rotation, and crank drives the second paddle to move in a circle by agitating shaft, so that mixed inside crystallization storehouse It closes object and is constantly in vibrating state, so that the finished product that crystallization is completed is not in that the excessive phenomenon of conglomeration makes feeding more square Just, not only reduce and smash the working strength of process, but also variable-frequency motor adjusts mixing speed so that crystallization effect improves, from And the quality of crystalline product is improved, make the vapor after evaporation become liquid through coiled pipe condensation by the reflux storehouse of setting Water reenters crystallization storehouse after valve opening and crystallizes again, so that the raw material contained in vapor be avoided to be wasted, and then subtracts Small production cost.
Detailed description of the invention
Fig. 1 is the surface structure schematic diagram of the utility model;
Fig. 2 is the schematic diagram of internal structure of the utility model;
Fig. 3 is the separated structure schematic diagram of the utility model.
In figure: 1, crystallization kettle main body;2, fixed disk;3, rotating electric machine;4, feed inlet;5, reflux storehouse;6, tee tube;7, close Closure door;8, variable-frequency motor;9, filtering cabin;10, heater;11, storehouse is crystallized;12, agitating shaft;13, the second paddle;14, crank; 15, the second shaft;16, coiled pipe;17, first rotating shaft;18, the first paddle.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3 is please referred to, a kind of embodiment provided by the utility model: a kind of dibazol refining crystallization kettle, including crystallization The middle position of kettle main body 1,1 top of crystallization kettle main body is socketed with fixed disk 2, and the bottom of fixed disk 2 is connected with filtering cabin 9, the middle position at 2 top of fixed disk is equipped with rotating electric machine 3, and the output end of rotating electric machine 3 is connected with and is through to filtering First rotating shaft 17 inside storehouse 9, the outside of first rotating shaft 17 are evenly arranged with the first paddle 18, are located at rotation at the top of fixed disk 2 The side of rotating motor 3 is provided with feed inlet 4, and the top of 1 two sides of crystallization kettle main body is all provided with reflux storehouse 5, and inside storehouse 5 of flowing back It is provided with the coiled pipe 16 being through to inside crystallization kettle main body 1, the middle position of 1 inner bottom of crystallization kettle main body is provided with knot Brilliant storehouse 11, and having heaters 10 is all installed in the bottom end of 1 inside two sides of crystallization kettle main body, the bottom in reflux storehouse 5 is connected with tee tube 6, and the output end of tee tube 6 has two groups, wherein 6 output end of a set of three links pipe through crystallization kettle main body 1 and extends to crystallization storehouse 11 inside, the bottom end of 1 side of crystallization kettle main body is equipped with variable-frequency motor 8, and the output end of variable-frequency motor 8 is connected with through knot Brilliant kettle main body 1 simultaneously extends to the second shaft 15 inside crystallization storehouse 11, and the middle position of crystallization 11 two sides inner wall of storehouse all passes through Bearing is rotatably connected to crank 14, agitating shaft 12 is provided between two groups of cranks 14, and the outside of agitating shaft 12 is evenly arranged with The bottom end of second paddle, 1 front surface of crystallization kettle main body is provided with hermatic door 7.
The variable-frequency motor 8 of the utility model setting drives crank 14 to rotate by the second shaft 15, and crank 14 passes through stirring Axis 12 drives the second paddle 13 to move in a circle, so that the mixture inside crystallization storehouse 11 is constantly in vibrating state, so that Crystallization complete finished product be not in that the excessive phenomenon of conglomeration makes feeding more convenient, not only reduce smash process work it is strong Degree, and variable-frequency motor 8 adjusts mixing speed so that crystallization effect improves, to improve the quality of crystalline product.
It please focus on refering to Fig. 2 and 3, the surface of filtering cabin 9 is evenly arranged with through-hole, and filter screen is equipped between through-hole, Sealing ring is provided at the position that crystallization kettle main body 1 is contacted with fixed disk 2.
This kind of dibazol refining crystallization kettle is filtered mixed liquor by setting filter screen in through-hole, so that after crystallization Quality improves, and can lead to wastage of material by the sealing ring of setting to avoid vapor leakage when crystallization.
It please focus on refering to Fig. 2 and 3, the second shaft 15 is rotatablely connected with wherein one group of crank 14, and the second shaft 15 passes through Crank 14 drives agitating shaft 12 to move in a circle.
This kind of dibazol refining crystallization kettle variable-frequency motor 8 drives crank 14 to rotate by the second shaft 15, and crank 14 passes through Agitating shaft 12 drives 13 circular motion of the second paddle, so that the solution inside crystallization storehouse 11 is in the state of concussion, passes through Variable-frequency motor 8 adjusts revolving speed and makes, and when crystallization is not in the excessive phenomenon of conglomeration, and the quality of crystallization can be improved.
Please be emphatically refering to fig. 1 with 2, two groups of output ends of tee tube 6 are all provided with valve, and the first section of coiled pipe 16 is to fall The funnel-form set.
The aqueous solution with raw material enters after the adjustable condensation of valve that this kind of dibazol refining crystallization kettle passes through setting The time for crystallizing storehouse 11, can crystallization rate be improved, the first section of coiled pipe 16 is that inverted funnel-form can be improved The water vapor absorption rate that crystallization is generated.
Working principle: first powering on this kind of device, and the raw material mixed liquor for needing to crystallize is added from feed inlet 4 In filtering cabin 9, rotating electric machine 3 drives the first paddle 18 to be rotated by first rotating shaft 17, and mixed liquor is by filter screen It is flowed into crystallization storehouse 11 under filtering from through-hole, the temperature inside 10 pairs of heater crystallization storehouses 11 is regulated and controled so that crystallizing in storehouse 11 It is suitable for the temperature crystallized that portion's temperature, which is in, and variable-frequency motor 8 drives crank 14 to be rotated by the second shaft 15 at the same time, bent Handle 14 drives the second paddle 13 to carry out circular motion by agitating shaft 12, so that the mixed liquor inside crystallization storehouse 11 is in Concussion state avoids the excessive phenomenon of conglomeration occur when crystallization, and the vapor that when crystallization generates enters from the head end of coiled pipe 16, Become liquid under condensation by coiled pipe 16 and flow into reflux storehouse 5, opens simultaneously the valve close to 1 side of crystallization kettle main body Door, condensed liquid are again introduced into crystallization storehouse 11 and are crystallized, and then vapor is avoided to carry waste caused by raw material, weight Multiple above-mentioned crystallisation step three times, makes full use of raw material, and hereafter opening the valve far from crystallization kettle main body 1 makes solution stream Out, hermatic door 7 is opened after the completion of crystallization, the raw material that crystallization is completed takes out, and completes the workflow of crystallization kettle.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting Related claim.

Claims (6)

1. a kind of dibazol refining crystallization kettle, including crystallization kettle main body (1), it is characterised in that: at the top of the crystallization kettle main body (1) Middle position be socketed with fixed disk (2), and the bottom of fixed disk (2) is connected with filtering cabin (9), fixed disk (2) top The middle position in portion is equipped with rotating electric machine (3), and the output end of rotating electric machine (3) is connected with and is through in filtering cabin (9) The first rotating shaft (17) in portion is evenly arranged with the first paddle (18) on the outside of the first rotating shaft (17), the fixed disk (2) The side that top is located at rotating electric machine (3) is provided with feed inlet (4), and the top of crystallization kettle main body (1) two sides is all provided with It flows back storehouse (5), and reflux storehouse (5) is internally provided with and is through to the internal coiled pipe (16) of crystallization kettle main body (1), the crystallization kettle The middle position of main body (1) inner bottom is provided with crystallization storehouse (11), and the bottom end of the internal two sides of crystallization kettle main body (1) is all pacified Equipped with heater (10), the bottom of reflux storehouse (5) is connected with tee tube (6), and the output end of tee tube (6) has two groups, Wherein (6) output end of tee tube described in one group runs through crystallization kettle main body (1) and extends to the inside of crystallization storehouse (11), the crystallization The bottom end of kettle main body (1) side is equipped with variable-frequency motor (8), and the output end of variable-frequency motor (8) is connected with through crystallization kettle master Body (1) simultaneously extends to internal the second shaft (15) of crystallization storehouse (11), the middle position of crystallization storehouse (11) two sides inner wall It is all rotatably connected to crank (14), is provided between crank described in two groups (14) agitating shaft (12), and agitating shaft by bearing (12) the second paddle is evenly arranged on the outside of, the bottom end of crystallization kettle main body (1) front surface is provided with hermatic door (7).
2. a kind of dibazol refining crystallization kettle according to claim 1, it is characterised in that: the surface of the filtering cabin (9) It is evenly arranged with through-hole, and filter screen is installed between through-hole.
3. a kind of dibazol refining crystallization kettle according to claim 1, it is characterised in that: second shaft (15) and its In the rotation connection of crank (14) described in one group, and the second shaft (15) drives agitating shaft (12) to do circumference fortune by crank (14) It is dynamic.
4. a kind of dibazol refining crystallization kettle according to claim 1, it is characterised in that: two groups of the tee tube (6) Output end is all provided with valve.
5. a kind of dibazol refining crystallization kettle according to claim 1, it is characterised in that: the first section of the coiled pipe (16) For inverted funnel-form.
6. a kind of dibazol refining crystallization kettle according to claim 1, it is characterised in that: the crystallization kettle main body (1) with Sealing ring is provided at the position of fixed disk (2) contact.
CN201821641884.9U 2018-10-10 2018-10-10 A kind of dibazol refining crystallization kettle Active CN209138033U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821641884.9U CN209138033U (en) 2018-10-10 2018-10-10 A kind of dibazol refining crystallization kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821641884.9U CN209138033U (en) 2018-10-10 2018-10-10 A kind of dibazol refining crystallization kettle

Publications (1)

Publication Number Publication Date
CN209138033U true CN209138033U (en) 2019-07-23

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113289368A (en) * 2021-05-25 2021-08-24 山东信科环化有限责任公司 Continuous crystallization device of barium chloride
CN116239135A (en) * 2022-12-27 2023-06-09 宿迁华虹电子工业有限公司 Aluminum chloride crystallization process with pretreatment feeding equipment
CN116392847A (en) * 2023-06-02 2023-07-07 北京市弘洁蓝天科技股份有限公司 Evaporation crystallization device for fly ash water washing liquid

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113289368A (en) * 2021-05-25 2021-08-24 山东信科环化有限责任公司 Continuous crystallization device of barium chloride
CN113289368B (en) * 2021-05-25 2022-08-23 山东信科环化有限责任公司 Continuous crystallization device of barium chloride
CN116239135A (en) * 2022-12-27 2023-06-09 宿迁华虹电子工业有限公司 Aluminum chloride crystallization process with pretreatment feeding equipment
CN116239135B (en) * 2022-12-27 2023-10-27 宿迁华虹电子工业有限公司 Aluminum chloride crystallization process with pretreatment feeding equipment
CN116392847A (en) * 2023-06-02 2023-07-07 北京市弘洁蓝天科技股份有限公司 Evaporation crystallization device for fly ash water washing liquid
CN116392847B (en) * 2023-06-02 2023-08-22 北京市弘洁蓝天科技股份有限公司 Evaporation crystallization device for fly ash water washing liquid

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