CN208459205U - Fully-automatic ceramic brick boiling process moisture content test case - Google Patents

Fully-automatic ceramic brick boiling process moisture content test case Download PDF

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CN208459205U
CN208459205U CN201820999391.6U CN201820999391U CN208459205U CN 208459205 U CN208459205 U CN 208459205U CN 201820999391 U CN201820999391 U CN 201820999391U CN 208459205 U CN208459205 U CN 208459205U
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test
water
temperature
experimental tank
specimen holder
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郑靓
王元光
段瑞斌
王新祥
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Guangdong Provincial Academy of Building Research Group Co Ltd
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Guangdong Provincial Academy of Building Research Group Co Ltd
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Abstract

The utility model discloses a kind of fully-automatic ceramic brick boiling process moisture content test case, it further includes temperature control system and test water cooling recirculation system that chamber, which includes experimental tank, specimen holder, porous barrier,;Specimen holder is mounted in experimental tank, the slot bottom 5cm or more of distance test (DT) sink;The heating rod of temperature control system is arranged below specimen holder, porous barrier is laid between specimen holder and heating rod, the temperature controller of temperature control system passes through the water temperature of temperature sensor monitoring test sink, control heating rod work whether and operating time, the inlet and outlet of test water cooling recirculation system are connected to experimental tank, temperature controller is connect with test water cooling recirculation system simultaneously, whether Control experiment is water-cooled circulatory system work.Boiling test is carried out to Ceramic Tiles using chamber, the working efficiency of testing crew can be greatlyd improve, while being conducive to improve the accuracy of test result.

Description

Fully-automatic ceramic brick boiling process moisture content test case
Technical field
The utility model relates to Ceramic Tiles water absorption rate determination techniques, and in particular to a kind of fully-automatic ceramic brick boiling process water suction Rate chamber.
Background technique
Ceramic Tiles are one of most important most common decorating and renovating materials, the main performance of Ceramic Tiles include presentation quality, Dimensional discrepancy, water absorption rate, breakdown strength, wearability and anti-glaze fragility etc., wherein water absorption rate is most important parameter, is to determine pottery The important indicator of ceramic tile quality good or not.
When usual water absorption rate refers to that Ceramic Tiles unit mass reaches saturation water suction under drying regime, the quality hundred of moisture is absorbed Divide rate.The foundation that national standard GB/T4100-2015 " Ceramic Tiles " uses water absorption rate to classify as Ceramic Tiles.
The test method of existing Ceramic Tiles water absorption rate mainly has national standard GB/T3810.3-2016 " Ceramic Tiles test method 3 parts: the measurement of water absorption rate, apparent porosity, apparent relative density and bulk density " defined boiling process and vacuum method.Above-mentioned mark Standard clearly states boiling process suitable for Ceramic Tiles classification and the description of product, and vacuum method is suitable for apparent porosity, apparent relative density With the water absorption rate measurement in addition to classification.The method for carrying out product classification and quality inspection to Ceramic Tiles should use boiling process.
National standard GB/T3810.3-2016 provides as follows ceramic tile boiling process test process: brick is vertically placed on to Sheng Have in the heating device of deionized water, brick is made to be not in contact with each other, from the water surface at least 5cm, lower part should be maintained far from the bottom on the top of brick At least distance of 5cm, and should all keep the water surface to be higher than brick top surface 5cm or more in entire test.It heats water to boiling and protects Fluidized state 2h is held, heat source is then cut off.There are two types of operations below: it is cooled to room temperature first, being completely sunk in the water brick, and 4 ± 0.25h is impregnated at room temperature;Second, can also after keeping fluidized state 2h, under room temperature deionized water or refrigerator will Sample is cooled to room temperature, and then impregnates 4 ± 0.25h at room temperature.Finally, requiring to be soaked with one piece and the chamois leather wrung out is put Every piece of surface turned is lightly dried on platform, and surface water is trippingly wiped using chamois leather for concave-convex or card-cut surface Point, it then weighs, records the weighing result of every piece of sample, water absorption rate E=(m1-m0)/m0× 100%, wherein m0Indicate ceramics Dry mass after brick drying, m1Quality after indicating Ceramic Tiles water suction.
Above-mentioned national standard has only simply specified test procedure, and the corresponding test apparatus used is not suggested.Currently, people Electromagnetic oven etc. is mostly used to boil Ceramic Tiles greatly, and complete ceramics in such a way that manual time-keeping plus cooling water are cooling The boiling test of brick.Above-mentioned test process whole process needs are artificial on duty, first have to when artificial observation boils, set 2h after boiling Be then shut off test apparatus, then give sample cooling, finally reset the soaking at room temperature time, although workload is little, it is time-consuming compared with It is long, it greatly affected the working efficiency of testing crew, since different step interval time is longer, testing crew is very in practice The problem of hardly possible guards always on side, often will appear too long boiling time or long soaking time causes test result inaccurate.
In conclusion the test apparatus of existing Ceramic Tiles boiling test, greatly affected the test efficiency of testing crew, And easily lead to test result inaccuracy.
Utility model content
Technical problem to be solved by the utility model is to provide a kind of fully-automatic ceramic brick boiling process moisture content tests Case carries out boiling test to Ceramic Tiles using it, can greatly improve the working efficiency of testing crew, while being conducive to improve examination Test the accuracy of result.
The utility model technical problem solves by following technical solution: a kind of fully-automatic ceramic brick boiling process water absorption rate examination Tryoff, including experimental tank, specimen holder, porous barrier further include temperature control system and test water cooling recirculation system;
The specimen holder is mounted in the experimental tank, the slot bottom 5cm or more apart from the experimental tank;
The temperature control system includes heating rod, and the heating rod is arranged below the specimen holder, it is described it is porous every Plate is laid between the specimen holder and the heating rod, and the temperature control system further includes temperature sensor and temperature control Device, the temperature sensor are arranged in the experimental tank, and the temperature controller is arranged on the outside of experimental tank, and described Temperature sensor is connected with the heating rod, and the temperature controller is detected in the experimental tank by the temperature sensor The water temperature of test water, then control the heating rod work whether and operating time;
The inlet and outlet of the test water cooling recirculation system are connected to the experimental tank, the temperature Controller is connect with the test water cooling recirculation system, whether controlling test water cooling recirculation system work.
The experimental tank recommended configuration sink cover.
As the preferred of test water cooling recirculation system and experimental tank connection type: the test water cooling cycle The communicating position of the water outlet of system and the experimental tank is located at below the porous barrier.
Porous barrier is used for balanced water temperature, so that sample is heated, is cooled uniformly.
Preferred embodiment as specimen holder: the specimen holder includes two guide rails, and two guide rails are arranged in parallel, and is used for support Two cylindrical slides are at least set on the two sides of sample, every guide rail, which prevents simultaneously for being spaced apart different samples Sample is toppled over.The guide rail is made of the bracket that top surface is provided with card slot, on the cross section of the guide rail, the card slot notch two With a certain distance from side all has from corresponding side cell wall the widest part;The sliding block lower section is embedded in the card slot, the lesser upper section of diameter It is pierced by from the notch of the card slot.
Preferred embodiment as test water cooling recirculation system: the test water cooling recirculation system includes electricity Magnet valve, water circulating pump, filter, condenser, they are connected in turn on the pipeline for being connected to the water inlet and water outlet.
Preferred embodiment as the chamber: the chamber further includes having box shell, and the experimental tank is fixed On the inside of the box shell, experimental tank notch is exposed by the top of the box shell.Box shell is promoted for experimental tank to be isolated The safety of chamber.
The chamber is integrated machine, wherein the test water cooling recirculation system is arranged in the box shell, is located at In space below the experimental tank, the temperature controller is fixed on the tank wall of the box shell.
Fully-automatic ceramic brick boiling process moisture content test method based on above-mentioned chamber, steps are as follows:
1) sample is placed on specimen holder, is then injected into deionized water, guarantee water surface distance sample top surface 5cm or more;
2) setting temperature controller is required according to national standard GB/T3810.3-2016
The boiling temperature of set temperature controller, temperature controller detect test water water temperature by temperature sensor, When water temperature reaches the boiling temperature, start timing, control the heating rod work on 2h then stop;
The cooling temperature of set temperature controller, the cooling temperature are usually arranged as room temperature, generally 20~25 °C, heating After stick stops working, temperature controller controls the test water cooling recirculation system work, reduces test water water temperature, temperature Controller detects test water water temperature, when water temperature is reduced to the cooling temperature, temperature controller control by temperature sensor It makes the test water cooling recirculation system to stop working, and starts timing, impregnate 4 ± 0.25h;
3) after impregnating, ceramics sample is taken out, is dried, weighed, record the weighing result of every piece of sample, calculate water suction Rate.
The test water cooling recirculation system by water temperature be reduced to cooling temperature process duration control 30~ 40min is advisable.Anti- defervescence boil after ceramic tile because chilling generate cracking and stomata shrink and closing, and then influence test result, It can be according to parameters such as test water tank volumes, when the cooling recirculation system of corresponding heat radiation power being selected to reach above-mentioned cooling to control It is long.
Compared with the prior art, the utility model has the following beneficial effects:
1) the utility model chamber is passed for second of mode of operation design of boiling method in background technique by temperature Sensor detects test water water temperature, then deploys heating rod according to water temperature and test water cooling recirculation system works, test people Member need to only complete preparation i.e. above-mentioned steps 1 originally), and round-off work, that is, above-mentioned steps 3 after the test), remaining Work boils boiling and boils the control of time, then to being cooled to room temperature and the control of soak at room temperature time, completely by testing Case is automatically performed, and after experimenter completes preliminary preparation, can do other things, and then later period ending is done in timing back Work can greatly improve the test efficiency of testing crew, only one whole time limit needs to go to grasp, and reduce artificial The influence of factor is conducive to the accuracy for improving test result;The utility model chamber considers to realize test process except simple It automatically controls outer, it is also contemplated that influence of the chamber mechanical structure to test effect is such as added the porous barrier of balanced water temperature, made Sample is heated during heating and cooling, is cooled uniformly, the test error for avoiding experimental rig defect to introduce as far as possible;
2) the utility model specimen holder uses the combination of guide rail and sliding block, and sliding block is used to support and is spaced different samples, By adjusting the distance between two sliding blocks, it can be adapted to the sample of different-thickness, the utility model chamber can once complete multiple groups The test of different size sample;
3) the boiling process moisture content test is completed using above-mentioned chamber, can greatly improve the test efficiency of testing crew, The accuracy for being conducive to improve test result simultaneously improves water in addition, the chamber test water uses cooling cycle mode Utilization efficiency, saved water resource.
Detailed description of the invention
Fig. 1 is the chamber structural schematic diagram of the utility model embodiment one;
Fig. 2 is the structural schematic diagram of the porous barrier of embodiment one;
Fig. 3 is embodiment a sample frame wherein a guide rail and top view of cylindrical slide thereon;
Fig. 4 front view of cylindrical slide for guide rail in Fig. 3 and thereon;
Fig. 5 A-A cross-sectional view of cylindrical slide for guide rail in Fig. 3 and thereon.
Specific embodiment
Embodiment one
The chamber of embodiment one is designed according to second of mode of operation of boiling method in background technique, as shown in Figure 1, its Using all-in-one machine structure, comprising: box shell 1, experimental tank 1.1, specimen holder 2, porous barrier 3, further include temperature control system and Test water cooling recirculation system.
Experimental tank 1.1 is fixed on 1 inside of box shell, and 1.1 notch of experimental tank passes through outside the opening on the top plate of box shell 1 Dew, is sealedly and fixedly connected with the open edge.Box shell 1 is for experimental tank 1.1 to be isolated, the safety of lifting test case.Examination Sink 1.1 is tested equipped with sink cover (being not drawn into the present embodiment), lid reduces moisture loss, simultaneously for guarantee test safety Prevent dust from falling into.
Specimen holder 2 is mounted in experimental tank 1.1, the slot bottom 5cm or more of distance test (DT) sink 1.1.Such as the institute of Fig. 1,3,4 Show, specimen holder 2 includes two guide rails 2.1, and two guide rails 2.1 are arranged in parallel, for support on the two sides of sample, every guide rail 2.1 Several (two or more) cylindrical slides 2.2 are provided with, which prevents sample from inclining for being spaced apart different samples ?.Guide rail 2.1 is made of the bracket that top surface is provided with card slot 2.11, and 2.11 structure of card slot is as shown in figure 5,2.2 lower section of sliding block is embedded in In card slot 2.11, the lesser upper section of diameter is pierced by from the notch of card slot 2.11, can be slided along card slot 2.11.The specimen holder of the structure 2 can easily be adapted to the sample of different-thickness.
Water temperature of the temperature control system for test water in Control experiment sink 1.1, including heating rod 5, temperature sensing Device 4 and temperature controller 14.Heating rod 5 is arranged below specimen holder 2, porous barrier 3 be laid in specimen holder 2 and heating rod 5 it Between, temperature sensor 4 be arranged in experimental tank 1.1, temperature controller 14 is then fixed in box shell 1, temperature controller 14 with Temperature sensor 4 and heating rod 5 connect, and temperature controller 14 detects test water in experimental tank 1.1 by temperature sensor 4 Water temperature, then control heating rod 5 work whether and operating time.
It is big to be uniformly distributed aperture as shown in Fig. 2, be made by stainless steel plate for the structure of above-mentioned porous barrier 3 on steel plate The about circular hole of 10mm, hole back gauge range 10-12mm are preferred.Porous barrier 3 is used for balanced water temperature, so that sample is heated, is cooled It is even.
The inlet and outlet of test water cooling recirculation system are connected to experimental tank 1.1, and communicating position position In 3 lower section of mesh partition.Test water cooling recirculation system is arranged in box shell 1, is particularly located at the sky of 1.1 lower section of experimental tank Between in, as shown in Figure 1.Test water cooling recirculation system includes solenoid valve 6, water circulating pump 7, filter 9, condenser 10, it Be connected to connection test in turn and be water-cooled on the water inlet of the circulatory system and the pipeline 8 of water outlet.Temperature controller 14 with Solenoid valve 6 connects, and is controlled by temperature controller 14, and solenoid valve 6 is used to control the opening and closing of pipeline 8.Water circulating pump 7 is used in pipeline In the case that 8 open, test water circulating cooling in condenser 10 and experimental tank 1.1 is driven.Filter 9 is for filtering examination It tests and uses water, and can be cleaned with regular dismounting.
Power switch 12 and water circulating pump power switch 13 are also equipped in box shell 1.Power switch 12 is entire for controlling The power supply of chamber, water circulating pump power switch 13 is then for controlling the power supply of water pump.
The temperature controller 14 used in above-described embodiment is the intelligent PID temperature digital display controller of anthone.
The condenser 10 used in above-described embodiment is the copper pipe radiator up to company's production of putting forth energy.
In above-described embodiment water circulating pump 7 using Nanjing letter can company production synthetic material circulating pump WS246.
When temperature controller 14 controls the unlatching pipeline 8 of solenoid valve 6, while controlling above-mentioned condenser 10, water circulating pump 7 etc. Power supply is connected, to control above-mentioned test water cooling recirculation system work.
Fully-automatic ceramic brick boiling process moisture content test method based on above-mentioned chamber, includes the following steps:
1) sample is placed on specimen holder, is then injected into deionized water, guarantee water surface distance sample top surface 5cm or more, Cover slot cover.Sample also relates to preparation of samples.Preparation of samples provides to carry out according to standard GB/T3810.3-2016, and according to Drying to constant weight for standard requirements, weighs after cooling and reaches initial weight.
2) setting temperature controller is required according to national standard GB/T3810.3-2016
The boiling temperature of set temperature controller, temperature controller detect test water water temperature by temperature sensor, When water temperature reaches the boiling temperature, start timing, control the heating rod work on 2h then stop;
The cooling temperature of set temperature controller, the cooling temperature are usually arranged as room temperature, generally 20-25 °C, heating After stick stops working, temperature controller controls the test water cooling recirculation system work, reduces test water water temperature, temperature Controller detects test water water temperature, when water temperature is reduced to the cooling temperature, temperature controller control by temperature sensor It makes the test water cooling recirculation system to stop working, and starts timing, impregnate 4 ± 0.25h.
3) after impregnating, ceramics sample is taken out, the chamois leather for being soaked and being wrung out with one piece, which is placed on platform, lightly to be wiped Every piece of surface turned is done, weighing records the weighing result of every piece of sample, calculates water absorption rate.
Water temperature is reduced to the control of cooling temperature process duration by test water cooling recirculation system to be advisable in 30-40min.
Note: the utility model step 2 is automatically performed by chamber, when step 1) adds deionized water, should ensure that in step During the rapid boiling for 2) being up to two hours is boiled, the water surface can all be kept above the distance of sample top surface 5cm or more.Specific steps 1) The deionized water water surface of middle addition is higher by the degree of sample top surface, generally after carrying out above-mentioned test process more than once, according to Empirical value is confirmable.
Embodiment two
Embodiment two and embodiment one the difference is that eliminate test water cooling recirculation system namely embodiment two its It is second of mode of operation design according to boiling method in background technique in fact.

Claims (8)

1. a kind of fully-automatic ceramic brick boiling process moisture content test case, which is characterized in that including experimental tank, specimen holder, porous Partition further includes temperature control system and test water cooling recirculation system;
The specimen holder is mounted in the experimental tank, the slot bottom 5cm or more apart from the experimental tank;
The temperature control system includes heating rod, and the heating rod is arranged below the specimen holder, and the porous barrier is flat It being layered between the specimen holder and the heating rod, the temperature control system further includes temperature sensor and temperature controller, The temperature sensor is arranged in the experimental tank, and the temperature controller is arranged on the outside of experimental tank, with the temperature Degree sensor is connected with the heating rod, and the temperature controller detects the experimental tank pilot scale by the temperature sensor The water temperature with water is tested, whether then controlling heating rod work and operating time;
The inlet and outlet of the test water cooling recirculation system are connected to the experimental tank, the temperature control Device is connect with the test water cooling recirculation system, whether controlling test water cooling recirculation system work.
2. chamber according to claim 1, which is characterized in that the experimental tank is configured with sink cover.
3. chamber according to claim 2, which is characterized in that the water outlet of the test water cooling recirculation system with The communicating position of the experimental tank is located at below the porous barrier.
4. chamber according to claim 3, which is characterized in that the specimen holder includes two guide rails, and two guide rails are set in parallel It sets, two cylindrical slides is at least set on the two sides of sample, every guide rail for support.
5. chamber according to claim 4, which is characterized in that the guide rail is made of the bracket that top surface is provided with card slot, On the cross section of the guide rail, the card slot is in convex;The sliding block lower section is embedded in the card slot, on diameter is lesser Section is pierced by from the relatively narrow notch of the card slot.
6. chamber according to claim 4, which is characterized in that the test water cooling recirculation system includes electromagnetism Valve, water circulating pump, filter, condenser, they are connected in turn on the pipeline for being connected to the water inlet and water outlet.
7. chamber according to claim 6, which is characterized in that the chamber further includes having box shell, the test water Slot is fixed on the inside of the box shell, and experimental tank notch is exposed by the top of the box shell.
8. chamber according to claim 7, which is characterized in that the chamber is integrated machine, wherein the test is used Water-cooling circulating system is arranged in the box shell, and in the space below the experimental tank, the temperature controller is solid It is scheduled on the tank wall of the box shell.
CN201820999391.6U 2018-06-27 2018-06-27 Fully-automatic ceramic brick boiling process moisture content test case Active CN208459205U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108956358A (en) * 2018-06-27 2018-12-07 广东省建筑科学研究院集团股份有限公司 Fully-automatic ceramic brick boiling process moisture content test case and the test method based on the chamber

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108956358A (en) * 2018-06-27 2018-12-07 广东省建筑科学研究院集团股份有限公司 Fully-automatic ceramic brick boiling process moisture content test case and the test method based on the chamber

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