CN208171674U - A kind of fluid sampling device under inert atmosphere protection - Google Patents

A kind of fluid sampling device under inert atmosphere protection Download PDF

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Publication number
CN208171674U
CN208171674U CN201820700805.0U CN201820700805U CN208171674U CN 208171674 U CN208171674 U CN 208171674U CN 201820700805 U CN201820700805 U CN 201820700805U CN 208171674 U CN208171674 U CN 208171674U
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China
Prior art keywords
sampling
inert atmosphere
way pipe
dottle pin
atmosphere protection
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CN201820700805.0U
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Chinese (zh)
Inventor
张立春
胡云霞
牟善文
刘廷亮
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SHANDONG AUSTRALIA RUN CHEMICAL TECHNOLOGY Co Ltd
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SHANDONG AUSTRALIA RUN CHEMICAL TECHNOLOGY Co Ltd
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Priority to CN201820700805.0U priority Critical patent/CN208171674U/en
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Abstract

The utility model discloses the fluid sampling device under a kind of inert atmosphere protection, is made of sampler, four-way pipe, valve, sealing dottle pin, sampler one end is connected by pipeline with sample tap, and valve is arranged on pipeline;The sampler other end is connect with four-way pipe axial passageway, and junction sets the first sealing dottle pin;Four-way pipe axial passageway top setting sampling cap and the second sealing dottle pin, sampling cap centre are equipped with hole;The external inert atmosphere protection device of the radial line of four-way pipe, junction set third sealing dottle pin.Utility model device structure is simple, samples quick and safe and easy to carry;Device good seal performance is not wasted without leakage in sampling process;Device liquid sample can be stored temporarily, guarantee sample trackability, selective examination, check convenient for sample, the analysis detection link especially suitable for the flammable and combustible liquids in production and use process.

Description

A kind of fluid sampling device under inert atmosphere protection
Technical field
The utility model relates to chemical plants, and in particular to the fluid sampling device under a kind of inert atmosphere protection.
Background technique
Very extensive to the sample detection of liquid during modern production, the suitable material that samples is to detection work It goes on smoothly highly beneficial.Currently, being to be in sampling even tee tube, a port for the sample mode of inflammable and explosive fried liquid Inert gas shielding branch, a related glass sampling bottle for having branch pipe of the pressure-resistant emulsion tube of port.Alkyl aluminum, alkylaluminoxane Very sensitive to air and moisture, the operation for being related to such product has been required to inert gas (N2, Ar) protection.This method behaviour Make cumbersome, connecting portion is more, increases risk of leakage, and risk is larger in sampling process.Therefore, a kind of both corrosion resistants are designed and produced The sampling instrument lose, be hardly damaged, is highly-safe, being convenient for carrying carries out periodic analysis for product in production process or intermediate product Detection is crucial quality control and the adjustment of technique.
Utility model content
In view of the above-mentioned problems, the utility model provides the liquid sampling dress under the inert atmosphere protection of safe and convenient a kind of It sets.
To achieve the above object, the technical solution adopted in the utility model is:A kind of liquid under inert atmosphere protection takes Sampling device is made of sampler, four-way pipe, valve, sealing dottle pin, and sampler one end is connected by pipeline with sample tap, pipeline Upper setting valve;The sampler other end is connect with four-way pipe axial passageway, and junction sets the first sealing dottle pin;Four-way pipe is axially logical Road top setting sampling cap and the second sealing dottle pin, sampling cap centre are equipped with hole;The external inert atmosphere of the radial line of four-way pipe Protective device, junction set third sealing dottle pin.The external inert atmosphere protection device of four-way pipe, facilitates and fills to the inside of four-way pipe Inert gas improves safety when sampling;Sealing dottle pin facilitates the taking-up of liquid after sampling convenient for penetrating.
Graduation mark is provided on the lateral wall of sampler.Graduation mark, which facilitates, records taken liquid capacity when sampling, and passes through quarter Spend the sampling of the different sampling specifications of progress of the line property of can choose.
Valve connects sampling head, and sampling head is in section cone, and upward, section is conical for the portlet of section cone Portlet connecting valve.Sampling head in section cone, upper port diameter be less than lower port diameter, facilitate heterogeneity liquid into Sample keeps sampling more accurate.
It samples cap and is located at the second sealing dottle pin top.
First sealing dottle pin, second sealing dottle pin and third sealing dottle pin use with can puncture anti-corrosive rubber material Matter.
Operating procedure when fluid sampling device under inert atmosphere protection samples:
The air-tight test of sampler:First sampler is external on the pipeline of inert atmosphere protection device, is filled with inertia Gas checking air-tightness.
The displacement and charging of sampler:Sampler to be pumped into negative pressure, opens valve, liquid material flows directly into sampler, With inert gas purge sample tap to material remaining between valve, valve is closed, sampling terminates.
Liquid sampling:Four-way pipe radial line is passed through inert gas, by the sampled cap of the syringe needle of sampling probe along four-way pipe axis It is inserted into sampler to pipeline, extracts quantitative liquid sample;Syringe needle, which retracts, after sampling enters in four-way pipe radial line, then is pumped into one Quantitative inert gas makes syringe needle form gas embolism, syringe needle is fully drawn out and completes sampling process.
Compared with prior art, the utility model is had the advantages that:
Apparatus structure is simple, samples quick and safe and easy to carry;Device good seal performance, without leakage in sampling process, It does not waste;Device liquid sample can be stored temporarily, guarantee sample trackability, selective examination, check convenient for sample, especially suitable in life The analysis detection link of flammable and combustible liquids in production and use process.
Detailed description of the invention
A kind of fluid sampling device structural schematic diagram under Fig. 1, inert atmosphere protection;
A kind of fluid sampling device sampling process flow chart under Fig. 2, inert atmosphere protection;
Wherein, 1, sampler, 2, four-way pipe, 3, valve, the 4, first sealing dottle pin, 5, sampling cap, the 6, second sealing dottle pin, 7, third seals dottle pin.
Specific embodiment
The utility model is described further combined with specific embodiments below.
Embodiment 1
By taking the sampling of trimethyl aluminium liquid as an example, the use process of the utility model is described in detail in conjunction with Fig. 1 and 2.
The sampling process of the present embodiment is as shown in Figure 2:
The air-tight test of sampler 1:First sampler 1 is external on the pipeline of inert atmosphere protection device, is filled with lazy Property gas checking air-tightness, pressure does not decline in 5 minutes in pipeline, then air-tight test is qualified.
The displacement and charging of sampler 1:Sampler 1 is pumped into negative pressure, opens valve 3, liquid material flows directly into sampling Device 1 closes valve with inert gas purge sample tap to material remaining between valve, and sampling terminates.
Liquid sampling:2 radial line of four-way pipe is passed through inert gas, by the sampled cap 5 of the syringe needle of sampling probe along four-way pipe 2 Axial duct is inserted into sampler 1, extracts quantitative liquid sample;Syringe needle, which retracts, after sampling enters in 2 radial line of four-way pipe, then takes out Enter a certain amount of inert gas, so that syringe needle is formed gas embolism, syringe needle is fully drawn out and completes sampling process.
Further, four-way pipe 2 described in the present embodiment uses stainless steel material.
Further, valve 3 described in the present embodiment is the needle valve of controllable flow rate.
Further, internal screw thread is arranged in the lower end inner wall of the axial duct of four-way pipe 2 described in the present embodiment, with four-way pipe The external screw thread being meshed with four-way pipe inner thread, the first sealing of junction setting is arranged in the pipeline outer wall of the sampler 1 of 2 connections Dottle pin 4.
Further, external screw thread is arranged in the upper end outer wall of the axial duct of four-way pipe 1 described in the present embodiment, samples cap 5 The internal screw thread being meshed therewith, junction setting the second sealing dottle pin 6 is arranged in inner wall.
The present embodiment apparatus structure is simple, samples quick and safe and easy to carry;Device good seal performance, in sampling process Without leakage, do not waste;Device liquid sample can be stored temporarily, guarantee sample trackability, selective examination, check convenient for sample.

Claims (4)

1. the fluid sampling device under a kind of inert atmosphere protection, it is characterised in that:Liquid sampling dress under inert atmosphere protection It sets and is made of sampler (1), four-way pipe (2), valve (3), sealing dottle pin, sampler (1) one end passes through pipeline and sample tap phase Even, valve (3) are set on pipeline;Sampler (1) other end is connect with four-way pipe (2) axial passageway, and junction sets the first sealing Dottle pin (4);Four-way pipe (2) axial passageway top setting sampling cap (5) and the second sealing dottle pin (6), sampling cap (5) is intermediate to be equipped with Hole;The external inert atmosphere protection device of the radial line of four-way pipe (2), junction set third sealing dottle pin (7).
2. the fluid sampling device under a kind of inert atmosphere protection according to claim 1, it is characterised in that:Described takes Graduation mark is provided on the lateral wall of sample device (1).
3. the fluid sampling device under a kind of inert atmosphere protection according to claim 1, it is characterised in that:The valve Door (3) connect sampling head, sampling head in section cone, the portlet of section cone upward, the portlet of section cone Connecting valve (3).
4. the fluid sampling device under a kind of inert atmosphere protection according to claim 1, it is characterised in that:Described takes Sample cap (5) is located at second sealing dottle pin (6) top.
CN201820700805.0U 2018-05-11 2018-05-11 A kind of fluid sampling device under inert atmosphere protection Active CN208171674U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820700805.0U CN208171674U (en) 2018-05-11 2018-05-11 A kind of fluid sampling device under inert atmosphere protection

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820700805.0U CN208171674U (en) 2018-05-11 2018-05-11 A kind of fluid sampling device under inert atmosphere protection

Publications (1)

Publication Number Publication Date
CN208171674U true CN208171674U (en) 2018-11-30

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110484959A (en) * 2019-09-11 2019-11-22 东阳市艾克思科技有限公司 A kind of protective atmosphere ionic liquid coating apparatus liquid transfer device
CN114062040A (en) * 2021-11-10 2022-02-18 惠州市绿色能源与新材料研究院 Liquid storage and quantitative sampling device and method and application thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110484959A (en) * 2019-09-11 2019-11-22 东阳市艾克思科技有限公司 A kind of protective atmosphere ionic liquid coating apparatus liquid transfer device
CN110484959B (en) * 2019-09-11 2024-05-10 东阳市艾克思科技有限公司 Protective atmosphere ionic liquid plating equipment liquid transfer device
CN114062040A (en) * 2021-11-10 2022-02-18 惠州市绿色能源与新材料研究院 Liquid storage and quantitative sampling device and method and application thereof
CN114062040B (en) * 2021-11-10 2024-06-04 惠州市绿色能源与新材料研究院 Liquid storage and quantitative sampling device, method and application thereof

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