CN208390021U - A kind of catalytic degradation synthesizes the reaction generation tank of medicinal sulphadiazine - Google Patents
A kind of catalytic degradation synthesizes the reaction generation tank of medicinal sulphadiazine Download PDFInfo
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- CN208390021U CN208390021U CN201820783851.1U CN201820783851U CN208390021U CN 208390021 U CN208390021 U CN 208390021U CN 201820783851 U CN201820783851 U CN 201820783851U CN 208390021 U CN208390021 U CN 208390021U
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- Prior art keywords
- tank body
- fixedly connected
- top cover
- cover
- sulphadiazine
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Abstract
The utility model discloses the reaction generation tanks that a kind of catalytic degradation synthesizes medicinal sulphadiazine, including tank body, top cover is installed at the top of the tank body, the bottom of the tank body is equipped with bottom cover, rabbling mechanism is installed in the tank body, the rabbling mechanism includes stirring motor, the stirring motor is mounted on the top of top cover, the output shaft of the stirring motor and the middle part of top cover are rotatablely installed, the output shaft of the stirring motor is also fixedly connected with agitating shaft, the bottom of the agitating shaft is extended at bottom cover by the endoceliac middle part of tank, agitating plate is fixedly connected on the agitating shaft, side on the top cover at the top of it is fixedly connected with first charging aperture, the other side on the top cover at the top of it is fixedly connected with second charging aperture.The utility model effectively stirs mixed liquor when water sample is prepared, improves the degradation rate of SDZ, the effect used is preferable by the cooperation of above-mentioned dependency structure.
Description
Technical field
The utility model relates to sulphadiazines to degrade with reaction generating device technical field, specially a kind of catalytic degradation conjunction
The reaction generation tank of patent medicine sulphadiazine.
Background technique
Antibiotic plays positive effect in human health and Animal husbandry production, but is not completely absorbed and Li Tong
Antibiotic or other metabolins the approach such as will drain by urine, excrement and enter water body, ecological security to water environment and
Human health constitutes a threat to, and thus, traces of antibiotic appearance in the environment and its potential hazard cause more and more passes
Note.To using the photocatalytic oxidation degradation behavior of relatively broad broad spectrum antimicrobial agent sulphadiazine (SDZ) in water to study,
Inquire into illumination, Ti0 in reaction process2The factors pair such as dosage, the reaction starting initial mass concentration of PH, SDZ, reaction time
The influence of SDZ degradation efficiency.Experiment content include water sample prepare, observation the parts such as phenomenon and experimental summary, water sample prepare when
It waits, the SDZ and then addition sodium hydroxide for first weighing constant weight are transferred to be mixed equal in certain density SDZ mother liquor after dissolving
A certain amount of Ti0 is added after even2, pH value is adjusted, and then be stirred, aeration after liquid mixing sufficiently to be mixed, Mei Geyi
Section time sampling, for sample after 0.45 micron of filtering with microporous membrane, HPLC surveys its peak area, is calculated according to the reduction of peak area
Its degradation rate needs to be stirred mixed liquor when water sample is prepared, and traditional agitating mode generallys use stirring
Stick is stirred mixed liquor, increases labor intensity, and efficiency is not also high, the effect used is bad.
Utility model content
The purpose of this utility model is to provide the reaction generation tanks that a kind of catalytic degradation synthesizes medicinal sulphadiazine, have
Simple, the easy to use advantage of structure solves the problems, such as that traditional product stirring is inconvenient.
To achieve the above object, the utility model provides the following technical solutions: a kind of medicinal sulfanilamide (SN) of catalytic degradation synthesis is phonetic
The reaction generation tank of pyridine, including tank body are equipped with top cover at the top of the tank body, and the bottom of the tank body is equipped with bottom cover, institute
It states and rabbling mechanism is installed in tank body.
The rabbling mechanism includes stirring motor, and the stirring motor is mounted on the top of top cover, the stirring motor
The rotational installation of the middle part of output shaft and top cover, the output shaft of the stirring motor are also fixedly connected with agitating shaft, the agitating shaft
Bottom extended at bottom cover by the endoceliac middle part of tank, agitating plate is fixedly connected on the agitating shaft, on the top cover
Side at the top of it is fixedly connected with first charging aperture, and the other side on the top cover at the top of it is fixedly connected with the
Two feed inlets, the bottom of the bottom cover are fixedly connected with discharge port, and the surface of the bottom cover is fixedly connected with supporting leg.
Preferably, the tank body, top cover and bottom cover are transparent light-transmitting materials.
Preferably, the top cover is detachably installed with tank body and bottom cover with tank body.
Preferably, the quantity of the agitating plate is no less than five, each agitating plate along the outer surface of agitating shaft on to
Under be sequentially arranged at intervals.
Preferably, the quantity of the supporting leg is three, annular centered on three supporting legs center of circle of circle where bottom cover bottom surface
Array.
Compared with prior art, the utility model has the beneficial effects that the utility model by stirring motor, agitating shaft with
The mixed liquor being mainly made of SDZ is effectively stirred in the cooperation of agitating plate, is uniformly mixed mixed liquor, accelerates SDZ's
Degradation, is finally sampled by discharge port, calculates the degradation rate of SDZ, the effect used is preferable.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model tank body front view；
Fig. 2 is the structural schematic diagram of the partial sectional view of the utility model tank body front view；
Fig. 3 is the structural schematic diagram of the partial sectional view of the utility model discharge port front view.
In figure: 1- tank body, 2- top cover, 3- bottom cover, 4- rabbling mechanism, 5- stirring motor, 6- agitating shaft, 7- agitating plate, 8-
First charging aperture, 9- second charging aperture, 10- discharge port, 11- supporting leg.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Please refer to Fig.1 to Fig.3, the utility model provides a kind of technical solution: a kind of medicinal sulfanilamide (SN) of catalytic degradation synthesis is phonetic
The reaction generation tank of pyridine, including tank body 1, the top of tank body 1 are equipped with top cover 2, and the bottom of tank body 1 is equipped with bottom cover 3, tank body 1,
Top cover 2 and bottom cover 3 are transparent light-transmitting materials, and illumination can also influence the degradation rate of sulphadiazine, and transparent light-transmitting materials can be square
Just light transmits, and top cover 2 and tank body 1 and bottom cover 3 are detachably installed with tank body 1, and top cover 2 and bottom cover 3 pass through screw and tank
Body 1 is installed, convenient to dismount in the future, and rabbling mechanism 4 is equipped in tank body 1.
Rabbling mechanism 4 includes stirring motor 5, and the device model that stirring motor 5 uses is YDS slowspeed machine, by external electrical
Source power supply, stirring motor 5 are mounted on the top of top cover 2, and the output shaft of stirring motor 5 and the middle part of top cover 2 are rotatablely installed, stirring
The output shaft of motor 5 is also fixedly connected with agitating shaft 6, and the bottom of agitating shaft 6 extends to bottom cover 3 by the intracavitary middle part of tank body 1
Locate, is fixedly connected with agitating plate 7 on agitating shaft 6, by agitating plate 7, mixed liquor is stirred, the quantity of agitating plate 7 is many
In five, each agitating plate 7 is sequentially arranged at intervals along the outer surface of agitating shaft 6 from top to bottom, multiple by being arranged, to tank body
The mixed liquor of different levels is stirred in 1, stirs mixed liquor more abundant, and the side on top cover 2 at the top of it is fixed
It is connected with first charging aperture 8, the other side on top cover 2 at the top of it is fixedly connected with second charging aperture 9, the bottom of bottom cover 3
It is fixedly connected with discharge port 10, the surface of bottom cover 3 is fixedly connected with supporting leg 11, and the quantity of supporting leg 11 is three, three supporting legs 11
Using the center of circle of circle where 3 bottom surface of bottom cover as center annular array.
Working principle: the catalytic degradation synthesizes the reaction generation tank of medicinal sulphadiazine in use, preparing first in water sample
When, it first weighs then the sodium hydroxide dissolution of 0.01mol/L is added in 12.5mgSDZ after and is transferred in 250ml volumetric flask and matches
It is made in the SDZ mother liquor of 50mg/L and is poured into tank body 1 together again, a certain amount of Ti0 is secondly added2, pH value is adjusted, is then stirred
Mixing motor 5 drives agitating plate 7 to be stirred mixed liquor, aeration after liquid to be mixed mixing sufficiently, first charging aperture 8 and second into
Material mouth 9, which is arranged to Flange-shaped Parts, can facilitate external ventilating mechanisms, convenient for the aeration of mixed liquor, finally sample at regular intervals, with
A sample is taken subject to 12min, sample surveys its peak area after 0.45 micron of filtering with microporous membrane, through HPLC, according to peak face
Long-pending reduction calculates its degradation rate, it is worth mentioning at this point that the parameters such as weight, concentration here are not fixed, can be according to practical application
It is selected in the process, by the cooperation of above structure, the mixed liquor being mainly made of SDZ is effectively stirred, makes to mix
It closes liquid to be uniformly mixed, accelerates the degradation of SDZ, be finally sampled by discharge port 10, the effect used is preferable.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (5)
1. a kind of catalytic degradation synthesizes the reaction generation tank of medicinal sulphadiazine, including tank body (1), the top of the tank body (1)
It is equipped with top cover (2), the bottom of the tank body (1) is equipped with bottom cover (3), it is characterised in that: be equipped with and stir in the tank body (1)
Mix mechanism (4)；
The rabbling mechanism (4) includes stirring motor (5), and the stirring motor (5) is mounted on the top of top cover (2), described to stir
The middle part of the output shaft and top cover (2) of mixing motor (5) is rotatablely installed, and the output shaft of the stirring motor (5) is also fixedly connected with
The bottom of agitating shaft (6), the agitating shaft (6) is extended at bottom cover (3) by the intracavitary middle part of tank body (1), the agitating shaft
(6) it is fixedly connected on agitating plate (7), the side on the top cover (2) at the top of it is fixedly connected with first charging aperture
(8), the other side on the top cover (2) at the top of it is fixedly connected with second charging aperture (9), the bottom of the bottom cover (3)
It is fixedly connected with discharge port (10), the surface of the bottom cover (3) is fixedly connected with supporting leg (11).
2. the reaction generation tank that a kind of catalytic degradation according to claim 1 synthesizes medicinal sulphadiazine, it is characterised in that:
The tank body (1), top cover (2) and bottom cover (3) are transparent light-transmitting materials.
3. the reaction generation tank that a kind of catalytic degradation according to claim 1 synthesizes medicinal sulphadiazine, it is characterised in that:
The top cover (2) and tank body (1) and bottom cover (3) and tank body (1) detachable installation.
4. the reaction generation tank that a kind of catalytic degradation according to claim 1 synthesizes medicinal sulphadiazine, it is characterised in that:
The quantity of the agitating plate (7) is no less than five, each agitating plate (7) along the outer surface of agitating shaft (6) from top to bottom successively
It is alternatively arranged.
5. the reaction generation tank that a kind of catalytic degradation according to claim 1 synthesizes medicinal sulphadiazine, it is characterised in that:
The quantity of the supporting leg (11) is three, and three supporting legs (11) are using the center of circle of circle where bottom cover (3) bottom surface as center annular array.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820783851.1U CN208390021U (en) | 2018-05-24 | 2018-05-24 | A kind of catalytic degradation synthesizes the reaction generation tank of medicinal sulphadiazine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820783851.1U CN208390021U (en) | 2018-05-24 | 2018-05-24 | A kind of catalytic degradation synthesizes the reaction generation tank of medicinal sulphadiazine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208390021U true CN208390021U (en) | 2019-01-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820783851.1U Expired - Fee Related CN208390021U (en) | 2018-05-24 | 2018-05-24 | A kind of catalytic degradation synthesizes the reaction generation tank of medicinal sulphadiazine |
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| CN (1) | CN208390021U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113351132A (en) * | 2021-05-13 | 2021-09-07 | 西北矿冶研究院 | Device for correspondingly degrading ziram through photo-magnetic cooperation and use method |
-
2018
- 2018-05-24 CN CN201820783851.1U patent/CN208390021U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113351132A (en) * | 2021-05-13 | 2021-09-07 | 西北矿冶研究院 | Device for correspondingly degrading ziram through photo-magnetic cooperation and use method |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190118 Termination date: 20200524 |
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| CF01 | Termination of patent right due to non-payment of annual fee |