CN207899014U - A kind of separator being used in carbolineum extraction handle mixed triolein - Google Patents

A kind of separator being used in carbolineum extraction handle mixed triolein Download PDF

Info

Publication number
CN207899014U
CN207899014U CN201721891917.0U CN201721891917U CN207899014U CN 207899014 U CN207899014 U CN 207899014U CN 201721891917 U CN201721891917 U CN 201721891917U CN 207899014 U CN207899014 U CN 207899014U
Authority
CN
China
Prior art keywords
plate
inner housing
crystallization
carbolineum
separator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201721891917.0U
Other languages
Chinese (zh)
Inventor
陈建学
罗国林
侯海林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
QUJIN ZHONGYI FINECHEMICAL CO Ltd
Original Assignee
QUJIN ZHONGYI FINECHEMICAL CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by QUJIN ZHONGYI FINECHEMICAL CO Ltd filed Critical QUJIN ZHONGYI FINECHEMICAL CO Ltd
Priority to CN201721891917.0U priority Critical patent/CN207899014U/en
Application granted granted Critical
Publication of CN207899014U publication Critical patent/CN207899014U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

Abstract

The utility model discloses the separators that mixed triolein is handled in a kind of extraction for carbolineum, including inner housing, outer housing, auxiliary heat-exchanging mechanism and Crystallization Separation component, it is coaxially disposed inner housing in the outer housing, the auxiliary heat-exchanging mechanism is set on the outer wall of inner housing, the Crystallization Separation component is set in inner housing, the input port of the top setting access inner housing of outer housing, air bleeding valve, leakage fluid dram of the bottom of outer housing at least provided with three access inner housings, filled layer is set between inner housing and outer housing, temperature measurer is provided in the inner housing.The utility model is easy to use, mixed triolein by crystallization plates on piece be arranged arcuate structure exchange runner, enable high temperature mixed triolein quickly with exchanges liquid heat exchange, to fast cooling crystallization, it is passed through heat source in exchanging runner again, carbolic oil, naphtalene oil, washing oil are isolated respectively;Crystalline rate is high, and low energy consumption, is conducive to energy conservation and environmental protection and reduces production cost, to promote production economy benefit.

Description

A kind of separator being used in carbolineum extraction handle mixed triolein
Technical field
The utility model belongs to carbolineum extraction technical field of processing equipment, and in particular to one kind in carbolineum extraction for handling The separator of mixed triolein.
Background technology
The carbolineum contained in separation and Extraction coal tar industrially by coal tar concentrated processing and other compounds, are being extracted During carbolineum, mixed triolein will produce, the mixture that mixed triolein is then made of carbolic oil, naphtalene oil, washing oil, and carbolic oil, naphtalene oil, wash Oil all has higher utility value, it is therefore desirable to be extracted respectively to carbolic oil, naphtalene oil, washing oil;But traditional mixed triolein separation Long the time required to extracting mode, processing capacity is relatively low, high energy consumption, is unfavorable for energy conservation and environmental protection and expand production can needs.
Therefore, a kind of mixed triolein separator that crystallization is quick and efficient of development is the key that solve the problems, such as.
Utility model content
It is mixed that the utility model is intended to provide processing three during a kind of pollution-free, crystallization is quick and the efficient extraction for carbolineum The separator of oil.
What the purpose of this utility model was realized in:Including inner housing, outer housing, auxiliary heat-exchanging mechanism and Crystallization Separation Component is coaxially disposed inner housing in the outer housing, and the auxiliary heat-exchanging mechanism is set on the outer wall of inner housing, the crystallization Separation assembly is set in inner housing, the input port of the top setting access inner housing of outer housing, air bleeding valve, the bottom of outer housing The leakage fluid dram of access inner housing is set;Wherein, the Crystallization Separation component includes crystallizing plate, inlet tube, outlet tube, holder, It is respectively provided with exchange runner in the tow sides of crystallization plate, crystallization plate sequential setting makes between adjacent crystallization plate Exchange runner combine to be formed for exchange liquid by cavity, be respectively provided with inlet at the top of crystallization plate, each inlet it Between connected by inlet tube, crystallization plate bottom be respectively provided with liquid outlet, connected by outlet tube between each inlet, tie One end of each exchange runner on brilliant plate connects inlet by upper diversion trench, and the other end connects out liquid by lower diversion trench Mouthful, the two sides of the crystallization plate are respectively provided with holder, and the central part of the crystallization plate is arranged fulcrum, fulcrum is made to coordinate holder Crystallization plate is fixedly mounted.
Advantageous effect:The utility model is simple in structure, easy to use, and mixed triolein in crystallization plates on piece by being arranged arc knot The exchange runner of structure makes the turbulent flow of exchange liquid reinforce, and improves heat exchange efficiency, keeps the high temperature mixed triolein being discharged from reaction tower fast Speed exchanges heat with liquid is exchanged, and to which fast cooling crystallizes, then heat source is passed through in exchanging runner, according to carbolic oil, naphtalene oil, washing oil physics The different characteristic of melting point, respectively isolates carbolic oil, naphtalene oil, washing oil;Present apparatus crystallization time is short, and processing capacity is higher, crystallization Efficient, low energy consumption, is conducive to energy conservation and environmental protection and reduces production cost, production economy benefit purpose is promoted to reach.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the left view structural representation of the utility model;
Figure label:1 ~ outer housing, 2 ~ inner housing, 3 ~ heat exchange straight tube, 4 ~ heat exchange endless tube, 5 ~ filled layer, 6 ~ input port, 7 ~ Leakage fluid dram, 8 ~ crystallization plate, 9 ~ transition ring flat-plate, 10 ~ spacer ring, 11 ~ sealing ring, 12 ~ exchange runner, 13 ~ inlet, 14 ~ feed liquor Pipe, 15 ~ liquid outlet, 16 ~ outlet tube, 17 ~ upper diversion trench, 18 ~ lower diversion trench, 19 ~ holder, 20 ~ fulcrum.
Specific implementation mode
The utility model is further described with reference to embodiment, but the utility model is not added in any way With limitation, is transformed or replaced based on any made by the utility model introduction, belong to the scope of protection of the utility model.
Separator shown in 1 ~ 2 for handling mixed triolein in carbolineum extraction with reference to the accompanying drawings, including inner housing 2, shell Body 1, auxiliary heat-exchanging mechanism and Crystallization Separation component are coaxially disposed inner housing 2, the auxiliary heat-exchanging mechanism in the outer housing 1 It is set on the outer wall of inner housing 2, the Crystallization Separation component is set in inner housing 2, in the top setting access of outer housing 1 The input port 6 of shell 2, air bleeding valve, the leakage fluid dram 7 of the bottom setting access inner housing 2 of outer housing 1;Wherein, the Crystallization Separation Component includes crystallization plate 8, inlet tube 14, outlet tube 16, holder 19, and exchange current is respectively provided in the tow sides of crystallization plate 8 Road 12, crystallization 8 sequential of plate setting make the combination of exchange runner 12 between adjacent crystallization plate 8 be formed logical for exchanging liquid The cavity crossed is respectively provided with inlet 13 at the top of crystallization plate 8, is connected by inlet tube 14 between each inlet 13, The bottom of crystallization plate 8 is respectively provided with liquid outlet 15, is connected by outlet tube 16 between each inlet 13, crystallizes on plate 8 Each one end for exchanging runner 12 connects inlet 13 by upper diversion trench 17, and the other end connects liquid outlet by lower diversion trench 18 15, the two sides of the crystallization plate 8 are respectively provided with holder 19, and the central part of the crystallization plate 8 is arranged fulcrum 20, makes fulcrum 20 Coordinate holder 19 that crystallization plate 8 is fixedly mounted.
Exchange runner 12 on the crystallization plate 8 is arcuate structure, wherein is in the diameter between two stands 19 The exchange runner 12 of top half is arranged with the diameter symmetry for crossing inlet 13 and liquid outlet 15, straight between two stands 19 The exchange runner 12 of the lower half portion of diameter is staggered with the diameter for crossing inlet 13 and liquid outlet 15.
Each inlet 13 being corresponded on the inlet 13, dispersion liquid hole being set, dispersion liquid hole is connected to upper diversion trench 17;It is described Liquid outlet 15 on correspond to each liquid outlet 15 liquid collecting hole be set, the lower diversion trench of liquid collecting hole connection 18.
The crystallization plate 8 is arranged at disc structure, and setting transition ring flat-plate 9 at the outer rim of crystallization plate 8, the mistake Cross setting spacer ring 10 on ring flat-plate 9.
At least one sealing ring 11 is arranged in the external of transition ring flat-plate 9 on the crystallization plate 8.
The auxiliary heat-exchanging mechanism includes heat exchange straight tube 3, heat exchange endless tube 4, and 3 circumference of heat exchange straight tube is axially set in On the outer wall of inner housing 2, heat exchange endless tube 4 is respectively arranged at the both ends of heat exchange straight tube 3, makes heat exchange endless tube 4 each heat exchange straight tube 3 It is series at one, wherein a heat exchange endless tube 4 is provided into heat exchange straight tube 3 exchanges liquid, another heat exchange endless tube 4 is heat exchange straight tube Exchange liquid discharge in 3.
Filled layer 5 is set between the inner housing 2 and outer housing 1, improves and exchanges heat between inner housing 2 and heat exchange straight tube 3 Efficiency.
It is provided with temperature measurer in the inner housing 2.
The leakage fluid dram 7 at least there are three, respectively discharge carbolic oil, naphtalene oil, washing oil, prevent from mixing again.
The external equipment that thermal insulation layer is set, scald staff or indirectly heat periphery are prevented of the outer housing 1, drop Low equipment production safety hidden danger.
The working method of the utility model:From the mixed triolein being discharged in reaction tower after delivery pipe is delivered in inner housing 2, Low temperature is provided into Crystallization Separation component and auxiliary heat-exchanging mechanism respectively and exchanges liquid, it is logical that the low temperature in Crystallization Separation component exchanges liquid The each dispersion liquid hole crossed on inlet tube 14 flow to diversion trench 17, and low temperature, which is exchanged liquid, by upper diversion trench 17 distributes to exchange current road 12 combination formed for low temperature exchange liquid by cavity in, make low temperature exchange liquid lower water conservancy diversion is flowed downward under the guiding of cavity Slot 18, lower diversion trench 18 are delivered in outlet tube 16 by each liquid collecting hole after collecting, are discharged by outlet tube 16;And inner housing 2 In mixed triolein wrap crystallization plate 8, and by its included temperature by crystallize plate 8 pass to low temperature exchange liquid, make low Temperature exchanges liquid and the temperature in mixed triolein is taken away, and realizes that mixed triolein exchanges the heat exchange of liquid with low temperature, makes mixed triolein fast cooling And form crystallization;After crystallization, then empties the bottom temperature in Crystallization Separation component and auxiliary heat-exchanging mechanism and exchange liquid, and respectively It is passed through high temperature and exchanges liquid, the high temperature in Crystallization Separation component and auxiliary heat-exchanging mechanism is made to exchange liquid synchronous matching heating inner housing 2 In the mixed triolein that has crystallized, according to the different characteristic of carbolic oil, naphtalene oil, washing oil physics melting point, respectively carbolic oil, naphtalene oil, washing oil according to Secondary separation simultaneously goes out from leakage fluid dram 7.

Claims (10)

1. handling the separator of mixed triolein in a kind of extraction for carbolineum, it is characterised in that:Including inner housing(2), outer housing (1), auxiliary heat-exchanging mechanism and Crystallization Separation component, the outer housing(1)Middle coaxial arrangement inner housing(2), the auxiliary heat-exchanging Mechanism is set to inner housing(2)Outer wall on, the Crystallization Separation component is set to inner housing(2)In, outer housing(1)Top Setting access inner housing(2)Input port(6), air bleeding valve, outer housing(1)Bottom setting access inner housing(2)Leakage fluid dram (7);Wherein, the Crystallization Separation component includes crystallization plate(8), inlet tube(14), outlet tube(16), holder(19), tying Brilliant plate(8)Tow sides be respectively provided with exchange runner(12), crystallize plate(8)Sequential is arranged, and makes adjacent crystallization plate (8)Between exchange runner(12)Combination formed for exchange liquid by cavity, crystallization plate(8)Top be respectively provided with feed liquor Mouthful(13), each inlet(13)Between pass through inlet tube(14)Series connection, in crystallization plate(8)Bottom be respectively provided with liquid outlet (15), each inlet(13)Between pass through outlet tube(16)Series connection crystallizes plate(8)On each exchange runner(12)One End passes through upper diversion trench(17)Connect inlet(13), the other end passes through lower diversion trench(18)Connect liquid outlet(15), the knot Brilliant plate(8)Two sides be respectively provided with holder(19), the crystallization plate(8)Central part be arranged fulcrum(20), make fulcrum (20)Coordinate holder(19)Crystallization plate is fixedly mounted(8).
2. handling the separator of mixed triolein in the extraction according to claim 1 for carbolineum, it is characterised in that:Described Crystallize plate(8)On exchange runner(12)For arcuate structure, wherein be in two stands(19)Between diameter top half Exchange runner(12)To cross inlet(13)And liquid outlet(15)Diameter symmetry setting, be in two stands(19)Between it is straight The exchange runner of the lower half portion of diameter(12)To cross inlet(13)And liquid outlet(15)Diameter be staggered.
3. handling the separator of mixed triolein in the extraction according to claim 1 or 2 for carbolineum, it is characterised in that:Institute The inlet stated(13)The upper each inlet of correspondence(13)Dispersion liquid hole, the upper diversion trench of dispersion liquid hole connection are set(17);Described goes out Liquid mouth(15)The upper each liquid outlet of correspondence(15)Liquid collecting hole, the lower diversion trench of liquid collecting hole connection are set(18).
4. handling the separator of mixed triolein in the extraction according to claim 2 for carbolineum, it is characterised in that:Described Crystallize plate(8)It is arranged at disc structure, and crystallizes plate(8)Outer rim at be arranged transition ring flat-plate(9), the transition ring flat-plate (9)Upper setting spacer ring(10).
5. handling the separator of mixed triolein in the extraction according to claim 3 for carbolineum, it is characterised in that:Described Crystallize plate(8)On transition ring flat-plate(9)External at least one sealing ring is set(11).
6. handling the separator of mixed triolein in the extraction according to claim 1 for carbolineum, it is characterised in that:Described Auxiliary heat-exchanging mechanism includes heat exchange straight tube(3), heat exchange endless tube(4), the heat exchange straight tube(3)Circumference is axially set in inner housing (2)Outer wall on, exchange heat endless tube(4)It is respectively arranged at heat exchange straight tube(3)Both ends, make heat exchange endless tube(4)Each heat exchange is straight Pipe(3)It is series at one, wherein a heat exchange endless tube(4)To heat exchange straight tube(3)Middle offer exchanges liquid, another heat exchange endless tube (4)Heat exchange straight tube(3)In exchange liquid discharge.
7. handling the separator of mixed triolein in the extraction according to claim 1 for carbolineum, it is characterised in that:Described Inner housing(2)With outer housing(1)Between filled layer is set(5).
8. handling the separator of mixed triolein in the extraction according to claim 1 for carbolineum, it is characterised in that:Described Inner housing(2)In be provided with temperature measurer.
9. handling the separator of mixed triolein in the extraction according to claim 1 for carbolineum, it is characterised in that:Described Leakage fluid dram(7)There are three at least.
10. handling the separator of mixed triolein in the extraction according to claim 1 for carbolineum, it is characterised in that:It is described Outer housing(1)External thermal insulation layer is set.
CN201721891917.0U 2017-12-29 2017-12-29 A kind of separator being used in carbolineum extraction handle mixed triolein Active CN207899014U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721891917.0U CN207899014U (en) 2017-12-29 2017-12-29 A kind of separator being used in carbolineum extraction handle mixed triolein

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721891917.0U CN207899014U (en) 2017-12-29 2017-12-29 A kind of separator being used in carbolineum extraction handle mixed triolein

Publications (1)

Publication Number Publication Date
CN207899014U true CN207899014U (en) 2018-09-25

Family

ID=63569454

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721891917.0U Active CN207899014U (en) 2017-12-29 2017-12-29 A kind of separator being used in carbolineum extraction handle mixed triolein

Country Status (1)

Country Link
CN (1) CN207899014U (en)

Similar Documents

Publication Publication Date Title
CN109608353B (en) Continuous production process and device for m-aminoacetanilide
CN207899014U (en) A kind of separator being used in carbolineum extraction handle mixed triolein
CN204115519U (en) A kind of built-in lower perforated plate formula graphite heat exchanger
CN204208551U (en) A kind of chemical industry liquid reactions still
CN101893351A (en) Multi-stage heat exchanger
CN205472658U (en) High -efficient sulfur trioxide transition system
CN204251354U (en) A kind of energy-saving copper sulfate crystal tripping device
CN207805104U (en) A kind of Crystallization Separation component for handling mixed triolein
CN203653465U (en) Continuous production device for benzoic acid
CN204495077U (en) A kind of high-temperature calcination stove helical form petroleum coke cooling jacket
CN202542891U (en) Evaporation crystallizer for crystallization of magnesium sulfate solution
CN204952603U (en) High -efficient graphite falling liquid film absorber
CN206014730U (en) A kind of phenylacetic acid continuous production device
CN102764518A (en) Salt crystallizer
CN103435628A (en) Purification method of benzenetetracarboxylic anhydride
CN203448097U (en) Nitration reaction kettle
CN207169678U (en) A kind of liquid material combination cooling device
CN202893211U (en) Water glass dissolving waste heat recovery device
CN206142823U (en) High -purity sulphuric acid purification equipment
CN203053260U (en) Gas and water mixer
CN205137395U (en) High -temperature heat pipe formula high temperature melting furnace sediment steam generator
CN202322797U (en) Cooling device for distillation
CN202666455U (en) Salt set crystallizer
CN203315769U (en) Corrosion-resistant magnesium nitrate heater
CN205980440U (en) Take chemical heat pump of multichannel membrane reactor

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant