CN207507451U - A kind of reaction kettle - Google Patents

A kind of reaction kettle Download PDF

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Publication number
CN207507451U
CN207507451U CN201721087046.7U CN201721087046U CN207507451U CN 207507451 U CN207507451 U CN 207507451U CN 201721087046 U CN201721087046 U CN 201721087046U CN 207507451 U CN207507451 U CN 207507451U
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Prior art keywords
reaction
reaction cavity
pump
cavity
heat
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CN201721087046.7U
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Chinese (zh)
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雷震
余雪玲
丁轶
黄仕科
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Zhuhai Najin Technology Co Ltd
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Zhuhai Najin Technology Co Ltd
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Abstract

The utility model belongs to chemical reaction device technical field, a kind of reaction kettle is provided, including reaction cavity, it is connected to the feed inlet of the reaction cavity upper end, the rate controlling component that is connected with the feed inlet and it is connected to the temperature control component on the reaction cavity and for controlling the reaction chamber body temperature, and it is connected to the reaction cavity bottom and the mixing component for accelerating the discharge component of discharging with being connected on the reaction cavity and be used to accelerate reaction, the temperature control component includes the passage of heat being attached on the reaction cavity inner wall and the circulating pump being connected on the passage of heat, the discharge component includes discharging pump and the material storing box for connecting the discharging pump;Design can solve the problem of that existing consersion unit blowing error is big, reaction temperature cannot intelligently control and discharging time length easily leads to overreaction in this way.

Description

A kind of reaction kettle
Technical field
The utility model belongs to chemical reaction device technical field more particularly to a kind of reaction kettle.
Background technology
Reaction kettle is a kind of common consersion unit in chemical plant, and it is anti-to stir mainly to drive agitating shaft by motor Object is answered, it is made fully to react to obtain required substance.With the continuous development of chemical field, people are to the original of chemical products The precision of material and chemical products all improves requirement, and corresponding people are to the important equipment in chemical reaction -- and reaction kettle also carries Higher requirement is gone out.It is by manually feeding to commonly use traditional reaction kettle charge door at present, and drain hole is to pass through nature Gravity carries out blowing, realizes that long-time constant temperature is kept the temperature by way of heating.But existing reaction kettle is due to artificial side Formula charging will appear larger error, and reaction temperature cannot cool down quickly, and the time of discharging is long, easily leads to reaction It excessively carries out, influences the quality of raw material reaction.
Utility model content
The purpose of this utility model is to provide a kind of reaction kettles, it is intended to solve existing consersion unit blowing error it is big, The problem of reaction temperature cannot intelligently control, and discharging time length easily leads to overreaction.
The utility model solves in this way:A kind of reaction kettle including reaction cavity, is connected to the reaction cavity upper end Feed inlet, the rate controlling component that is connected with the feed inlet and be connected on the reaction cavity and for controlling the reaction chamber The temperature control component of body temperature and be connected to the reaction cavity bottom and for accelerate discharging discharge component and be connected to Mixing component on the reaction cavity and for accelerating reaction, the temperature control component include being attached at the reaction cavity inner wall On passage of heat and the circulating pump that is connected on the passage of heat, the discharge component include discharging pump and go out described in connecting Expect the material storing box of pump.
Further, the feed inlet includes the feeding-in solid body mouth and liquid feedstock that are arranged on the reaction cavity top Mouthful, the rate controlling component connection is on the liquid inlet opening.
Further, the rate controlling component includes the connecting tube being connected on the liquid inlet opening, is connected to the company The rate controlling valve taken over and the syringe pump for being connected to the connection pipe end.
Further, flowing has conductive fluid in the passage of heat, and feed liquor is further opened on the side wall of the reaction cavity Mouth and liquid outlet, the inlet connect the circulating pump with the liquid outlet.
Further, the inlet is located at the lower section of the liquid outlet.
Further, it is connected with the first connecting tube between the inlet and the circulating pump, the liquid outlet and described The second connecting tube is connected between circulating pump, the first check valve, second connecting tube are also associated in first connecting tube On be also associated with the second check valve.
Further, the discharging pump is the anti-acid and alkali pumps of industry, and the reaction cavity bottom is in funnel-form, the discharging Discharge nozzle is also associated between pump and the reaction cavity, the top of the discharge nozzle connects the bottom of the reaction cavity.
Further, total baiting valve is also associated on the discharge nozzle, is additionally provided with triple valve in the discharging pump, described three One end of port valve connects the discharge nozzle, and one end connects the material storing box, other end connection ash can, the discharging pump with it is described The first shut-off valve is equipped between material storing box, the second shut-off valve is equipped between the discharging pump and the ash can.
Further, the level height of the material storing box is higher than the level height of the reaction cavity bottom.
Further, the mixing component includes the driving motor being connected on the reaction cavity, is connected to the drive Drive shaft on dynamic motor is located at the blender for driving shaft end, the drive shaft is connected in the reaction cavity Between.
The technique effect that reaction kettle provided by the utility model has compared with the prior art is:By on feed inlet Rate controlling component is connected, and then the speed of charging and the quantity of charging can be automatically controlled, it is anti-caused by so as to avoid hand feed Answer the error of result;Simultaneously temperature control component setting reaction cavity can be heated in advance or during the reaction into Row heating, and then the control of temperature is more flexible, and can rapidly be realized by circulating pump and passage of heat and cooperation The cooling of reaction cavity avoids cooling caused overreact not in time;And reaction cavity bottom connection discharging pump and material storing box, So as to realize that the stoste after reaction detaches as soon as possible, and then avoid the purity and quality of overreaction influence stoste.
Description of the drawings
It, below will be to embodiment or the prior art in order to illustrate more clearly of the technical scheme in the embodiment of the utility model Attached drawing is briefly described needed in description, it should be apparent that, the accompanying drawings in the following description is only that this practicality is new Some embodiments of type, for those of ordinary skill in the art, without having to pay creative labor, can be with Other attached drawings are obtained according to these attached drawings.
Fig. 1 is the structure diagram for the reaction kettle that the utility model embodiment provides.
Specific embodiment
In order to make the purpose of the utility model, technical solutions and advantages more clearly understood, below in conjunction with attached drawing and implementation Example, the present invention is further described in detail.It should be appreciated that specific embodiment described herein is only used to explain The utility model is not used to limit the utility model.
It should be noted that when element is referred to as " being fixed on " or " being set to " another element, it can be directly another On one element or it is connected on another element.When an element is known as " being connected to " another element, it can To be directly to another element or be indirectly connected on another element.
It is to be appreciated that term " length ", " width ", " on ", " under ", "front", "rear", "left", "right", " vertical ", The orientation or position relationship of the instructions such as " level ", " top ", " bottom " " interior ", " outer " are to be closed based on orientation shown in the drawings or position System is for only for ease of description the utility model and simplifies description rather than instruction or imply that signified device or element are necessary With specific orientation, with specific azimuth configuration and operation, therefore it is not intended that limitation to the utility model.
In addition, term " first ", " second " are only used for description purpose, and it is not intended that instruction or hint relative importance Or the implicit quantity for indicating indicated technical characteristic.Define " first " as a result, the feature of " second " can be expressed or Implicitly include one or more this feature." multiple " are meant that two or two in the description of the present invention, More than, unless otherwise specifically defined.
It please refers to shown in attached drawing 1, in the utility model embodiment, provides a kind of reaction kettle, including reaction cavity 10, even It the feed inlet for being connected on 10 upper end of reaction cavity, the rate controlling component 20 connected with the feed inlet and is connected on the reaction cavity 10 Temperature control component 30 and be connected to the discharge component 40 of 10 bottom outside of reaction cavity and mixing component 50.The feed inlet For the addition reaction raw materials in reaction cavity 10, which is used to control adding speed and the addition of the reflection raw material Amount, this process can pass through procedure auto-control;The temperature control component 30 is used to control the temperature in the reaction cavity 10 quick Variation, and then the efficiency of reaction is improved, and can realize being quickly cooled down for reaction cavity 10.The discharge component 40 is used to quickly go out Material avoids the overreaction in reaction cavity 10 of the raw material after reaction.The setting of the mixing component 50 can accelerate the mistake of reaction Journey, and ensure the quality higher of reaction.The temperature control component 30 includes the passage of heat 11 for being attached at 10 inner wall of reaction cavity It is used to drive the fluid in the passage of heat 11 quick with the circulating pump 30a being connected on the passage of heat 11, circulating pump 30a Mobile heat exchange, can accelerate the process for heating up or cooling down, the efficiency for promoting reaction avoids overreaction simultaneously in this way.The discharging Component 40 includes discharging pump 40a and the material storing box 45 for connecting discharging pump 40a.Discharging pump 40a can will react the original completed Material is rapidly extracted out and is transferred in material storing box 45, so as to ensure the purity of reaction raw materials.
The reaction kettle designed above by connecting rate controlling component 20 on feed inlet, and then can automatically control charging Speed and the quantity of charging, the error of reaction result caused by so as to avoid hand feed;The setting of temperature control component 30 can simultaneously To heat or heat during the reaction, and then the control of temperature is more flexible to reaction cavity 10 in advance, And the cooling of reaction cavity 10 can be rapidly realized by the cooperation of circulating pump 30a and passage of heat 11, avoids cooling not Overreact caused by time;And 10 bottom of reaction cavity connection discharging pump 40a and material storing box 45, so as to realize as soon as possible Stoste after reaction detaches, and then avoids the purity and quality of overreaction influence stoste.
Specifically, as shown in Figure 1, in the utility model embodiment, which includes being arranged on the reaction cavity 10 The feeding-in solid body mouth 14 on top and liquid inlet opening 15, the feeding-in solid body mouth 14 and liquid inlet opening 15 set up separately in the reaction cavity The both ends on 10 tops, the rate controlling component 20 are connected on the liquid inlet opening 15, so as to more precisely control liquid into Enter to the speed and quantity in reaction cavity 10.
Specifically, as shown in Figure 1, in the utility model embodiment, the rate controlling component 20 include be connected to the liquid into Connecting tube 21 in material mouth 15 is connected to the rate controlling valve of the connecting tube 21 and is connected to the syringe pump 20a of the connection pipe end.
In the present embodiment, which is preferably solenoid valve, and passes through controller and controlled, and then can be selected not The same different flow entered in reaction cavity 10, syringe pump 20a react stoste for quantitatively providing;So that reaction The dosage of raw material is more accurate, it is easier to control.
Specifically, as shown in Figure 1, in the utility model embodiment, flowing has conductive fluid in the passage of heat 11, and is somebody's turn to do Inlet 13 and liquid outlet 12 are further opened on the side wall of reaction cavity 10, which connects this with the liquid outlet 12 and follow Ring pumps 30a.
In the present embodiment, circulating pump 30a is preferably connected to the outside of the reaction cavity 10, and the circulating pump The both ends of 30a are connected respectively by the connecting tube of heat preservation with inlet 13 and liquid outlet 12;By the driving of circulating pump 30a, make It obtains the conductive fluid to circulate in the passage of heat 11, so as to which the reaction raw materials in reaction cavity 10 be heated.
Specifically, as shown in Figure 1, in the utility model embodiment, which is located at the lower section of the liquid outlet 12. What the inlet 13 entered is the conductive fluid of high temperature, after conductive fluid flows through entire passage of heat 11 from the bottom to top, from top Liquid outlet 12 flows out, and design in this way can ensure the more efficient of heat conduction.
Specifically, as shown in Figure 1, in the utility model embodiment, the company between the inlet 13 and circulating pump 30a It takes over as the first connecting tube 32, the connecting tube connected between the liquid outlet 12 and circulating pump 30a is the second connecting tube 31, this The first check valve is also associated in one connecting tube 32, the second check valve is also associated in second connecting tube 31.This is first unidirectional Valve and the second check valve can prevent conductive fluid from flowing backwards, while after completion of the reaction, and inlet 13 stops feed liquor, circulating pump Conductive fluid in 30a driving passage of heat 11 is quickly flowed out from liquid outlet 12, so that the temperature in reaction cavity 10 Rapid drawdown, so as to prevent the reaction being deposited in reaction cavity 10 stoste from quality problems occur by transient response.
Specifically, as shown in Figure 1, in the utility model embodiment, discharging pump 40a is the anti-acid and alkali pumps of industry, and 10 bottom of reaction cavity is in funnel-form, in this way the outflow convenient for reaction stoste, between discharging pump 40a and the reaction cavity 10 Discharge nozzle 41 is also associated with, the top of the discharge nozzle 41 connects the bottom of the reaction cavity 10.Design can equally be protected in this way Stoste in card reaction cavity 10 can flow out faster.
Specifically, as shown in Figure 1, in the utility model embodiment, total baiting valve 42 is also associated on the discharge nozzle 41, Triple valve is additionally provided in discharging pump 40a, one end of the triple valve connects the discharge nozzle 41, and one end connects the material storing box 45, separately One end connects ash can (not shown), and the first shut-off valve 44, the discharging pump are equipped between discharging pump 40a and the material storing box 45 The second shut-off valve 43 is equipped between 40a and the ash can.
In the present embodiment, the setting of the triple valve can so that the flow direction of stoste is clearer and more definite, while discharging pump 40a is set Putting can ensure that stoste can quickly be flowed into material storing box 45 out of reaction cavity 10, in order to subsequent use.And this is useless The setting of hopper can be in order to the cleaning of late phase reaction cavity 10.
Specifically, as shown in Figure 1, in the utility model embodiment, the level height of the material storing box 45 is higher than the reaction The level height of 10 bottom of cavity.Since traditional reaction cavity 10 is to automatically flow into material storing box by gravity stoste 45, the height of material storing box 45 is limited in this way so that and subsequent use and operation are more inconvenient, and the application designs in this way, Just do not have to limitation material storing box 45 to have in the lower section of reaction cavity 10.
Specifically, as shown in Figure 1, in the utility model embodiment, which includes being connected to the reaction chamber Driving motor 51 on body 10, the drive shaft 52 being connected on the driving motor 51 and the stirring for being connected to 52 end of drive shaft Device 53, the drive shaft 52 are located at the centre of the reaction cavity 10.It can be designed so that the stirring of the mixing component 50 so more It is uniform.
In the present embodiment, the 53 preferred multilayer of blender is along the outwardly extending stirring bar in 52 surface of drive shaft, and And between the adjacent two layers stirring bars there are certain gap, while the drive shaft 52 is also both preferably with stirring bar and connects this Passage of heat 11;Design can be in order to more uniformly heating the reaction raw materials in reaction cavity 10 in this way.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this All any modification, equivalent and improvement made within the spirit and principle of utility model etc., should be included in the utility model Protection domain within.

Claims (10)

1. a kind of reaction kettle, it is characterised in that:Including reaction cavity, it is connected to feed inlet and the institute of the reaction cavity upper end It states the rate controlling component of feed inlet connection and is connected to the temperature on the reaction cavity and for controlling the reaction chamber body temperature It controls component and is connected to the reaction cavity bottom and is used to accelerate the discharge component of discharging and is connected to the reaction cavity The mixing component of reaction is gone up and is used to accelerate, the temperature control component includes the passage of heat being attached on the reaction cavity inner wall With the circulating pump being connected on the passage of heat, the circulating pump is used to that the fluid in the passage of heat to be driven quickly to move Heat exchange, to accelerate to heat up or cool down;The discharge component includes discharging pump and the material storing box for connecting the discharging pump, with as soon as possible Realize that the stoste after reaction detaches.
2. reaction kettle as described in claim 1, it is characterised in that:The feed inlet includes being arranged on the reaction cavity top Feeding-in solid body mouth and liquid inlet opening, rate controlling component connection is on the liquid inlet opening.
3. reaction kettle as claimed in claim 2, it is characterised in that:The rate controlling component includes being connected to the liquid inlet opening On connecting tube, the rate controlling valve that is connected in the connecting tube and the syringe pump for being connected to the connection pipe end.
4. reaction kettle as described in claim 1, it is characterised in that:Flowing has conductive fluid, the reaction in the passage of heat Inlet and liquid outlet are further opened on the side wall of cavity, the inlet connects the circulating pump with the liquid outlet.
5. reaction kettle as claimed in claim 4, it is characterised in that:The inlet is located at the lower section of the liquid outlet.
6. reaction kettle as claimed in claim 4, it is characterised in that:First is connected between the inlet and the circulating pump Connecting tube is connected with the second connecting tube between the liquid outlet and the circulating pump, is also associated in first connecting tube One check valve is also associated with the second check valve in second connecting tube.
7. reaction kettle as described in claim 1, it is characterised in that:The discharging pump is the anti-acid and alkali pumps of industry, and the reaction Cavity bottom is in funnel-form, and discharge nozzle, the top of the discharge nozzle are also associated between the discharging pump and the reaction cavity Connect the bottom of the reaction cavity.
8. reaction kettle as claimed in claim 7, it is characterised in that:Be also associated with total baiting valve on the discharge nozzle, it is described go out Triple valve is additionally provided in material pump, one end of the triple valve connects the discharge nozzle, and one end connects the material storing box, and the other end connects Logical ash can, is equipped with the first shut-off valve, between the discharging pump and the ash can between the discharging pump and the material storing box Equipped with the second shut-off valve.
9. such as claim 1-8 any one of them reaction kettles, it is characterised in that:The level height of the material storing box is higher than described The level height of reaction cavity bottom.
10. such as claim 1-8 any one of them reaction kettles, it is characterised in that:The mixing component includes being connected to described Driving motor on reaction cavity, the drive shaft being connected on the driving motor and the stirring for being connected to the driving shaft end Device, the drive shaft are located at the centre of the reaction cavity.
CN201721087046.7U 2017-08-28 2017-08-28 A kind of reaction kettle Active CN207507451U (en)

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CN201721087046.7U CN207507451U (en) 2017-08-28 2017-08-28 A kind of reaction kettle

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Application Number Priority Date Filing Date Title
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CN207507451U true CN207507451U (en) 2018-06-19

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107456937A (en) * 2017-08-28 2017-12-12 珠海纳金科技有限公司 A kind of reactor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107456937A (en) * 2017-08-28 2017-12-12 珠海纳金科技有限公司 A kind of reactor

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