CN207708983U - A kind of novel speed up gas and liquid or the device of liquid liquid mixing - Google Patents
A kind of novel speed up gas and liquid or the device of liquid liquid mixing Download PDFInfo
- Publication number
- CN207708983U CN207708983U CN201721492442.8U CN201721492442U CN207708983U CN 207708983 U CN207708983 U CN 207708983U CN 201721492442 U CN201721492442 U CN 201721492442U CN 207708983 U CN207708983 U CN 207708983U
- Authority
- CN
- China
- Prior art keywords
- liquid
- reaction kettle
- mixing chamber
- pipe
- outlet pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 68
- 238000006243 chemical reaction Methods 0.000 claims abstract description 59
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 51
- 238000003756 stirring Methods 0.000 claims abstract description 34
- 239000007864 aqueous solution Substances 0.000 claims abstract description 30
- 239000004615 ingredient Substances 0.000 claims abstract description 19
- 238000013517 stratification Methods 0.000 claims abstract description 7
- 239000000284 extract Substances 0.000 claims abstract description 4
- 239000007858 starting material Substances 0.000 claims abstract description 4
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 239000000523 sample Substances 0.000 claims description 14
- 238000004140 cleaning Methods 0.000 claims description 12
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 abstract description 22
- 239000006228 supernatant Substances 0.000 abstract description 2
- 239000003054 catalyst Substances 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 239000000243 solution Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 3
- 238000006555 catalytic reaction Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model discloses the device of a kind of novel speed up gas and liquid or the mixing of liquid liquid,Including reaction kettle and mixing chamber,The top of reaction kettle is equipped with feed pipe and water inlet pipe,Stirring rod is equipped in reaction kettle,The end of stirring rod is equipped with stirring blade,The bottom of reaction kettle is equipped with water outlet,Water outlet is equipped with outlet pipe,Reaction kettle is connected to by outlet pipe with mixing chamber,Organic Ingredients liquid organic starting material is separated into lower aqueous solution and supernatant liquid raw material after stratification,Lower aqueous solution is flow to by reaction kettle in mixing chamber by outlet pipe,It is equipped with flowing water Valve and suction pump successively along the direction of lower aqueous solution flowing on outlet pipe,Suction pump extracts the water in reaction kettle to mixing chamber,Raschig ring is equipped in mixing chamber,Mixing chamber is connected to by water inlet pipe with reaction kettle,Entered in reaction kettle by water inlet pipe by the lower aqueous solution of Raschig ring.The utility model can remove the aluminium chloride in Organic Ingredients liquid.
Description
Technical field
The utility model belongs to mixing arrangement field, is more particularly to the dress of a kind of novel speed up gas and liquid or the mixing of liquid liquid
It sets.
Background technology
Existing mixing arrangement is the reaction kettle with agitating function, and water droplet is added in material, depends merely on stirring to mix
Close material and water, achieve the effect that from organic matter to wash catalyst into water, but because mixing plant rotating speed it is unsuitable it is excessively high can not
It thoroughly cleans up, causes material in back segment process, attachment becomes waste discharge in the catalyst, increases production cost.
Therefore, existing mixing arrangement the problem is that：It is easy to take impurity to the next section of increase for causing waste, improves life
Produce cost；Since stirring efficiency is bad, causes processing time long, influence production scheduling.
Utility model content
The purpose of this utility model is to provide that a kind of mixing velocity is very fast and the preferably novel speed up gas and liquid of the uniformity or liquid
The device of liquid mixing.
One side according to the present utility model provides the device of a kind of novel speed up gas and liquid or the mixing of liquid liquid, including
Reaction kettle and mixing chamber,
The top of the reaction kettle is equipped with feed pipe and water inlet pipe, and Organic Ingredients liquid passes through described in feed pipe entrance
In reaction kettle,
Stirring rod is equipped in the reaction kettle, the end of the stirring rod is equipped with stirring blade, the stirring rod and motor
Rotation axis connection, the motor drives the stirring rod to drive stirring blade rotation to organic original in the reaction kettle
Material liquid organic starting material is stirred,
The bottom of the reaction kettle is equipped with water outlet, and the water outlet is equipped with outlet pipe, and the reaction kettle passes through described
Outlet pipe is connected to the mixing chamber, and Organic Ingredients liquid organic starting material is separated into lower aqueous solution and upper after stratification
Layer liquid charging stock, lower aqueous solution flow to by the reaction kettle in the mixing chamber by outlet pipe, on the outlet pipe along
The direction of lower aqueous solution flowing is equipped with flowing water Valve and suction pump successively, and the suction pump extracts the water in the reaction kettle
In to the mixing chamber,
Raschig ring is equipped in the mixing chamber, the mixing chamber is connected to by water inlet pipe with the reaction kettle, by drawing west
The lower aqueous solution of ring is entered by water inlet pipe in reaction kettle.
Liquid to be layered is entered by feed pipe in reaction kettle, and under the stirring of stirring rod and stirring blade, liquid fills
Stratification again after point mixing in the lower aqueous solution of layering or can contain catalyst aluminum chloride, and suction pump will contain catalysis
The aqueous solution of agent is pumped into mixing chamber, and the Raschig ring in mixing chamber may filter that aluminium chloride in aqueous solution, filter out aluminium chloride
Aqueous solution entered in reaction kettle by water inlet pipe continue to stir to obtain be free of catalyst aluminum chloride Organic Ingredients solution.
In some embodiments, the outlet pipe is also associated with probe tube, the company of the probe tube and the outlet pipe
Node is connect between the outlet valve and the suction pump, the probe tube is equipped with sample cock.By probe tube to anti-
Organic Ingredients solution in kettle is answered to be sampled, when its saturation degree reaches 1.23-1.24, liquid charging stock is added in stopping.
In some embodiments, the outlet pipe is also associated with cleaning pipe, the company of the cleaning pipe and the outlet pipe
Node is connect between the outlet valve and the suction pump, the cleaning pipe is equipped with wash-out valve.It needs to whole device
When being cleaned, then a large amount of clear water is injected into device by cleaning pipe, whole device is cleaned.
In some embodiments, the water inlet pipe be located on the side wall of the end in the reaction kettle offer it is multiple go out
Water hole.Water is set uniformly to spray into reaction kettle.
A kind of mixed method of novel speed up gas and liquid or the device of liquid liquid mixing,
Material is entered by the feed pipe in the reaction kettle, is mixed with the water in the reaction kettle；
After the stirring rod drives the stirring blade stirring material and water under the driving of motor, stratification；
Lower aqueous solution in the reaction kettle is entered via the outlet pipe in the mixing chamber by the water outlet；
Catalyst aluminum chloride in the indoor Raschig ring removal aqueous solution of mixing；
The indoor aqueous solution of mixing, which enters via the water inlet pipe in reaction kettle, to be continued to be stirred until obtaining not
Organic Ingredients solution containing catalyst aluminum chloride.
Description of the drawings
Fig. 1 is the structural representation of a kind of novel speed up gas and liquid of one embodiment of the utility model or the device of liquid liquid mixing
Figure.
Specific implementation mode
Fig. 1 schematically shows a kind of novel speed up gas and liquid of embodiment of the utility model or the dress of liquid liquid mixing
It sets.As shown in Figure 1, the novel speed up gas and liquid or the device of liquid liquid mixing include reaction kettle 1 and mixing chamber 2.
The top of reaction kettle 1 is equipped with feed pipe 11 and water inlet pipe 12.Water inlet pipe 12 is located at the side wall of the end in reaction kettle 1
On offer multiple apopores.Water is set uniformly to spray into reaction kettle 1.Organic Ingredients liquid is entered by feed pipe 11 to react
In 1 kettle.Stirring rod 31 is equipped in reaction kettle 1.The end of stirring rod 31 is equipped with stirring blade 32.The rotation of stirring rod 31 and motor
Axis connection, motor driving stirring rod 31 drive the rotation of stirring blade 32 to be stirred the Organic Ingredients liquid in reaction kettle 1.Instead
The bottom of kettle 1 is answered to be equipped with water outlet, water outlet is equipped with outlet pipe 13.Reaction kettle 1 is connected to by outlet pipe 13 with mixing chamber 2.
Organic Ingredients liquid is separated into lower aqueous solution and supernatant liquid raw material after stratification.Lower aqueous solution passes through outlet pipe
13 are flow to by reaction kettle 1 in mixing chamber 2.It is equipped with flowing water Valve successively along the direction of lower aqueous solution flowing on outlet pipe 13
131 and suction pump 132.Flowing water Valve 131 is opened, suction pump 132 extracts the water in reaction kettle 1 to mixing chamber 2.Mixing chamber
Raschig ring 21 is equipped in 2.Mixing chamber 2 is connected to by water inlet pipe 12 with reaction kettle 1.Lower aqueous solution by Raschig ring 21 passes through
Water inlet pipe 12 enters in reaction kettle 1.Organic Ingredients liquid is entered by feed pipe 11 in reaction kettle 1, and Organic Ingredients liquid is abundant
Stratification again after mixing in the lower aqueous solution of layering or can contain catalyst aluminum chloride, and suction pump 132 will contain catalysis
The aqueous solution of agent is pumped into mixing chamber 2, and the Raschig ring 21 in mixing chamber 2 may filter that aluminium chloride in aqueous solution, filter out chlorine
The aqueous solution of change aluminium, which is entered by water inlet pipe 12 in reaction kettle 1, to be continued to stir to obtain Organic Ingredients solution.Outlet pipe 13 is also associated with
Probe tube 14.The connecting node of probe tube 14 and outlet pipe 13 is between outlet valve 131 and suction pump 132.On probe tube 14
Equipped with sample cock 141.The Organic Ingredients solution in reaction kettle 1 is sampled by probe tube 14, when its saturation degree reaches
1.23-1.24 stopping that liquid charging stock is added.Outlet pipe 13 is also associated with cleaning pipe 15, the connection of cleaning pipe 15 and outlet pipe 13
Node is between outlet valve 131 and suction pump 132.Cleaning pipe 15 is equipped with wash-out valve 151.It needs to carry out whole device
When cleaning, wash-out valve 151 is opened, a large amount of clear water is injected into device by cleaning pipe 15, whole device is cleaned.
The present embodiment is by taking the mixing of liquid liquid as an example.
A kind of mixed method of novel speed up gas and liquid or the device of liquid liquid mixing：Material enters reaction kettle by feed pipe 11
In 1, mixed with the water in reaction kettle 1；It is quiet after stirring rod 31 drives stirring blade 32 to stir material and water under the driving of motor
Set layering；Lower aqueous solution in reaction kettle 1 is entered via outlet pipe 13 in mixing chamber 2 by water outlet；Drawing in mixing chamber 2
Western ring 21 removes the catalyst aluminum chloride in aqueous solution；Mix indoor aqueous solution via water inlet pipe 12 enter reaction kettle in continue
It is stirred until obtaining the Organic Ingredients solution without catalyst aluminum chloride.
Above-described is only some embodiments of the utility model.For those of ordinary skill in the art, exist
Under the premise of not departing from the concept of the present invention, various modifications and improvements can be made, it is new that these belong to this practicality
The protection domain of type.
Claims (4)
1. a kind of novel speed up gas and liquid or the device of liquid liquid mixing, which is characterized in that including reaction kettle and mixing chamber,
The top of the reaction kettle is equipped with feed pipe and water inlet pipe, and Organic Ingredients liquid enters the reaction by the feed pipe
In kettle, stirring rod is equipped in the reaction kettle, the end of the stirring rod is equipped with stirring blade, the rotation of the stirring rod and motor
Shaft connects, and the motor drives the stirring rod to drive the stirring blade rotation to the Organic Ingredients liquid in the reaction kettle
Body Organic Ingredients is stirred,
The bottom of the reaction kettle is equipped with water outlet, and the water outlet is equipped with outlet pipe, and the reaction kettle passes through the water outlet
Pipe is connected to the mixing chamber, and Organic Ingredients liquid organic starting material is separated into lower aqueous solution and upper liquid after stratification
Body raw material, lower aqueous solution is flow to by the reaction kettle in the mixing chamber by outlet pipe, along lower layer on the outlet pipe
The direction of aqueous solution flowing is equipped with flowing water Valve and suction pump successively, and the suction pump extracts the water in the reaction kettle to institute
It states in mixing chamber, Raschig ring is equipped in the mixing chamber, the mixing chamber is connected to by water inlet pipe with the reaction kettle, by drawing
The lower aqueous solution of western ring is entered by water inlet pipe in reaction kettle.
2. novel speed up gas and liquid according to claim 1 or the device of liquid liquid mixing, which is characterized in that the outlet pipe is also
Be connected with probe tube, the connecting node of the probe tube and the outlet pipe between the outlet valve and the suction pump,
The probe tube is equipped with sample cock.
3. novel speed up gas and liquid according to claim 1 or the device of liquid liquid mixing, which is characterized in that the outlet pipe is also
Be connected with cleaning pipe, the connecting node of the cleaning pipe and the outlet pipe between the outlet valve and the suction pump,
The cleaning pipe is equipped with wash-out valve.
4. novel speed up gas and liquid according to claim 1 or the device of liquid liquid mixing, which is characterized in that the water inlet pipe position
In offering multiple apopores on the side wall of the end in the reaction kettle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721492442.8U CN207708983U (en) | 2017-11-09 | 2017-11-09 | A kind of novel speed up gas and liquid or the device of liquid liquid mixing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721492442.8U CN207708983U (en) | 2017-11-09 | 2017-11-09 | A kind of novel speed up gas and liquid or the device of liquid liquid mixing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207708983U true CN207708983U (en) | 2018-08-10 |
Family
ID=63061097
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721492442.8U Expired - Fee Related CN207708983U (en) | 2017-11-09 | 2017-11-09 | A kind of novel speed up gas and liquid or the device of liquid liquid mixing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207708983U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107803156A (en) * | 2017-11-09 | 2018-03-16 | 大丰鑫源达化工有限公司 | A kind of new speed up gas and liquid or the device of liquid liquid mixing |
-
2017
- 2017-11-09 CN CN201721492442.8U patent/CN207708983U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107803156A (en) * | 2017-11-09 | 2018-03-16 | 大丰鑫源达化工有限公司 | A kind of new speed up gas and liquid or the device of liquid liquid mixing |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180810 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |