CN207108740U - A kind of purifier based on WinCC control programs - Google Patents
A kind of purifier based on WinCC control programs Download PDFInfo
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- CN207108740U CN207108740U CN201720386133.6U CN201720386133U CN207108740U CN 207108740 U CN207108740 U CN 207108740U CN 201720386133 U CN201720386133 U CN 201720386133U CN 207108740 U CN207108740 U CN 207108740U
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- water
- wincc
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- control
- control case
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- 238000001914 filtration Methods 0.000 claims abstract description 53
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- 238000005086 pumping Methods 0.000 claims abstract description 29
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 27
- 241000894006 Bacteria Species 0.000 claims abstract description 23
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 230000000249 desinfective effect Effects 0.000 claims abstract description 16
- 238000012544 monitoring process Methods 0.000 claims abstract description 12
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- 238000005374 membrane filtration Methods 0.000 claims description 6
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
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- 239000003431 cross linking reagent Substances 0.000 description 6
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- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
- 230000005260 alpha ray Effects 0.000 description 3
- 125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 description 3
- 239000004305 biphenyl Substances 0.000 description 3
- YMHQVDAATAEZLO-UHFFFAOYSA-N cyclohexane-1,1-diamine Chemical compound NC1(N)CCCCC1 YMHQVDAATAEZLO-UHFFFAOYSA-N 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
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- 230000032050 esterification Effects 0.000 description 3
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- CJGXMNONHNZEQQ-JTQLQIEISA-N ethyl (2s)-2-amino-3-phenylpropanoate Chemical compound CCOC(=O)[C@@H](N)CC1=CC=CC=C1 CJGXMNONHNZEQQ-JTQLQIEISA-N 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 125000005395 methacrylic acid group Chemical group 0.000 description 3
- 239000011812 mixed powder Substances 0.000 description 3
- OIVLDUXIJRSENC-UHFFFAOYSA-N n-(sulfonylamino)aniline Chemical compound O=S(=O)=NNC1=CC=CC=C1 OIVLDUXIJRSENC-UHFFFAOYSA-N 0.000 description 3
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- AIDQCFHFXWPAFG-UHFFFAOYSA-N n-formylformamide Chemical compound O=CNC=O AIDQCFHFXWPAFG-UHFFFAOYSA-N 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
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- 238000012545 processing Methods 0.000 description 3
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- 238000003756 stirring Methods 0.000 description 3
- 229910021642 ultra pure water Inorganic materials 0.000 description 3
- 239000012498 ultrapure water Substances 0.000 description 3
- RFVNOJDQRGSOEL-UHFFFAOYSA-N 2-hydroxyethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCO RFVNOJDQRGSOEL-UHFFFAOYSA-N 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000012644 addition polymerization Methods 0.000 description 2
- 235000010290 biphenyl Nutrition 0.000 description 2
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- 229950007687 macrogol ester Drugs 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- UHANVDZCDNSILX-UHFFFAOYSA-N n-phenylbutanamide Chemical compound CCCC(=O)NC1=CC=CC=C1 UHANVDZCDNSILX-UHFFFAOYSA-N 0.000 description 2
- 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 description 2
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 125000001973 tert-pentyl group Chemical group [H]C([H])([H])C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 2
- 238000003466 welding Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
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- 239000007789 gas Substances 0.000 description 1
- 150000002429 hydrazines Chemical class 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- DNHVXYDGZKWYNU-UHFFFAOYSA-N lead;hydrate Chemical compound O.[Pb] DNHVXYDGZKWYNU-UHFFFAOYSA-N 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012806 monitoring device Methods 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 229920001515 polyalkylene glycol Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 125000001501 propionyl group Chemical group O=C([*])C([H])([H])C([H])([H])[H] 0.000 description 1
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- 238000000926 separation method Methods 0.000 description 1
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- 238000003860 storage Methods 0.000 description 1
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Landscapes
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The utility model provides a kind of purifier based on WinCC control programs, including water holding tank to be clean, water inlet pumping installations, purification agent set, WinCC programme-control casees.Purification agent set sets gradually by-pass filtration film, secondary filtration film tablet, disinfecting instrument from top to bottom.Launch a large amount of engineering bacterias that purify water in the surface of by-pass filtration film；The treatment effeciency for the engineering bacteria that purifies water is sent to by WinCC programme-control casees by electric signal while secondary filtration film tablet purifies water, WinCC programme-control case is according to electric signal control flow of inlet water.The secondary filtration film tablet that the utility model uses is prepared for high polymer material, and detergent power is strong.Monitoring of Disinfection Efficacy instrument is set simultaneously, to monitoring water quality in real time, and feedback signal is sent to WinCC programme-control case, WinCC programme-control case increases the voltage of disinfecting instrument both sides accordingly.Water purifying apparatus structure provided by the utility model is new reasonable, easy to operate, and purifying property is high, and the purification for being suitable for polytype water uses.
Description
Technical field
The utility model belongs to water correction plant field, and in particular to a kind of purifier based on WinCC control programs.
Background technology
China purification water process career development it is very fast, now in the world, the various techniques and equipment that advanced country uses I
Domestic have.The purifying water treatment device in China is compared with external same category of device, and in technical performance, in energy-conservation, gap is not
It is very big, but commercially, domestic equipment is implicitly present in very big gap compared with external same category of device, because：
1) bid, the bidding work in China are lack of standardization, and the same industry is mutually demanded a lower price, and causes middle target equipment price very low, most
Low tender price, township enterprise equipment can not be compared with external best brand of product.
2) home equipment differs too big with the price of overseas equipment, therefore can not compare.
3) raw material market in China, stainless steel, the section bar specification such as the angle steel of aluminum alloy material, channel-section steel are few, market shortage,
So the heavier-weight of the equipment such as mud scraper, power consumption are bigger.
1991 to 2000, the two stage treatment ability of China's municipal sewage surged to 2753.4 ten thousand from 193.5 ten thousand T/d
T/d, increase more than 14 times.China city purification water treatment business obtained it is unprecedented flourish, tentatively checked me
The situation that state's water environment seriously pollutes.But in huge achievement behind, but in the presence of an indisputable fact：The same period builds large quantities of net
In water chemical treatment factory up to 90% use be import foreign equipment.This has to allow compatriots to be domestic purifying water treatment device
Lose great business opportunity and deeply regret endlessly.Certainly, itself deficiency of domestic enterprise is one of key factor, but country is helped domestic enterprise
It is main reason to hold inadequate and unilateral utilize foreign capital.2000 to 2010, it is contemplated that at the biochemistry of China city purified water
Reason ability will increase to 5639.5 ten thousand T/d from 2753.4 ten thousand T/d, and disposal ability will double, and the purification water process newly increased is total
Amount is also more more than the summation of previous decade.The above situation illustrates that the development of following domestic purifying water treatment device also has very big machine
Meeting, this requires that country draws the experience and lessons of previous decade, adopting an important measure allows domestic purifying water treatment device process industry
Develop growth rapidly.
Existing conventional purifying water treatment device has:Aerating system equipment, block dirty equipment, spoil disposal residue extraction mechanism, separation set
Standby, mixing plant, filter plant, lifting means, sterilizing equipment decontaminating apparatus, various sludge concentrator, sludge screw pump, sludge dewatering equipment,
Sludge dryer, sludge centrifugal separator, sludge composting machinery, sludge incineration machinery, anaerobic sludge digestion gas storage facilities, hair
Electric equipment, water purification plant power supply unit, molten medicine equipment, water quality and quantity monitoring device, control device etc..
Under prior art conditions, the increase for handling the equipment construction cost and operating cost of life purified water will be as must
So, the shortcomings of existing traditional handicraft, processing method have technological process length, and control is complicated, take up an area greatly, and processing cost is high.
Utility model content
For above-mentioned the deficiencies in the prior art, the utility model provides the purifier based on WinCC control programs, device
Rational in infrastructure compact, integrated level is high, and filter membrane tablet is prepared using high polymer material, and detergent power is strong.
To achieve the above object, the utility model adopts the following technical scheme that：
A kind of purifier based on WinCC control programs, including：Water holding tank to be clean, water inlet pumping installations, purification
Agent set, WinCC programme-control casees；The both ends of the water inlet pumping installations are respectively communicated with the delivery port of water holding tank to be clean
With the water inlet of purification agent set；One end of the water inlet pumping installations is the pump connected with the delivery port of purified water holding tank
Power transmission machine, the other end are the water injector for being arranged at top in purification agent set；The pumping motor passes through with water injector
Water inlet manifold connects；The water inlet manifold is provided with feed water flow gauge and current opening and closing electrically-controlled valve；
The purification agent set sets cleaning position, quartz sand disinfection storehouse from top to bottom；The cleaning position from top to bottom according to
Secondary setting by-pass filtration film, secondary filtration film tablet；Disinfecting instrument and Monitoring of Disinfection Efficacy are set in the quartz sand disinfection storehouse
Instrument；Band purified water sprays from water injector, is successively purified through by-pass filtration film, secondary filtration film tablet, disinfecting instrument, Ran Houcong
Purify the delivery port discharge of agent set；
The pumping motor, feed water flow gauge, current opening and closing electrically-controlled valve, water injector, disinfecting instrument, the sensing of secondary filtration film
Plate, Monitoring of Disinfection Efficacy instrument are connected with WinCC programme-control case polygon control surveys respectively, and are controlled by WinCC programme-control case.
Further, the water injector includes the feedwater automatically controlled ring of assignment constraints；It is described feedwater the automatically controlled ring of assignment constraints be in
Rectangular tubular structure, bottom, which is provided with, divides sprinkler head, divides sprinkler head to be uniformly distributed along the automatically controlled side of ring four of feedwater assignment constraints；It is described to give
The automatically controlled ring of water assignment constraints is connected with WinCC programme-control case polygon control surveys, and is controlled by WinCC programme-control case.
Further, the secondary filtration film tablet is made up of the equally distributed W shapes broken line plate of some horizontal directions, W
The opening direction of shape broken line plate is vertical with water (flow) direction；Spacing between adjacent W shapes broken line plate is 7mm~19mm.
Further, the engineering bacteria that purifies water is launched on the surface of the by-pass filtration film.
Further, the secondary filtration film tablet is provided with viable bacteria selection instrument；The viable bacteria selection instrument connection
WinCC programme-control casees；The viable bacteria selection instrument perceives the treatment effeciency for the engineering bacteria that purifies water, when the engineering bacteria that purifies water
Treatment effeciency is less than 15%, then by electric signal, notifies WinCC programme-control case and alarm, WinCC programme-control casees pass through control
Water injector processed and feed water flow gauge reduce the flow of water；When the engineering bacteria that purifies water treatment effeciency be higher than 35%, then pass through
Electric signal, WinCC programme-control casees are notified, WinCC programme-control case is by controlling water injector and feed water flow gauge to increase water
Flow.
Further, fixed support, the fixed support and purification agent set are provided with below the purification agent set
Bottom is welded and fixed, and the fixed support bottom is provided with vibrating sensor, and vibrating sensor connects with WinCC programme-control casees wire
Connect.
Further, the pumping motor and water inlet manifold junction are provided with water quality testing meter, the water quality testing meter and
WinCC programme-control casees wire connects.
Further, the by-pass filtration film gross thickness is not less than 5cm~10cm, is passed in the middle provided with membrane filtration efficiency
Sensor, the membrane filtration efficiency sensor are connected with WinCC programme-control case wires.
The beneficial effects of the utility model are：
1st, the apparatus structure is rationally compact, and integrated level is high；
2nd, the device secondary filtration film tablet is prepared using high polymer material, and detergent power is strong；
3rd, ejecting device is using the automatically controlled ring of feedwater assignment constraints and be uniformly arranged on the feedwater automatically controlled ring of assignment constraints divide water
Shower nozzle so that water to be clean can uniformly flow to filter membrane, and filter membrane utilization rate is high, good filtration effect；
4th, using WinCC programme-control casees, automaticity is high, easy to operate；
5th, filter membrane tablet can perceive the treatment effeciency for the engineering bacteria that purifies water, and notify WinCC by electric signal
Programme-control case, to adjust flow of inlet water in real time, improve filter efficiency.
Brief description of the drawings
Fig. 1 is the purifier schematic diagram described in the utility model.
Fig. 2 is the water inlet pumping apparatus structure schematic diagram described in the utility model.
Fig. 3 is the purification agent set structural representation described in the utility model.
Fig. 4 is secondary filtration film sensing plate material described in the utility model and detergent power enhancing rate graph of a relation.
Fig. 5 is WinCC sequence circuits figure described in the utility model.
In figure 1 above~Fig. 3, water holding tank 1 to be clean, pumping installations 2 of intaking, pumping motor 2-1, water inlet manifold 2-
2, feed water flow gauge 2-3, current opening and closing electrically-controlled valve 2-4, feed water the automatically controlled ring 2-5 of assignment constraints, divides sprinkler head 2-6, purifies main body
Device 3, cleaning position 3-1, by-pass filtration film 3-2, secondary filtration film tablet 3-3, quartz sand disinfection storehouse 3-4, disinfecting instrument 3-5,
Monitoring of Disinfection Efficacy instrument 3-6, clear water delivery pipe 3-7, fixed support 4, WinCC programme-control case 5.
Embodiment
The utility model is further described below in conjunction with the accompanying drawings.
As shown in figure 1, it is a kind of signal of purifier based on WinCC control programs described in the utility model
Figure.Find out in figure, including：Water holding tank 1 to be clean, pumping installations 2 of intaking, purifies agent set 3, fixed support 4, WinCC
Programme-control case 5；The lower section of purification agent set 3 is provided with fixed support 4, the fixed support 4 and purification agent set 3 bottom
Portion is welded and fixed, and the fixed support bottom is provided with vibrating sensor, and the side of fixed support 4 is provided with water holding tank 1 to be clean, institute
State and connected between water holding tank 1 to be clean and purification agent set 3 by pumping installations 2 of intaking, the WinCC programme-control
Case 5 is located at the bottom of fixed support 4.
As shown in Fig. 2 it is the water inlet pumping apparatus structure schematic diagram described in the utility model.From Fig. 2 or Fig. 1
Go out, the water inlet pumping installations 2 includes：Pumping motor 2-1, water inlet manifold 2-2, feed water flow gauge 2-3, current opening and closing electrically-controlled valve
2-4, feed water the automatically controlled ring 2-5 of assignment constraints, divides sprinkler head 2-6；The pumping motor 2-1 is positioned over level ground, pumping motor
2-1 is connected with the polygon control survey of WinCC programme-control case 5；The water inlet manifold 2-2 profiles are in " catapult " shape structure, water inlet manifold
2-2 one end connects pumping motor 2-1, and pumping motor 2-1 tops are provided with water quality testing meter, the water inlet manifold 2-2 other ends connect to
The automatically controlled ring 2-5 of water assignment constraints；The automatically controlled ring 2-5 quantity of the feedwater assignment constraints is 2 groups, the automatically controlled ring 2-5 of feedwater assignment constraints
Rectangular tubular structure, feedwater assignment constraints automatically controlled ring 2-5 bottoms, which are provided with, divides sprinkler head 2-6, described to divide sprinkler head 2-6 nozzle sides
To straight down, dividing sprinkler head 2-6 quantity to be no less than 10 groups, divide sprinkler head 2-6 equal along the automatically controlled sides of ring 2-5 tetra- of feedwater assignment constraints
Even distribution；The water inlet manifold 2-2 is opened and closed electrically-controlled valve 2-4 by supreme feed water flow gauge 2-3 and the current of being sequentially connected in series in bottom, described
Feed water flow gauge 2-3 and current opening and closing electrically-controlled valve 2-4 are connected with the polygon control survey of WinCC programme-control case 5 respectively.
As shown in figure 3, it is the purification agent set structural representation described in the utility model.From Fig. 3 or Fig. 1
Go out, the purification agent set 3 includes：Cleaning position 3-1, by-pass filtration film 3-2, secondary filtration film tablet 3-3, quartz sand disappear
Malicious storehouse 3-4, disinfecting instrument 3-5, Monitoring of Disinfection Efficacy instrument 3-6, clear water delivery pipe 3-7；The cleaning position 3-1 is to be open up and down
Rectangular parallelepiped structure, cleaning position 3-1 be by thickness be 4mm~8mm stainless steel plate bending welding be made；The by-pass filtration film
3-2 is located at cleaning position 3-1 bosoms position, and the walls of by-pass filtration film 3-2 tetra- are adhered to cleaning position 3-1 inner wall surfaces, one-level mistake
Filter membrane 3-2 gross thickness is not less than 5cm~10cm, in the middle provided with membrane filtration efficiency sensor；The secondary filtration film sensing
Plate 3-3 is located at cleaning position 3-1 interior bottom portions position, and secondary filtration film tablet 3-3 is polyline shaped structure, secondary filtration film
Tablet 3-3 quantity is not less than 7~15 groups, and secondary filtration film tablet 3-3 horizontal homogeneous is distributed, adjacent two secondary filtrations film sense
Plate 3-3 spacing is answered between 7mm~19mm；The quartz sand disinfection storehouse 3-4 is located at cleaning position 3-1 bottoms, quartz sand disinfection storehouse
3-4 and cleaning position 3-1 bottom surfaces seamless welding, quartz sand disinfection storehouse 3-4 profiles are in " terrace with edge " shape structure, quartz sand disinfection storehouse 3-4
With being mutually communicated inside cleaning position 3-1；The disinfecting instrument 3-5 is located inside quartz sand disinfection storehouse 3-4, and disinfecting instrument 3-5 quantity is 3
~5 groups, disinfecting instrument 3-5 is evenly distributed vertically, and disinfecting instrument 3-5 both positive and negative polarities connect with the polygon control survey of WinCC programme-control case 5 respectively
Connect；The Monitoring of Disinfection Efficacy instrument 3-6 is located at quartz sand disinfection storehouse 3-4 inner wall surfaces, Monitoring of Disinfection Efficacy instrument 3-6 and WinCC
The polygon control survey of programme-control case 5 connects；The clear water delivery pipe 3-7 is located at quartz sand disinfection storehouse 3-4 bottoms, clear water delivery pipe 3-
7 connect with quartz sand disinfection storehouse 3-4, membrane filtration efficiency sensor, the electrically-controlled valve and WinCC programs on clear water delivery pipe 3-7 surfaces
The polygon control survey of control cabinet 5 connects.
A kind of process for purifying water described in the utility model is：
1st step：WinCC programme-control case 5 controls pumping motor 2-1 to be in starting state, and pumping motor 2-1 will be to be clean
Water pump to be clean is delivered in the automatically controlled ring 2-5 of feedwater assignment constraints in water holding tank 1, then passes through the automatically controlled ring 2- of the assignment constraints that feed water
What 5 bottoms were provided with divides the uniform spray feeds of sprinkler head 2-6 into cleaning position 3-1；In pumping procedure, feed water flow gauge 2-3 control water
Range of flow value is in 20m3/ h~50m3Between/h；
2nd step：Rate firstly flows through by-pass filtration film 3-2, by-pass filtration film 3-2 by water to be clean to water to be clean from the top down
Bulky grain suspended solid is adsorbed on its surface, while a large amount of engineering bacterias that purify water, purification are launched on by-pass filtration film 3-2 surfaces
Water quality engineering bacteria carries out redox processing to the bulky grain suspended solid of by-pass filtration film 3-2 adsorptions；
3rd step：Water to be clean after above-mentioned steps are handled continues to flow through downwards secondary filtration film tablet 3-3, two level
The indissoluble dissolved organic matter of the engineering bacteria that purifies water that filter membrane tablet 3-3 is treated in purified water carries out secondary purifying
Change；
4th step：Water to be clean continues to flow in quartz sand disinfection storehouse 3-4 downwards, while WinCC programme-control case 5 is opened
The disinfecting instrument 3-5 being provided with quartz sand disinfection storehouse 3-4 carries out disinfection processing to the bacterium that is remained in water and pathogen；Sterilizing
Cheng Zhong, Monitoring of Disinfection Efficacy instrument 3-6 detects the content value of bacterium and pathogen in water in real time, when bacterium and the content value of pathogen
During more than preset value, Monitoring of Disinfection Efficacy instrument 3-6 sends feedback signal, WinCC programme-control casees to WinCC programme-control case 5
The magnitude of voltage at 5 increase disinfecting instrument 3-5 both ends；
5th step：WinCC programme-control case 5 opens the electrically-controlled valve on clear water delivery pipe 3-7 surfaces, it is sterilized after clear water lead to
Cross clear water delivery pipe 3-7 discharge whole equipments.
A kind of quartzy sand filter water purifying apparatus structure based on WinCC control programs described in the utility model is novel to be closed
Reason, easy to operate, purifying property is high, and the purification for being suitable for polytype water uses.
The embodiment of secondary filtration film tablet 3-3 described in the utility model manufacturing process below, embodiment be for
Further explanation content of the present utility model, but should not be construed as to limitation of the present utility model.New without departing substantially from this practicality
In the case of type spirit and essence, the modification and replacement made to the utility model method, step or condition, this practicality is belonged to
New scope.
Unless otherwise specified, the conventional meanses that technological means used in embodiment is well known to those skilled in the art.
Embodiment 1
Secondary filtration film tablet 3-3 described in the utility model, and fraction meter by weight are manufactured according to following steps：
1st step：300 parts of the ultra-pure water that electrical conductivity is 1.10 μ S/cm is added in a kettle, is started in reactor and is stirred
Device, rotating speed 110rpm, start heat pump, reactor temperature is risen to 70 DEG C；Addition polymerization ethylene glycol-polymethyl successively
70 parts of sour N, N- dimethylaminoethyl-polycaprolactone, 90 parts of polymethylacrylic acid N, N- dimethylaminoethyl-polycaprolactone, first
130 parts of base polyalkylene glycol acrylate ester, to being completely dissolved, regulation pH value is 1.0, and agitator speed is adjusted into 110rpm for stirring,
Temperature is 110 DEG C, esterification 10 hours；
2nd step：Take 90 parts of poly- (acrylic acid-co- methyl methacrylates), methacrylic acid-N, N- dimethylaminoethyl
80 parts are crushed, and powder diameter is 50 mesh；Add N, two hydrazine of N'- bis- (4- substituted benzoyls) decanedioyl, 130 parts of mixing are
It is even, it is laid in pallet, tiling thickness is 10mm, and the alpha ray for using dosage to be 1.0MeV for 1.0kGy, energy irradiates 10 points
Clock, and the β x ray irradiation xs 80 minutes of Isodose；
3rd step：The mixed-powder handled through the 2nd step is dissolved in the 4- (2-N, N- dimethylamino-ethyl) that concentration is 30ppm
In 80 parts of sulfonyl-phenylhydrazine, reactor, agitator speed 90rpm are added, temperature is 100 DEG C, and starting vavuum pump makes reactor
Vacuum reach -0.30MPa, keep this state response 10 hours；Pressure release is simultaneously passed through nitrogen, makes the reacting kettle inner pressure be
0.20MPa, insulation stand 10 hours；Agitator speed is promoted to 100rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add
Double (the 5- tert-butyl groups -3- formoxyls -4-HBA methyl esters) 70 parts of the contracting cyclohexanediamine of (1R, 2R)-N, N'-, the 4- tert-butyl groups -
After 70 parts of 4'- methoxy dibenzoyl methanes are completely dissolved, add 90 parts of crosslinking agent and be stirred so that the parent of reactor solution
Hydrophile-lipophile balance value is 2.0, and insulation stands 10 hours；
4th step：When agitator speed is 100rpm, L-2- (the tertiary fourth oxygen acyl groups of N-) -3', 4'- dimethoxies are sequentially added
30 parts of base phenylalanine ethyl ester, N, N'-1,6- dihexyls two [3- tertiary butyl-4-hydroxy -5- methyl] 110 parts of hydrocinnamamide, N ' -
Diphenyl is along 30 parts of fourth diformamide, 4- [(1- butyl -5- cyano group -1,2- dihydro -6- hydroxy-4-methyl -2- oxo -3- pyridines
Base) azo] 30 parts of-N- (2- ethylhexyls) benzsulfamide, reactor pressure is lifted, reaches 0.90MPa, temperature is
100 DEG C, polymerisation 10 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, 10 DEG C is cooled to, discharging, enters pressing mold
Machine can be prepared by secondary filtration film tablet 3-3；
The crosslinking agent is 2- [double (1,1- dimethyl propyls) phenoxy groups of 2,4-] chloro- 4'- ethyls -2'- hydroxyls of -3', 5'- bis-
Base butyranilide.
Embodiment 2
Secondary filtration film tablet 3-3 described in the utility model, and fraction meter by weight are manufactured according to following steps：
1st step：1200 parts of the ultra-pure water that electrical conductivity is 1.80 μ S/cm is added in a kettle, is started in reactor and is stirred
Device, rotating speed 120rpm, start heat pump, reactor temperature is risen to 90 DEG C；Successively plus polyethylene glycol methyl-prop
130 parts of olefin(e) acid N, N- dimethylaminoethyl-polycaprolactone, polymethylacrylic acid N, N- dimethylaminoethyl-polycaprolactone 130
Part, 330 parts of methacrylic acid macrogol ester, to being completely dissolved, regulation pH value is 8.0, and agitator speed is adjusted to for stirring
220rpm, temperature are 170 DEG C, esterification 30 hours；
2nd step：Take 140 parts of poly- (acrylic acid-co- methyl methacrylates), methacrylic acid-N, N- dimethylaminoethyl
130 parts are crushed, and powder diameter is 120 mesh；Add N, two hydrazine of N'- bis- (4- substituted benzoyls) decanedioyl, 350 parts of mixing are
It is even, it is laid in pallet, tiling thickness is 40mm, and the alpha ray for using dosage to be 5.0MeV for 9.0kGy, energy irradiates 40 points
Clock, and the β x ray irradiation xs 170 minutes of Isodose；
3rd step：The mixed-powder handled through the 2nd step is dissolved in the 4- (2-N, N- dimethylamino-ethyl) that concentration is 120ppm
In 130 parts of sulfonyl-phenylhydrazine, reactor, agitator speed 190rpm are added, temperature is 140 DEG C, and starting vavuum pump makes reaction
The vacuum of kettle reaches -0.90MPa, keeps this state response 30 hours；Pressure release is simultaneously passed through nitrogen, makes the reacting kettle inner pressure be
0.80MPa, insulation stand 30 hours；Agitator speed is promoted to 200rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add
Double (the 5- tert-butyl groups -3- formoxyls -4-HBA methyl esters) 130 parts of the contracting cyclohexanediamine of (1R, 2R)-N, N'-, the 4- tert-butyl groups -
After 180 parts of 4'- methoxy dibenzoyl methanes are completely dissolved, add 130 parts of crosslinking agent and be stirred so that reactor solution
Hydrophilic lipophilic balance is 8.0, and insulation stands 30 hours；
4th step：When agitator speed is 170rpm, L-2- (the tertiary fourth oxygen acyl groups of N-) -3', 4'- dimethoxies are sequentially added
130 parts of base phenylalanine ethyl ester, N, N'-1,6- dihexyls two [3- tertiary butyl-4-hydroxy -5- methyl] 180 parts of hydrocinnamamide,
N '-diphenyl is along 90 parts of fourth diformamide, 4- [(1- butyl -5- cyano group -1,2- dihydro -6- hydroxy-4-methyl -2- oxos -3-
Pyridine radicals) azo] 170 parts of-N- (2- ethylhexyls) benzsulfamide, reactor pressure is lifted, reaches 1.70MPa, temperature
For 180 DEG C, polymerisation 30 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, 20 DEG C is cooled to, discharging, enters pressure
Mould machine can be prepared by secondary filtration film tablet 3-3；
The crosslinking agent is 2- [double (1,1- dimethyl propyls) phenoxy groups of 2,4-] chloro- 4'- ethyls -2'- hydroxyls of -3', 5'- bis-
Base butyranilide.
Embodiment 3
Secondary filtration film tablet 3-3 described in the utility model, and fraction meter by weight are manufactured according to following steps：
1st step：900 parts of the ultra-pure water that electrical conductivity is 1.50 μ S/cm is added in a kettle, is started in reactor and is stirred
Device, rotating speed 115rpm, start heat pump, reactor temperature is risen to 80 DEG C；Addition polymerization ethylene glycol-polymethyl successively
120 parts of sour N, N- dimethylaminoethyl-polycaprolactone, 110 parts of polymethylacrylic acid N, N- dimethylaminoethyl-polycaprolactone,
230 parts of methacrylic acid macrogol ester, to being completely dissolved, regulation pH value is 6.0, and agitator speed is adjusted to for stirring
150rpm, temperature are 130 DEG C, esterification 20 hours；
2nd step：Take 110 parts of poly- (acrylic acid-co- methyl methacrylates), methacrylic acid-N, N- dimethylaminoethyl
100 parts are crushed, and powder diameter is 70 mesh；Add N, two hydrazine of N'- bis- (4- substituted benzoyls) decanedioyl, 250 parts of mixing are
It is even, it is laid in pallet, tiling thickness is 30mm, and the alpha ray for using dosage to be 3.0MeV for 6.0kGy, energy irradiates 20 points
Clock, and the β x ray irradiation xs 110 minutes of Isodose；
3rd step：The mixed-powder handled through the 2nd step is dissolved in the 4- (2-N, N- dimethylamino-ethyl) that concentration is 70ppm
In 110 parts of sulfonyl-phenylhydrazine, reactor, agitator speed 120rpm are added, temperature is 130 DEG C, and starting vavuum pump makes reaction
The vacuum of kettle reaches -0.60MPa, keeps this state response 20 hours；Pressure release is simultaneously passed through nitrogen, makes the reacting kettle inner pressure be
0.60MPa, insulation stand 20 hours；Agitator speed is promoted to 150rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add
Double (the 5- tert-butyl groups -3- formoxyls -4-HBA methyl esters) 100 parts of the contracting cyclohexanediamine of (1R, 2R)-N, N'-, the 4- tert-butyl groups -
After 130 parts of 4'- methoxy dibenzoyl methanes are completely dissolved, add 110 parts of crosslinking agent and be stirred so that reactor solution
Hydrophilic lipophilic balance is 6.0, and insulation stands 20 hours；
4th step：When agitator speed is 130rpm, L-2- (the tertiary fourth oxygen acyl groups of N-) -3', 4'- dimethoxies are sequentially added
60 parts of base phenylalanine ethyl ester, N, N'-1,6- dihexyls two [3- tertiary butyl-4-hydroxy -5- methyl] 150 parts of hydrocinnamamide, N ' -
Diphenyl is along 40 parts of fourth diformamide, 4- [(1- butyl -5- cyano group -1,2- dihydro -6- hydroxy-4-methyl -2- oxo -3- pyridines
Base) azo] 140 parts of-N- (2- ethylhexyls) benzsulfamide, reactor pressure is lifted, reaches 1.70MPa, temperature is
120 DEG C, polymerisation 20 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, 15 DEG C is cooled to, discharging, enters pressing mold
Machine can be prepared by secondary filtration film tablet 3-3；
The crosslinking agent is N, double [β-(hydroxy phenyl of the 3,5- di-t-butyls 4) propionyl] hydrazines of N'-.
Reference examples
Reference examples are used for the service condition of the purification process of water for the secondary filtration film tablet of certain commercially available brand.
Embodiment 4
Secondary filtration film sensing described in the secondary filtration film tablet 3-3 and reference examples that embodiment 1~3 is prepared
The service condition that plate is used for the purification process of water is contrasted, and is produced with capacity of decomposition enhancing rate, purifying water effect enhancing rate, purification
Amount enhancing rate, pollutant conversion total amount enhancing rate are that technical indicator is counted, as a result as shown in table 1：
Secondary filtration film tablet described in the embodiment 1~3 of table 1 and reference examples is used for the service condition of the purification process of water
Parameters contrast
Table 1 is used for the use feelings of the purification process of water for the secondary filtration film tablet described in embodiment 1~3 and reference examples
The comparing result of the parameters of condition, as seen from Table 1, secondary filtration film tablet 3-3 described in the utility model, its resolution
Power enhancing rate, purifying water effect enhancing rate, purification yield enhancing rate, pollutant conversion total amount enhancing rate are above prior art production
Product.
In addition, as shown in figure 4, it is that secondary filtration film tablet 3-3 materials described in the utility model carry with detergent power
Rise rate graph of a relation.Find out in figure, secondary filtration film tablet 3-3 materials are evenly distributed used in embodiment 1~3, and detergent power carries
The rate of liter is high；Secondary filtration film tablet 3-3 described in the utility model is shown in figure, its detergent power enhancing rate is significantly better than existing
There is product.
Described above is only preferred embodiment of the present utility model, it should be pointed out that：For the common skill of the art
For art personnel, on the premise of the utility model principle is not departed from, some improvements and modifications can also be made, these improve and
Retouching also should be regarded as the scope of protection of the utility model.
Claims (8)
- A kind of 1. purifier based on WinCC control programs, it is characterised in that including：Water holding tank (1) to be clean, water inlet Pumping installations (2), purification agent set (3), WinCC programme-control case (5)；The both ends difference of the water inlet pumping installations (2) Connect the delivery port of water holding tank (1) to be clean and the water inlet of purification agent set (3)；The water inlet pumping installations (2) One end is the pumping motor (2-1) connected with the delivery port of purified water holding tank (1), and the other end is to be arranged at purification agent set (3) water injector of top in；The pumping motor (2-1) is connected with water injector by water inlet manifold (2-2)；The water inlet House steward (2-2) is provided with feed water flow gauge (2-3) and current opening and closing electrically-controlled valve (2-4)；The purification agent set (3) sets cleaning position (3-1), quartz sand disinfection storehouse (3-4) from top to bottom；The cleaning position (3-1) sets gradually by-pass filtration film (3-2), secondary filtration film tablet (3-3) from top to bottom；The quartz sand disinfection storehouse Disinfecting instrument (3-5) and Monitoring of Disinfection Efficacy instrument (3-6) are set in (3-4)；Band purified water sprays from water injector, successively through one-level Filter membrane (3-2), secondary filtration film tablet (3-3), disinfecting instrument (3-5) purification, then from the water outlet of purification agent set (3) Mouth discharge；The pumping motor (2-1), feed water flow gauge (2-3), current opening and closing electrically-controlled valve (2-4), water injector, disinfecting instrument (3- 5), secondary filtration film tablet (3-3), Monitoring of Disinfection Efficacy instrument (3-6) respectively with WinCC programme-control case (5) polygon control survey Connection, and controlled by WinCC programme-control case (5).
- A kind of 2. purifier based on WinCC control programs according to claim 1, it is characterised in that the water spray Device includes the feedwater automatically controlled ring of assignment constraints (2-5)；The described feedwater automatically controlled ring of assignment constraints (2-5) rectangular tubular structure, bottom Portion, which is provided with, divides sprinkler head (2-6), divides sprinkler head (2-6) to be uniformly distributed along the feedwater automatically controlled ring of assignment constraints (2-5) four side；It is described to give The automatically controlled ring of water assignment constraints (2-5) is connected with WinCC programme-control case (5) polygon control survey, and by WinCC programme-control case (5) Control.
- A kind of 3. purifier based on WinCC control programs according to claim 1, it is characterised in that the two level Filter membrane tablet (3-3) is made up of the equally distributed W shapes broken line plate of some horizontal directions, the opening direction of W shape broken line plates with Water (flow) direction is vertical；Spacing between adjacent W shapes broken line plate is 7mm~19mm.
- A kind of 4. purifier based on WinCC control programs according to claim 1, it is characterised in that the one-level Launch the engineering bacteria that purifies water in the surface of filter membrane (3-2).
- A kind of 5. purifier based on WinCC control programs according to claim 4, it is characterised in that the two level Filter membrane tablet (3-3) is provided with viable bacteria selection instrument；The viable bacteria selection instrument connection WinCC programme-control case (5)；The work Bacterium selection instrument perceives the treatment effeciency of engineering bacteria of purifying water, and when the treatment effeciency for the engineering bacteria that purifies water is less than 15%, then leads to Electric signal is crossed, notice WinCC programme-control case (5), WinCC programme-control case (5) is by controlling water injector and flow of inlet water Count the flow that (2-3) reduces water；When the engineering bacteria that purifies water treatment effeciency be higher than 35%, then pass through electric signal, notify WinCC Programme-control case (5), WinCC programme-control case (5) is by controlling water injector and feed water flow gauge (2-3) to increase the stream of water Amount.
- A kind of 6. purifier based on WinCC control programs according to claim 1, it is characterised in that the purification Fixed support (4) is provided with below agent set (3), the fixed support (4) is welded and fixed with purification agent set (3) bottom, Fixed support (4) bottom is provided with vibrating sensor, and the vibrating sensor is connected with WinCC programme-control case (5) wire.
- A kind of 7. purifier based on WinCC control programs according to claim 1, it is characterised in that the pumping Motor (2-1) is provided with water quality testing meter, the water quality testing meter and WinCC programme-control casees with water inlet manifold (2-2) junction (5) wire connects.
- A kind of 8. purifier based on WinCC control programs according to claim 1, it is characterised in that the one-level Filter membrane (3-2) gross thickness is not less than 5cm~10cm, in the middle provided with membrane filtration efficiency sensor, the membrane filtration efficiency Sensor is connected with WinCC programme-control case (5) wire.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720386133.6U CN207108740U (en) | 2017-04-13 | 2017-04-13 | A kind of purifier based on WinCC control programs |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720386133.6U CN207108740U (en) | 2017-04-13 | 2017-04-13 | A kind of purifier based on WinCC control programs |
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| CN207108740U true CN207108740U (en) | 2018-03-16 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106946410A (en) * | 2017-04-13 | 2017-07-14 | 徐州工程学院 | A kind of quartzy sand filter purifier and process for purifying water based on WinCC control programs |
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2017
- 2017-04-13 CN CN201720386133.6U patent/CN207108740U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106946410A (en) * | 2017-04-13 | 2017-07-14 | 徐州工程学院 | A kind of quartzy sand filter purifier and process for purifying water based on WinCC control programs |
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