CN207193165U - For synthesizing the device of peptide resin washing - Google Patents
For synthesizing the device of peptide resin washing Download PDFInfo
- Publication number
- CN207193165U CN207193165U CN201720958040.6U CN201720958040U CN207193165U CN 207193165 U CN207193165 U CN 207193165U CN 201720958040 U CN201720958040 U CN 201720958040U CN 207193165 U CN207193165 U CN 207193165U
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- funnel
- liquid
- peptide resin
- tank
- resin washing
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- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
Abstract
The utility model provides a kind of device for being used to synthesize peptide resin washing, including liquid-adding device, funnel device and the collection device being sequentially connected；The liquid-adding device includes liquid feeding tank, and the collection device includes collecting tank, and the funnel device includes funnel, wherein, the charging aperture of the funnel connects with liquid feeding tank, and the discharging opening of the funnel connects with collecting tank；Air inlet pipe and agitator are provided with the charging aperture of the funnel, the discharge outlet of the funnel is provided with valve.The utility model has the following advantages that：Enclosed system：The process entirely exposed in the past is carried out closed, it is therefore prevented that the volatilization of liquid, substantially improve environment；Pipeline：Whole reaction process is connected by pipeline, reaction is carried out continuously and is not interrupted because toppling over waste liquid, operating personnel is it also avoid and is contacted with the excessive of harmful liquid, improve security；Automation：By peristaltic pump, valve, automatic stirrer makes operation realize automation, reduces human resources.
Description
Technical field
Biochemical products washing field is the utility model is related to, in particular it relates to a kind of dress for being used to synthesize peptide resin washing
Put.
Background technology
Resin washing is that final step is also a very important step in cut-out is reacted.Resin washing mainly removes anti-
The impurity such as trifluoroacetic acid of residual in answering.Existing resin washing technology is exactly the amplification of laboratory Suction filtration device.Pass through sand mold
Funnel, bottle,suction, circulator bath pump carry out filtering and washing.Whole process is all pure manual operations.What it is due to processing is to be harmful to easily to wave
Lotion body, thus it is very big to contamination, while operating safety risks be present, bottle,suction volume not enough will often topple over useless
Liquid has an impact to the continuity of reaction, and the working time is long big to the infringement of circulator bath pump.
Utility model content
For in the prior art the defects of, the purpose of this utility model be to provide it is a kind of be used for synthesize peptide resin washing dress
Put.
According to a kind of device for being used to synthesize peptide resin washing provided by the utility model, including the liquid feeding dress being sequentially connected
Put, funnel device and collection device；
The liquid-adding device includes liquid feeding tank, and the collection device includes collecting tank, and the funnel device includes funnel, its
In, the charging aperture of the funnel connects with liquid feeding tank, and the discharging opening of the funnel connects with collecting tank；
Air inlet pipe and agitator are provided with the charging aperture of the funnel, the discharge outlet of the funnel is provided with valve.
Preferably, the liquid feeding tank is connected by feed tube with the charging aperture of funnel；The collecting tank by discharging tube with
The discharging opening connection of funnel.
Preferably, one end of the feed tube is connected by pump with liquid feeding tank, and other end shunting is provided with grading several times
Liquid pipe；
One end of the discharging tube is connected with collecting tank, and the other end is connected with buffer tank.
Preferably, the funnel device includes some funnels being set up in parallel, the charging aperture of each funnel and the secondary
Feed tube is connected, and the discharging opening of each funnel is connected by secondary discharging tube with the buffer tank；The number of the secondary discharging tube
Amount is consistent with the quantity of secondary feed tube.
Preferably, the valve is arranged on the secondary discharging tube.
Preferably, the funnel upper end is provided with top cover, and the air inlet pipe and agitator are arranged on top cover.
Preferably, it is provided with pressure gauge at the charging aperture of the funnel.
Preferably, the discharging opening of the funnel is connected by buffer tank with collecting tank, and the buffer tank is arranged on fixed branch
On support.
Preferably, the universal wheel of subsidiary brake gear is provided with the fixing support rack.
The utility model makes whole washing process link together, and the closed progress of whole process, realizes automation, uses
When feed tube and discharging tube are connected with funnel, by controlling pump come automatic liquid-feeding, carried out by the way of down blowing
Filtering, each funnel can control reaction process by valve, be arranged by agitator come mixed solution, waste liquid by the way that discharging tube is unified
Put to waste collecting device.
Compared with prior art, the utility model has following beneficial effect：
1st, enclosed system：The process entirely exposed in the past is carried out closed, it is therefore prevented that the volatilization of liquid, substantially improve
Environment.
2nd, pipeline：Whole reaction process is connected by pipeline, reaction is carried out continuously not because toppling over
Waste liquid and interrupt, while avoid the excessive of operating personnel and harmful liquid and contact, improve security.
3rd, automate：By peristaltic pump, valve, automatic stirrer makes operation realize automation, reduces human resources.
Brief description of the drawings
By reading the detailed description made with reference to the following drawings to non-limiting example, other spies of the present utility model
Sign, objects and advantages will become more apparent upon：
Fig. 1 is the schematic diagram that the utility model is used to synthesize the device of peptide resin washing；
It is discharging tube 1, funnel 2, agitator 3, air inlet pipe 4, pressure gauge 5, feed tube 6, pump 7, valve 8, collecting tank 9, solid in figure
Determine support frame 10, liquid feeding tank 11, secondary feed tube 12, secondary discharging tube 13, buffer tank 14, top cover 15.
Embodiment
The utility model is described in detail with reference to specific embodiment.Following examples will be helpful to this area
Technical staff further understands the utility model, but does not limit the utility model in any form.It should be pointed out that to ability
For the those of ordinary skill in domain, without departing from the concept of the premise utility, some changes and improvements can also be made.
These belong to the scope of protection of the utility model.
The utility model provides a kind of device for being used to synthesize peptide resin washing, as shown in figure 1, including being sequentially connected
Liquid-adding device, funnel device and collection device；The liquid-adding device includes liquid feeding tank 11, and the collection device includes collecting tank 9,
The funnel device includes funnel 2, and the charging aperture of the funnel 2 connects with liquid-adding device, the discharging opening of the funnel 2 and collection
Device connects；Air inlet pipe 4 and agitator 3 are provided with the charging aperture of the funnel 2, the discharge outlet of the funnel 2 is provided with
Valve 8.The collection device is waste collecting device, and the collecting tank 9 is used for the collection of waste liquid.
The liquid feeding tank 11 is connected by feed tube 6 with the charging aperture of funnel 2；The collecting tank 9 passes through discharging tube 1 and leakage
The discharging opening connection of bucket 2.
One end of the feed tube 6 is connected by pump 7 with liquid feeding tank 11, and other end shunting is provided with level feed tube several times
12；One end of the discharging tube 1 is connected with collecting tank 9, and the other end is connected with buffer tank 14.
The funnel device includes some funnels 2 being set up in parallel, the charging aperture of each funnel 2 and the secondary feed tube
12 connections, the discharging opening of each funnel 2 are connected by secondary discharging tube 13 with the buffer tank 14；The secondary discharging tube 13
Quantity is consistent with the quantity of secondary feed tube 12.As illustrated in fig. 1, it is preferred that the funnel 2 of 3 is set side by side with funnel device,
Meanwhile the quantity of secondary discharging tube 13 and secondary feed tube 12 is also 3.
The valve 8 is arranged on the secondary discharging tube 13.The secondary discharging tube 13 plays the support to funnel 2 simultaneously
Effect is fixed.
The upper end of funnel 2 is provided with top cover 15, and the air inlet pipe 4 and agitator 3 are arranged on top cover 15.It is described to stir
It can be automatic stirrer to mix device.One end of the air inlet pipe 4 is arranged on top cover 15, and other end connection nitrogen mouth, nitrogen mouth has
Nitrogen pressure control valve, the pressure size in funnel can be controlled by control valve.
Pressure gauge 5 is provided with the charging aperture of the funnel 2.
The discharging opening of the funnel 2 is connected by buffer tank 14 with collecting tank 9, and the buffer tank 14 is arranged on fixed support
On frame 10.The fixing support rack 10 installs the universal wheel of subsidiary brake gear additional.
By the utility model carry out synthesize peptide resin wash concrete operation step be：
(1) liquid feeding:The resin liquid that will be washed is placed in liquid feeding tank, is added resin liquid in each funnel by peristaltic pump
(flow that liquid feeding can be controlled by rotating speed).
(2) washing process:After the completion of liquid feeding, opening air inlet is passed through nitrogen and carries out blowing filter washing for the first time, and waste liquid passes through
The discharge of pipes connected under funnel is to waste collecting device.There is valve individually to control filter wash process below each funnel.
Resin has been dissolved after the completion of washing for the first time by agitator by the quantitative addition cleaning solution of peristaltic pump by liquid feeding tank
Entirely, it is passed through nitrogen and is blown filter for the second time.(liquid volume added can pass through wriggling at any time to the secondary step of washing repetition every time later
Pump controls).Washing times are determined by washing situation, until washing is completed.
It is provided by the utility model it is a kind of be used for synthesize peptide resin washing device, package unit mainly by liquid-adding device,
Funnel device, waste collecting device three parts composition.Wherein, the funnel device includes funnel, top cover, pressure gauge, automatic stirring
Mix device, air inlet, inlet, valve, fixing device (universal wheel for installing subsidiary brake gear additional)；Liquid feeding is controlled automatically by pump
System.
The device makes whole washing process link together, the closed progress of whole process, realizes automation, will during use
Feed tube and discharging tube connect with funnel, by controlling pump come automatic liquid-feeding, are filtered by the way of down blowing,
Each funnel can control reaction process by valve, by agitator come mixed solution, waste liquid by discharging tube uniform effluent extremely
Waste collecting device.
Specific embodiment of the utility model is described above.It is to be appreciated that the utility model not office
It is limited to above-mentioned particular implementation, those skilled in the art can make a variety of changes or change within the scope of the claims,
This has no effect on substantive content of the present utility model.In the case where not conflicting, the spy in embodiments herein and embodiment
Sign can be arbitrarily mutually combined.
Claims (9)
1. a kind of device for being used to synthesize peptide resin washing, it is characterised in that including liquid-adding device, the funnel device being sequentially connected
And collection device；
The liquid-adding device includes liquid feeding tank (11), and the collection device includes collecting tank (9), and the funnel device includes funnel
(2), wherein, the charging aperture of the funnel (2) connects with liquid feeding tank (11), and discharging opening and the collecting tank (9) of the funnel (2) connect
It is logical；
Air inlet pipe (4) and agitator (3) are provided with the charging aperture of the funnel (2), the discharge outlet of the funnel (2) is set
There is valve (8).
2. the device according to claim 1 for being used to synthesize peptide resin washing, it is characterised in that the liquid feeding tank (11) is logical
The charging aperture that feed tube (6) is crossed with funnel (2) connects；The collecting tank (9) passes through discharging tube (1) and the discharging opening of funnel (2)
Connection.
3. the device according to claim 2 for being used to synthesize peptide resin washing, it is characterised in that the feed tube (6)
One end is connected by pump (7) with liquid feeding tank (11), and other end shunting is provided with level feed tube (12) several times；
One end of the discharging tube (1) is connected with collecting tank (9), and the other end is connected with buffer tank (14).
4. the device according to claim 3 for being used to synthesize peptide resin washing, it is characterised in that the funnel device includes
Some funnels (2) being set up in parallel, the charging aperture of each funnel (2) are connected with the secondary feed tube (12), each funnel (2)
Discharging opening be connected by secondary discharging tube (13) with the buffer tank (14)；The quantity of the secondary discharging tube (13) and secondary
The quantity of feed tube (12) is consistent.
5. the device according to claim 4 for being used to synthesize peptide resin washing, it is characterised in that the valve (8) is arranged on
On the secondary discharging tube (13).
6. the device according to claim 1 for being used to synthesize peptide resin washing, it is characterised in that funnel (2) upper end
Top cover (15) is provided with, the air inlet pipe (4) and agitator (3) are arranged on top cover (15).
7. the device according to claim 1 for being used to synthesize peptide resin washing, it is characterised in that funnel (2) are entered
Pressure gauge (5) is provided with material mouth.
8. the device according to claim 1 for being used to synthesize peptide resin washing, it is characterised in that funnel (2) go out
Material mouth is connected by buffer tank (14) with collecting tank (9), and the buffer tank (14) is arranged on fixing support rack (10).
9. the device according to claim 8 for being used to synthesize peptide resin washing, it is characterised in that the fixing support rack
(10) universal wheel of subsidiary brake gear is provided with.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720958040.6U CN207193165U (en) | 2017-08-02 | 2017-08-02 | For synthesizing the device of peptide resin washing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720958040.6U CN207193165U (en) | 2017-08-02 | 2017-08-02 | For synthesizing the device of peptide resin washing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207193165U true CN207193165U (en) | 2018-04-06 |
Family
ID=61796110
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720958040.6U Active CN207193165U (en) | 2017-08-02 | 2017-08-02 | For synthesizing the device of peptide resin washing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207193165U (en) |
-
2017
- 2017-08-02 CN CN201720958040.6U patent/CN207193165U/en active Active
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