CN207769762U - A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle - Google Patents
A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle Download PDFInfo
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- CN207769762U CN207769762U CN201721494233.7U CN201721494233U CN207769762U CN 207769762 U CN207769762 U CN 207769762U CN 201721494233 U CN201721494233 U CN 201721494233U CN 207769762 U CN207769762 U CN 207769762U
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Abstract
The utility model discloses a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettles, including autoclave body, kettle cover, supersonic generator, microwave generator, controller, microwave heating waveguide pipe, oscillator；The kettle cover is located at autoclave body top, is covered to autoclave body opening；The autoclave body is equipped with first interface, for connecting oscillator；The oscillator is at least one, is connected with supersonic generator；The autoclave body bottom side wall is equipped with second interface, and microwave heating waveguide pipe is arranged at second interface, and microwave heating waveguide pipe is connected with microwave generator；The controller is separately connected ultrasonic generator and microwave generator, the working condition for controlling ultrasonic generator and microwave generator；There are heat-insulation system and electric heating system, electric heating system to be connected with controller outside the autoclave body, controller controls the working condition of electric heating system；The utility model can realize that the combination of a variety of single experimental situations or several experimental situations, operating mode are various in a reaction kettle.
Description
Technical field
The utility model belongs to chemical industry technical field, especially a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction
Kettle.
Background technology
Reaction kettle is in the eighties or so utility model, it has obtained the extensive use of chemical industry after this, and
Always all in fast development among.Recent domestic is ceaselessly being reformed and innovated with regard to its Development Techniques and method, to
It is better adapted to the chemical industry of rapid development.China's nowadays manufactured reaction kettle, mostly in 6000L or less.Due to anti-
The quality error in the volume size of kettle, batch production is answered to suffer from close contact to yield and product cost, so this
Affect the quality, cost and sales volume of chemical products.In addition, in the composition of reaction kettle, although via single blender
The forced circulation of double stirrer or additional pump is developed to, and external is even more also to make autoclave body along horizontal line other than blender is housed
Rotation, to improve reaction speed.But be increasingly difficult to meet the needs of chemical industry instantly, need to develop it is more efficient,
More applicable reaction kettle.Furthermore as global warming generates it while the development of chemical industry in recent years
Contamination control is also increasingly stringenter, so, from big trend, we to set about research reaction kettle, will larger from
It is energy saving, environmentally friendly and higher technological operation, and set about from material etc., to meet the variation in market and trend.
Invention content
The technical issues of the utility model is solved is to provide a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle, sharp
With the distinctive property of ultrasonic/microwave, with solve the problems, such as common response kettle have a single function and high energy consumption.
Realize that the technical solution of the utility model aim is：
A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle, including autoclave body, kettle cover, supersonic generator, microwave occur
Device, controller, microwave heating waveguide pipe, oscillator；
The kettle cover is located at autoclave body top, is covered to autoclave body opening；The autoclave body is equipped with first interface, for connecting
Connect oscillator；The oscillator is at least one, is connected with supersonic generator；The autoclave body bottom side wall is equipped with second interface,
Microwave heating waveguide pipe is arranged at second interface, and microwave heating waveguide pipe is connected with microwave generator；The controller difference
Connect ultrasonic generator and microwave generator, the working condition for controlling ultrasonic generator and microwave generator.
The utility model compared with prior art, remarkable advantage：
(1) the ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle of the utility model is simple in structure, small, and operates letter
Easily.
(2) versatility is good：Ultrasonic/microwave hydro-thermal/meto-super-critical the reaction kettle of the utility model can be used as hydro-thermal reaction
Kettle can also be used as meto-super-critical fluid reaction kettle.
(3) operating mode is various：Single electric heating system or ultrasound or microwave heating may be selected by controller, but
Combination of two heats, and can also be three and cooperatively acts on heating.
(4) the ultrasonic/microwave good directionality generated by ultrasonic generator and microwave generator, penetration capacity is strong, saves
In the reaction time, experiment process can be greatly speeded up, thermal energy can be also saved.
The utility model is described in further detail below in conjunction with the accompanying drawings.
Description of the drawings
Fig. 1 is the structure diagram of the ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle of the utility model.
Specific implementation mode
In order to illustrate the technical solution of the utility model and technical purpose, below in conjunction with the accompanying drawings and specific embodiment is to this reality
It is described further with novel.
A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle of the utility model, including autoclave body 1, kettle cover 2, ultrasonic wave hair
Raw device 4, microwave generator 3, controller 5, microwave heating waveguide pipe, oscillator 8；
The kettle cover 2 is located at 1 top of autoclave body, is covered to the opening of autoclave body 1；The autoclave body 1 is equipped with first interface 1-
1, for connecting oscillator 8；The oscillator 8 be at least one, be connected with supersonic generator 4, with by ultrasound in autoclave body 1
Liquid is vibrated and is heated；1 bottom sidewall of the autoclave body is equipped with second interface 1-2, and the setting of microwave heating waveguide pipe exists
At second interface 1-2, microwave heating waveguide pipe is connected with microwave generator 3, to heat to liquid in autoclave body 1；Institute
It states controller 5 and is separately connected ultrasonic generator and microwave generator 3, the work for controlling ultrasonic generator and microwave generator 3
Make state.
Further, there are heat-insulation system and electric heating system, electric heating system to be connected with controller 5 outside the autoclave body 1, control
Device 5 processed controls the working condition of electric heating system.While realizing the effect to being stirred in autoclave body 1 using ultrasound, microwave, also may be used
Autoclave body 1 is heated by electric heating system.
It is further improved, polytetrafluoroethylene (PTFE) retort is additionally provided in the autoclave body 1, polytetrafluoroethylene (PTFE) retort has sampling
Interface.
Further, the advantages of use of the autoclave body 1 Hastelloy or special steel alloy, the two, is intensity height, corrosion resistant
Corrosion is excellent.
Further, the first interface 1-1 is located at the bottom of autoclave body 1, and oscillator 8 is arranged in the bottom of autoclave body 1；Oscillator 8
Partition board 7 is arranged between autoclave body 1 to separate.Preferably, partition board 7 uses ceramic separator, has good heat-blocking action.
Further, the second interface 1-2 is sealed using the sapphire glass 6 of pressure high-temp resistant, sapphire glass 6
Outside is equipped with endless metal pipeline, is extended out with shield microwaves.
Further, it is connected with water load between the microwave generator 3 and microwave heating waveguide pipe, using water as negative
It carries resistance and plays the role of a protection.
Further, the second interface 1-2 uses flange form connecting interface, interface reliability and durability.
When work, the working condition of supersonic generator 4, microwave generator 3, electric heating system is controlled by controller 5,
Single electric heating system or ultrasound or microwave heating may be selected, but combination of two heats, and can also be three and cooperatively makees
With heating.Ultrasonic/microwave hydro-thermal/meto-super-critical the reaction kettle of the utility model can be used as hydrothermal reaction kettle, can also be used as
Meto-super-critical fluid reaction kettle, operating mode is various, versatility is good, can be as the reaction vessel of more Multi-example, and can be more
Soon, more thoroughly reactant is cleared up.
Ultrasonic/microwave hydro-thermal/meto-super-critical the reaction kettle of the utility model is simple in structure, small, and operates simple.It is logical
It is good with property：The ultrasonic/microwave good directionality generated by ultrasonic generator and microwave generator, penetration capacity is strong, and possesses brokenly
Broken function can play the role of a stirring to accelerate to react to the sample in autoclave body 1, save the reaction time, can be significantly
Accelerate experiment process, can also save thermal energy.
Claims (7)
1. a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle, including it is autoclave body (1), kettle cover (2), supersonic generator (4), micro-
Wave producer (3), controller (5), microwave heating waveguide pipe, oscillator (8)；
The kettle cover (2) is located at autoclave body (1) top, is covered to autoclave body (1) opening；The autoclave body (1) connects equipped with first
Mouth (1-1), for connecting oscillator (8)；The oscillator (8) is at least one, is connected with supersonic generator (4)；The kettle
Body (1) bottom sidewall is equipped with second interface (1-2), and microwave heating waveguide pipe is arranged at second interface (1-2), microwave heating wave
Conduit is connected with microwave generator (3)；The controller (5) is separately connected ultrasonic generator and microwave generator (3), for controlling
The working condition of ultrasonic generator and microwave generator (3) processed.
2. a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle as described in claim 1, which is characterized in that the autoclave body
(1) heat-insulation system and electric heating system, electric heating system are connected with controller (5) outside, controller (5) controls electric heating system
Working condition.
3. a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle as claimed in claim 1 or 2, which is characterized in that the kettle
It is additionally provided with polytetrafluoroethylene (PTFE) retort in body (1).
4. a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle as claimed in claim 1 or 2, which is characterized in that the kettle
Body (1) uses Hastelloy or special steel alloy.
5. a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle as described in claim 1, which is characterized in that described first connects
Mouth (1-1) is located at the bottom of autoclave body (1), and oscillator (8) is arranged in the bottom of autoclave body (1)；It is arranged between oscillator (8) and autoclave body (1)
Partition board (7) separates.
6. a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle as claimed in claim 5, which is characterized in that the partition board
(7) ceramic separator is used.
7. a kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle as described in claim 1 or 6, which is characterized in that described
Two interfaces (1-2) are sealed using the sapphire glass (6) of pressure high-temp resistant, and endless metal is equipped with outside sapphire glass (6)
Pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721494233.7U CN207769762U (en) | 2017-11-10 | 2017-11-10 | A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721494233.7U CN207769762U (en) | 2017-11-10 | 2017-11-10 | A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207769762U true CN207769762U (en) | 2018-08-28 |
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ID=63233231
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721494233.7U Active CN207769762U (en) | 2017-11-10 | 2017-11-10 | A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207769762U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107715816A (en) * | 2017-11-10 | 2018-02-23 | 西南科技大学 | A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reactor |
| CN111871351A (en) * | 2020-08-10 | 2020-11-03 | 邵武永太高新材料有限公司 | Lithium fluoride ultrasonic dynamic reaction crystallization process and ultrasonic dynamic reaction crystallization equipment thereof |
-
2017
- 2017-11-10 CN CN201721494233.7U patent/CN207769762U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107715816A (en) * | 2017-11-10 | 2018-02-23 | 西南科技大学 | A kind of ultrasonic/microwave hydro-thermal/meto-super-critical reactor |
| CN111871351A (en) * | 2020-08-10 | 2020-11-03 | 邵武永太高新材料有限公司 | Lithium fluoride ultrasonic dynamic reaction crystallization process and ultrasonic dynamic reaction crystallization equipment thereof |
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