CN208076339U - A kind of experiment circuit device of waxy crude oil wax deposit test - Google Patents

A kind of experiment circuit device of waxy crude oil wax deposit test Download PDF

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Publication number
CN208076339U
CN208076339U CN201820416138.3U CN201820416138U CN208076339U CN 208076339 U CN208076339 U CN 208076339U CN 201820416138 U CN201820416138 U CN 201820416138U CN 208076339 U CN208076339 U CN 208076339U
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China
Prior art keywords
wax deposit
crude oil
water
bath
waxy crude
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Expired - Fee Related
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CN201820416138.3U
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Chinese (zh)
Inventor
张旭鑫
陈湘
王楠
杨佳欣
杨梓颜
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China University of Petroleum East China
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China University of Petroleum East China
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Abstract

The utility model discloses a kind of waxy crude oil wax deposit test experiment circuit device, it can be achieved that waxy crude oil and water-oil emulsion the wax deposit characteristic under pipe flow condition test.Three pipelines in parallel are respectively set in test section and reference section, and caliber is different, can study affecting laws of the caliber to waxy crude oil wax deposit.Valve is arranged in the pipe ends of test section and reference section, and detachable experimental channel weighing measurement wax deposit keeps experimental result more accurate, while can directly observe wax deposit state.Sampling valve is arranged in circuit end, can obtain tube fluid in real time.Compared with existing wax deposit measuring device, the utility model have the characteristics that can to carry out the experiment of multi-pipe-diameter wax deposit, the visualization of wax deposit form, result it is accurate it is reliable, on-line period, functional, degree of variation are high, flow is simple, flexible and convenient operation.

Description

A kind of experiment circuit device of waxy crude oil wax deposit test
Technical field
The utility model belongs to the technical field of waxy crude oil physical characteristic, more particularly to a kind of waxy crude oil wax deposit The experiment circuit device of test.
Background technology
Pipeline transportation is the most important means of transportation of crude oil, there is that throughput rate is big, low energy consumption, fed distance is long.From pipe The angle of road conveying can substantially be divided into crude oil low low viscous crude oil, gelatinous crude oil, the height of coagulating of lightweight by flow behavior and glue heavy original Oil.The condensation point of gelatinous crude oil is higher, generally higher related with its wax content.Wax mass fraction is usually less than to 2.5% crude oil Referred to as low wax crude oil, 2.5%~10% referred to as waxy crude oil are known as high-wax oil higher than 10%.The crude oil of domestic product In the majority with easily solidifying high glutinous waxy crude oil, waxy crude oil generally has the characteristics such as condensation point is high, viscosity is big, mobility is poor, in conveying work The method that heating is typically chosen in skill improves its mobility, and often in the presence of conveying cost, higher, throughput rate changes such conveying technique The problem that area requirement is higher, stopped flow injection analysis is more difficult.During wax-containing oil pipe heated transportation, oil temperature is gradually reduced, Wax crystalline substance solubility is gradually reduced, wax after oil temperature is down to wax precipitation point in crude oil start crystallization be precipitated, often can on the inside of tube wall shape At wax deposit layer, to reduce pipeline flow section, increase pipe friction, reduction conveying capacity, for the safe transport band of pipeline Carry out hidden danger.Wax crystallization is reduced with constant temperature, finally mutually is connected to form reticular structure, seriously affects crude oil fluidity, even Pipeline is caused to arrhea accident.The measure for reducing security risk in engineering is generally regular pigging.Therefore, the wax of waxy crude oil is studied Deposition characteristics are particularly important the determination of period of removing the wax.
For the wax deposit characteristic of research waxy crude oil in the duct, Huang opens jade and proposes a kind of wax deposit experiment circuit device (Huang Qiyu, Zhang Jingjun, Gao Xuefeng wait Study on wax deposition of Daqing crude oil [J] petroleum journals, 2006,27 (4):125- 129.).It is based on surveying to circuit, mass flowmenter metered flow is tested using the crude oil in peristaltic pump or screw pump driving oil tank The pressure drop of examination section and reference section can obtain wax deposit thickness.There are main problems to be for it, and wax deposit thickness, knot are calculated merely with pressure drop Fruit error is larger, and can not directly observe wax deposit state.One group of test section and reference section is only arranged in experiment circuit, can not study Under the conditions of different tube diameters, changing rule of the waxy crude oil in Guan Liuzhong wax deposits.The experimental provision flow is complicated, and equipment is superfluous It is remaining, it is unfavorable for experimental implementation.
Invention content
In order to overcome the deficiencies of existing technologies, the purpose of this utility model is to provide a kind of test of waxy crude oil wax deposit Test circuit device.
The utility model can realize the test of the wax deposit characteristic under pipe flow condition to waxy crude oil and water-oil emulsion.Oil Electric mixing device is set in tank can prepare crude oil or water-oil emulsion, be driven using peristaltic pump in the fluid to circuit in oil tank, Mass flowmenter metered flow, two differential pressure pick-ups measure the pressure drop data of test section and reference section.Test section and reference section Three pipelines in parallel are respectively set, caliber is different, can study affecting laws of the caliber to waxy crude oil wax deposit.Test Valve is arranged in the pipe ends of section and reference section, and detachable experimental channel weighing measurement wax deposit keeps experimental result more accurate, It can directly observe wax deposit state simultaneously.Sampling valve is arranged in circuit end, can obtain tube fluid in real time.
The specific technical solution of the utility model is as follows:
A kind of experiment circuit device of waxy crude oil wax deposit test, including two parts of sample system and circuit system; The sample system includes the first water-bath, oil tank and blowdown valve;First water-bath is connected with the outer layer chuck of oil tank, can control Oil tank temperature;The blowdown valve is located at tank bottom, can discharge pot liquid;The circuit system includes mainly peristaltic pump, matter Amount flowmeter, test pipeline section, the first differential pressure pick-up, third water-bath, reference pipeline section, the second differential pressure pick-up, takes the second water-bath Sample valve and connecting line.The peristaltic pump and oil tank can provide power for system;The measurable fluid stream of mass flowmenter Amount;The both ends of the first differential pressure pick-up connecting test pipeline section, test pipeline section are positioned in the second water-bath, the first differential pressure sensing Device can measure the pressure drop of test pipeline section, the temperature of the second water-bath controllable testing pipeline section;The second differential pressure pick-up connection ginseng Than the both ends of pipeline section, reference pipeline section is positioned in third water-bath, and the second differential pressure pick-up can measure the pressure drop of reference pipeline section, third Water-bath can control the temperature of reference pipeline section;The sampling valve is placed in circuit end, can obtain fluid sample in real time.
The oil tank top is equipped with electric mixer, for stirring grease system, accelerates oil mixing with water speed.
The oil tank is equipped with outer layer chuck, and circulator bath is for controlling experimental temperature in tank.
The oil tank inlet and exit setting are across pipeline, it can be achieved that the more sealing and circulating flow of tank.
The test pipeline section is equipped with three pipelines in parallel, and the caliber of three pipelines is different, and every pipeline both ends setting Two ball valves, can dismantle pipeline.
The reference pipeline section is equipped with three pipelines in parallel, and the caliber of three pipelines is different, and every pipeline both ends setting Two ball valves, can dismantle pipeline.
If dry temperature sensor, pressure sensor are equipped with along the circuit, for acquiring circuit fluid flow parameters.
Compared with prior art, the present invention has the advantages that:
(1) device can carry out the wax deposit pipe flow experiment of waxy crude oil, water-oil emulsion.
(2) differential pressure calculating and two methods of weighing is used to measure wax deposit amount, experimental result is more accurate reliable.
(3) pipeline of three different tube diameters in parallel is set, affecting laws of the caliber to waxy crude oil wax deposit can be studied.
(4) circuit setting more tank pipeline is, it can be achieved that more tank sealing and circulating flowing.
(5) it uses peristaltic pump to drive fluid, can effectively avoid failure by shear of the pump to fluid.
(6) circuit end is equipped with sampling valve, can obtain the sample of fluid in real time.
Description of the drawings
Fig. 1 is the utility model overall structure diagram.
In figure:The first water-baths of 1-;2- oil tanks;3- blowdown valves;4- ball valves one;5- peristaltic pumps;6- mass flowmenters;7- second Water-bath;8- ball valves two;9- ball valves three;10- ball valves four;11- ball valves five;12- ball valves six;13- ball valves seven;The first differential pressures of 14- pass Sensor;15- ball valves eight;16- ball valves nine;17- ball valves ten;18- ball valves 11;19- ball valves 12;20- ball valves 13;21- Two differential pressure pick-ups;22- third water-baths;23- sampling valves;24- ball valves 14;25- ball valves 15.
Specific implementation mode
The utility model is described in detail below in conjunction with the accompanying drawings and by specific embodiment.It is specific the following content is combining Preferred embodiment further detailed description of the utility model is, and it cannot be said that be the specific implementation of the utility model It is confined to these explanations.For those of ordinary skill in the art, without departing from the concept of the premise utility, also Several simple deductions or replacement can be made, the scope of protection of the utility model is all shall be regarded as belonging to.
As shown in Figure 1, the utility model includes two parts of sample system and circuit system.
Wherein the sample system includes the first water-bath 1, oil tank 2, blowdown valve 3 and connection pipeline therein.Described One water-bath 1 is connected with the outer layer chuck of oil tank 2, controls temperature in tank.Electric mixer is arranged in 2 top of the oil tank, can be to tank Interior liquid is stirred, and lower part is equipped with blowdown valve 3, can discharge pot liquid.
The circuit system includes ball valve 1, peristaltic pump 5, mass flowmenter 6, the second water-bath 7, ball valve 28, ball valve three 9, ball valve 4 10, ball valve 5 11, ball valve 6 12, ball valve 7 13, the first differential pressure pick-up 14, ball valve 8 15, ball valve 9 16, ball valve 10, ball valve 11, ball valve 12, ball valve 13, the second differential pressure pick-up 21, third water-bath 22, sampling valve 23, ball Valve 14, ball valve 15.The peristaltic pump 5 is connected by ball valve 1 with the lower part of oil tank 2, for driving fluid to flow. The mass flowmenter 6 is connected with the outlet of peristaltic pump 5, for measuring fluid flow.The outlet of the mass flowmenter 6 is divided into The different parallel pipeline of three calibers is connected with ball valve 28, ball valve 39, ball valve 4 10 respectively.The ball valve 5 11, ball valve six 12, one end of ball valve 7 13 is connected with ball valve 28, ball valve 39, ball valve 4 10 respectively by one section of pipeline, and the other end is collected to One pipeline.The ball valve 28, ball valve 39, ball valve 4 10, ball valve 5 11, ball valve 6 12, ball valve 7 13 and pipe therein Road together constitutes test section.The both ends of first differential pressure pick-up 14 are respectively connected to the both ends of test section, can measure fluid In the pressure drop data of test section.It is corresponding with test section caliber that the test section by the circuit of one section of arc is divided into three calibers Parallel pipeline is connected with ball valve 8 15, ball valve 9 16, ball valve 10 respectively.The ball valve 8 15, ball valve 9 16, ball valve 10 One end be connected respectively with ball valve 11, ball valve 12, ball valve 13 by one section of pipeline, the other end is collected to one Pipeline.The ball valve 8 15, ball valve 9 16, ball valve 10, ball valve 11, ball valve 12, ball valve 13 and wherein Pipeline together constitute reference section.The both ends of second differential pressure pick-up 21 are respectively connected to the both ends of reference section, can measure Pressure drop data of the fluid in reference section.The reference section by being divided into two pipelines in parallel after one section of pipeline, respectively with ball valve 14, ball valve 15 is connected.The ball valve 15 is connected with 2 top of oil tank.The ball valve 14 enters with peristaltic pump 5 It is connected at mouthful.The sampling valve 23 is located at reference section rear portion, and the end of circuit can obtain fluid sample in real time.Cloth along circuit Pressure sensor and four temperature sensors there are four setting, wherein P1、T1After mass flowmenter 6, P2、T2Positioned at test Section rear portion, P3、T3Positioned at reference section front, P4、T4Positioned at sampling valve front.
The utility model specific operation process is described as follows:
The preparation of water-oil emulsion:The first water-bath 1 will be opened to oil in a certain amount of crude oil and water injection oil tank 2,2 into Row heating, the electric mixing device for opening 2 top of oil tank are stirred grease, and stirring after a certain period of time, completes grease emulsus The preparation of liquid.
Waxy crude oil wax deposit circuit is tested:Close ball valve 14, ball valve 39, ball valve 4 10, ball valve 6 12, ball valve 7 13, ball valve 8 15, ball valve 9 16, ball valve 11, ball valve 12 open ball valve 1, ball valve 28, ball valve 5 11, ball Valve 10, ball valve 13, ball valve 15 start peristaltic pump 5 and drive crude oil/water-oil emulsion in oil tank 2 to circuit It is interior, immediate boiling flow.After flowing is stablized, ball valve 14 is opened, closes ball valve 1, ball valve 15, flow, which is converted to, closes Formula flow.Open the second water-bath 7 and third water-bath 22, set temperature to experimental temperature, sensor acquires fluid stream along circuit Dynamic data, can get fluid sample by sampling valve 23.After data acquisition, peristaltic pump 5 is closed, by ball valve 28 and ball valve Pipeline dismounting among 5 11 is weighed, and the quality of wax deposit, while the form of observable wax deposit are obtained.
To sum up, wax deposit experimental apparatus for testing can complete what waxy crude oil or water-oil emulsion were tested in Guan Liuzhong wax deposits Circuit is tested.Water-oil emulsion can be prepared using self- poking arrangement, peristaltic pump drives fluid.The parallel transistor of three different tube diameters Road can study affecting laws of the caliber to wax deposit, observe wax deposit form using dismountable pipeline, measure its quality, in conjunction with Pressure decline method can determine wax deposit amount, as a result more accurate reliable.Circuit is equipped with sampler, can obtain Guan Liuzhong fluids in real time Sample.Therefore, device, which has, can carry out the experiment of multi-pipe-diameter wax deposit, wax deposit form visualizes, result is accurate reliably, take online The features such as sample, functional, degree of variation are high, flow is simple, flexible and convenient operation.

Claims (7)

1. a kind of experiment circuit device of waxy crude oil wax deposit test, it is characterised in that the device includes sample system and circuit Two parts of system;The sample system includes the first water-bath, oil tank and blowdown valve;The outer layer of first water-bath and oil tank presss from both sides Set is connected, and can control oil tank temperature;The blowdown valve is located at tank bottom, can discharge pot liquid;The circuit system is main Including peristaltic pump, mass flowmenter, the second water-bath, test pipeline section, the first differential pressure pick-up, third water-bath, reference pipeline section, second Differential pressure pick-up, sampling valve and connecting line;The peristaltic pump and oil tank can provide power for system;The mass flowmenter Measurable fluid flow;The both ends of the first differential pressure pick-up connecting test pipeline section, test pipeline section are positioned in the second water-bath, First differential pressure pick-up can measure the pressure drop of test pipeline section, the temperature of the second water-bath controllable testing pipeline section;Second differential pressure Sensor connects the both ends of reference pipeline section, and reference pipeline section is positioned in third water-bath, and the second differential pressure pick-up can measure reference tube The pressure drop of section, third water-bath can control the temperature of reference pipeline section;The sampling valve is placed in circuit end, can obtain fluid-like in real time This.
2. the experiment circuit device of waxy crude oil wax deposit test according to claim 1, it is characterised in that:The oil tank Top is equipped with electric mixer, for stirring grease system, accelerates oil mixing with water speed.
3. the experiment circuit device of waxy crude oil wax deposit test according to claim 1, it is characterised in that:The oil tank Equipped with outer layer chuck, circulator bath is for controlling experimental temperature in tank.
4. the experiment circuit device of waxy crude oil wax deposit test according to claim 1, it is characterised in that:The oil tank Inlet and exit setting are across pipeline, it can be achieved that the more sealing and circulating flow of tank.
5. the experiment circuit device of waxy crude oil wax deposit test according to claim 1, it is characterised in that:The test Pipeline section is equipped with three pipelines in parallel, and the caliber of three pipelines is different, and two ball valves are arranged in every pipeline both ends, can be to pipeline It is dismantled.
6. the experiment circuit device of waxy crude oil wax deposit test according to claim 1, it is characterised in that:The reference Pipeline section is equipped with three pipelines in parallel, and the caliber of three pipelines is different, and two ball valves are arranged in every pipeline both ends, can be to pipeline It is dismantled.
7. the experiment circuit device of waxy crude oil wax deposit test according to claim 1, it is characterised in that:The circuit If dry temperature sensor, pressure sensor are equipped with along the line, for acquiring circuit fluid flow parameters.
CN201820416138.3U 2018-03-26 2018-03-26 A kind of experiment circuit device of waxy crude oil wax deposit test Expired - Fee Related CN208076339U (en)

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CN201820416138.3U CN208076339U (en) 2018-03-26 2018-03-26 A kind of experiment circuit device of waxy crude oil wax deposit test

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109458566A (en) * 2018-12-21 2019-03-12 西安石油大学 A kind of device and method measuring solid precipitation characteristic at pipeline difference wall surface
CN110108444A (en) * 2019-04-28 2019-08-09 辽宁石油化工大学 A kind of sulfur-containing gas pipeline sulphur sedimentation experiment device
CN110608868A (en) * 2019-10-22 2019-12-24 中国海洋石油集团有限公司 Device and method for measuring change of outage state and restarting stress of oil-water mixed transportation sea pipe
CN111175167A (en) * 2020-02-20 2020-05-19 西南石油大学 Wax deposition characteristic and pipe flow characteristic simulation experiment device for wax-containing crude oil
CN111855513A (en) * 2019-04-29 2020-10-30 中国石油化工股份有限公司 Experimental device for be used for simulating wax deposit
CN112945963A (en) * 2021-02-01 2021-06-11 中国石油大学(北京) Observation sample and observation method

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109458566A (en) * 2018-12-21 2019-03-12 西安石油大学 A kind of device and method measuring solid precipitation characteristic at pipeline difference wall surface
CN110108444A (en) * 2019-04-28 2019-08-09 辽宁石油化工大学 A kind of sulfur-containing gas pipeline sulphur sedimentation experiment device
CN110108444B (en) * 2019-04-28 2020-12-01 辽宁石油化工大学 Sulfur deposition experimental device for sulfur-containing natural gas pipeline
CN111855513A (en) * 2019-04-29 2020-10-30 中国石油化工股份有限公司 Experimental device for be used for simulating wax deposit
CN110608868A (en) * 2019-10-22 2019-12-24 中国海洋石油集团有限公司 Device and method for measuring change of outage state and restarting stress of oil-water mixed transportation sea pipe
CN111175167A (en) * 2020-02-20 2020-05-19 西南石油大学 Wax deposition characteristic and pipe flow characteristic simulation experiment device for wax-containing crude oil
CN112945963A (en) * 2021-02-01 2021-06-11 中国石油大学(北京) Observation sample and observation method

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Granted publication date: 20181109

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