CN208449299U - A kind of antioxidant consersion unit - Google Patents
A kind of antioxidant consersion unit Download PDFInfo
- Publication number
- CN208449299U CN208449299U CN201820599312.2U CN201820599312U CN208449299U CN 208449299 U CN208449299 U CN 208449299U CN 201820599312 U CN201820599312 U CN 201820599312U CN 208449299 U CN208449299 U CN 208449299U
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- CN
- China
- Prior art keywords
- reaction kettle
- antioxidant
- charging aperture
- consersion unit
- cooling jacket
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- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 19
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims abstract description 55
- 230000007246 mechanism Effects 0.000 claims abstract description 27
- 238000001816 cooling Methods 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000003381 stabilizer Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 3
- 238000012824 chemical production Methods 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 3
- 238000007259 addition reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model provides a kind of antioxidant consersion unit, more particularly to technical field of chemical production equipment, including reaction kettle ontology, feeding cylinder, condensing mechanism, rabbling mechanism and microwave generator component, heater strip is arranged with outside the reaction kettle body outer wall, the heater strip is externally provided with insulating layer, the reaction kettle bodies top is equipped with first charging aperture and second charging aperture, the feeding cylinder is equipped in the first charging aperture, the feeding cylinder is equipped with valve, the condensing mechanism is movably equipped in the second charging aperture, the rabbling mechanism is equipped in the reaction kettle ontology, the reaction kettle body bottom portion is further fixed on the microwave generator component.The utility model has the advantages of improving reaction rate, improving yield.
Description
Technical field
The utility model belongs to technical field of chemical production equipment, and in particular to a kind of antioxidant consersion unit.
Background technique
Hinered phenols antioxidant is needed when synthesizing by mikey addition reaction, and reaction is generally heated in mikey addition reaction,
It needs to carry out at relatively high temperatures, that there are reaction speeds is slower in synthesis for existing Hinered phenols antioxidant, when needing to react
Between longer, the problems such as reaction yield is low.
Patent antioxidant reaction unit (application No. is 201520347457.X) discloses a kind of antioxidant reaction unit,
Including reaction kettle ontology, reaction kettle bodies top is equipped with top cover, and bottom is equipped with bottom cover, bottom cover and top cover respectively with react
It being threadedly coupled between kettle ontology, top cover is equipped with feed inlet, and feed inlet uses a rectangle nozzle, is equipped with filtering plug in feed inlet,
Filtering plug is fixed on feed inlet, and feed inlet is equipped with sealing cover at upper surface, detachable between sealing cover and feed inlet
It connects, destilling tower is installed in reaction kettle ontology, destilling tower is fixed on reaction kettle ontology, and distilling path is equipped in bottom cover, is steamed
It evaporates channel roof to correspond to destilling tower setting and be connected, bottom is arranged across bottom cover.This antioxidant reaction unit can be effective
Eliminate the unstability of solution of organic compound, it is ensured that the safety of production, reaction process is mild, and equipment is not easily susceptible to corrode,
Distilling effect is obvious, and reactant purity is high feeds intake easily controllable, easy to operate, is suitable for being widely used.However the utility model
Reaction rate can not be improved.
Therefore, it is badly in need of a kind of raising reaction rate, improves the antioxidant consersion unit of yield.
Utility model content
In order to solve the problems, such as that existing antioxidant production equipment reaction rate is low, the purpose of the utility model is to provide one kind
The advantages of antioxidant consersion unit has and improves reaction rate, improves yield.
The utility model provides the following technical solution:
A kind of antioxidant consersion unit, including reaction kettle ontology, feeding cylinder, condensing mechanism, rabbling mechanism and microwave occur
Device assembly, the reaction kettle body outer wall are arranged with heater strip outside, and the heater strip is externally provided with insulating layer, the reaction kettle ontology
Top is equipped with first charging aperture and second charging aperture, and the feeding cylinder is equipped in the first charging aperture, is set on the feeding cylinder
There is valve, the condensing mechanism be movably equipped in the second charging aperture, is equipped with the rabbling mechanism in the reaction kettle ontology,
The reaction kettle body bottom portion is further fixed on the microwave generator component.
The reaction kettle body bottom portion is equipped with microwave generator component, and microwave has internal heating as a kind of new energy,
Quickly the advantages that heating, and the setting of the heater strip and the insulating layer can improve reaction temperature quickly, be greatly improved
Chemical reaction rate, the feeding cylinder can be such that raw material is slowly added into, and reaction is promoted to carry out, and the condensing mechanism can be such that raw material returns
Stream improves yield.
Preferably, the rabbling mechanism includes motor, agitating shaft and agitating paddle, and the agitating shaft is connected with the motor,
The agitating paddle is fixed on the agitating shaft, and the agitating shaft and the agitating paddle are respectively positioned in the reaction kettle ontology, institute
Motor is stated to be located above the reaction kettle ontology.
Preferably, the condensing mechanism includes condenser pipe and the cooling jacket outside the condenser pipe, the condenser pipe
Interior to be equipped with several baffles being staggered, the cooling jacket bottom is equipped with the cold water inlet pipe being connected with the cooling jacket,
The cold water outlet pipe being connected with the cooling jacket is equipped at the top of the cooling jacket.
Preferably, the reaction kettle body bottom portion is additionally provided with discharge port.
Preferably, several stabilizer blades are further fixed on the reaction kettle body bottom portion outer wall.
The beneficial effects of the utility model are: reaction kettle body bottom portion is equipped with microwave generator component, microwave is as a kind of
New energy has many advantages, such as internal heating, quickly heats, and the setting of heater strip and insulating layer can improve reaction temperature quickly
Degree, is greatly improved chemical reaction rate, and feeding cylinder can be such that raw material is slowly added into, and reaction is promoted to carry out, and condensing mechanism can make
Raw material reflux, improves yield.
Detailed description of the invention
Attached drawing is used to provide a further understanding of the present invention, and constitutes part of specification, practical with this
Novel embodiment is used to explain the utility model together, does not constitute limitations of the present invention.In the accompanying drawings:
Fig. 1 is the utility model structure diagram；
In the figure, it is marked as 1, reaction kettle ontology；11, heater strip；12, insulating layer；13, first charging aperture；14, the second charging
Mouthful；15, discharge port；16, stabilizer blade；2, feeding cylinder；21, valve；3, condensing mechanism；31, condenser pipe；311, baffle；32, cold water presss from both sides
Set；321, cold water inlet pipe；322, cold water outlet pipe；4, rabbling mechanism；41, motor；42, agitating shaft；43, agitating paddle；5, microwave is sent out
Raw device assembly.
Specific embodiment
Specific embodiment of the present utility model is described with reference to the accompanying drawing.
As shown in Figure 1, a kind of antioxidant consersion unit, including reaction kettle ontology 1, feeding cylinder 2, condensing mechanism 3, blender
Structure 4 and microwave generator component 5,1 outer wall of reaction kettle ontology are arranged with heater strip 11 outside, and heater strip 11 is externally provided with insulating layer 12,
It is equipped with first charging aperture 13 and second charging aperture 14 at the top of reaction kettle ontology 1, feeding cylinder 2, charging are equipped in first charging aperture 13
Cylinder 2 is equipped with valve 21, and condensing mechanism 3 is movably equipped in second charging aperture 14, is equipped with rabbling mechanism 4 in reaction kettle ontology 1, instead
1 bottom of kettle ontology is answered to be further fixed on microwave generator component 5, microwave generator component 5 is by isolated tube and microwave generator group
At microwave generator includes that microwave tube and microwave tube power supply two parts form, microwave tube power supply (abbreviation power supply or microwave source)
Effect is that common AC energy is become direct current energy, is created conditions for the work of microwave tube, 1 bottom of reaction kettle ontology is also set
There is discharge port 15, several stabilizer blades 16 are further fixed in 1 bottom outer wall of reaction kettle ontology.
Specifically, rabbling mechanism 4 includes motor 41, agitating shaft 42 and agitating paddle 43, agitating shaft 42 is connected with motor 41, stirs
It mixes paddle 43 to be fixed on agitating shaft 42, agitating shaft 42 and agitating paddle 43 are respectively positioned in reaction kettle ontology 1, and motor 41 is located at reaction kettle
1 top of ontology.
Specifically, condensing mechanism 3 includes condenser pipe 31 and the cooling jacket 32 outside condenser pipe 31, set in condenser pipe 31
There are several baffles 311 being staggered, 32 bottom of cooling jacket is equipped with the cold water inlet pipe 321 being connected with cooling jacket 32, cold
The cold water outlet pipe 322 being connected with cooling jacket 32 is equipped at the top of water leg 32.
Utility model works mode: putting in raw material from first charging aperture 13 and second charging aperture 14, rabbling mechanism 4 into
Row stirring, condensing mechanism 3 flow back, and feeding cylinder 2 is added slowly thereto a kind of raw material, and microwave generator component 5 works,
Product is released from discharge port 15 after reaction.
The above descriptions are merely preferred embodiments of the present invention, is not intended to limit the utility model, although ginseng
The utility model is described in detail according to previous embodiment, it for those skilled in the art, still can be with
It modifies the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features.It is all
Within the spirit and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in practical
Within novel protection scope.
Claims (5)
1. a kind of antioxidant consersion unit, which is characterized in that including reaction kettle ontology, feeding cylinder, condensing mechanism, rabbling mechanism and
Microwave generator component, the reaction kettle body outer wall are arranged with heater strip outside, and the heater strip is externally provided with insulating layer, described anti-
Answer kettle bodies top to be equipped with first charging aperture and second charging aperture, be equipped with the feeding cylinder in the first charging aperture, it is described into
Barrel is equipped with valve, and the condensing mechanism is movably equipped in the second charging aperture, is equipped in the reaction kettle ontology described
Rabbling mechanism, the reaction kettle body bottom portion are further fixed on the microwave generator component.
2. a kind of antioxidant consersion unit according to claim 1, which is characterized in that the rabbling mechanism include motor,
Agitating shaft and agitating paddle, the agitating shaft are connected with the motor, and the agitating paddle is fixed on the agitating shaft, the stirring
Axis and the agitating paddle are respectively positioned in the reaction kettle ontology, and the motor is located above the reaction kettle ontology.
3. a kind of antioxidant consersion unit according to claim 1, which is characterized in that the condensing mechanism includes condenser pipe
With the cooling jacket being located at outside the condenser pipe, the condenser pipe is interior to be equipped with several baffles being staggered, the cooling jacket
Bottom is equipped with the cold water inlet pipe being connected with the cooling jacket, is equipped at the top of the cooling jacket and is connected with the cooling jacket
Logical cold water outlet pipe.
4. a kind of antioxidant consersion unit according to claim 1, which is characterized in that the reaction kettle body bottom portion is also set
There is discharge port.
5. a kind of antioxidant consersion unit according to claim 1, which is characterized in that the reaction kettle body bottom portion outer wall
On be further fixed on several stabilizer blades.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820599312.2U CN208449299U (en) | 2018-04-25 | 2018-04-25 | A kind of antioxidant consersion unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820599312.2U CN208449299U (en) | 2018-04-25 | 2018-04-25 | A kind of antioxidant consersion unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208449299U true CN208449299U (en) | 2019-02-01 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820599312.2U Active CN208449299U (en) | 2018-04-25 | 2018-04-25 | A kind of antioxidant consersion unit |
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| Country | Link |
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| CN (1) | CN208449299U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112516935A (en) * | 2020-12-16 | 2021-03-19 | 江苏长青农化股份有限公司 | Preparation method of fomesafen |
-
2018
- 2018-04-25 CN CN201820599312.2U patent/CN208449299U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112516935A (en) * | 2020-12-16 | 2021-03-19 | 江苏长青农化股份有限公司 | Preparation method of fomesafen |
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| Date | Code | Title | Description |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: No. 68, Hongyan Road, salt chemical industry development zone, Hongze County, Huai'an City, Jiangsu Province, 223000 Patentee after: Jiangsu Bade Polyurethane Co.,Ltd. Country or region after: China Address before: No. 68, Hongyan Road, salt chemical industry development zone, Hongze County, Huai'an City, Jiangsu Province, 223000 Patentee before: HUAIAN BUD POLYURETHANE SCIENCE & TECHNOLOGY Co.,Ltd. Country or region before: China |