CN207066126U - A kind of mini-sintering system - Google Patents

A kind of mini-sintering system Download PDF

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Publication number
CN207066126U
CN207066126U CN201720965114.9U CN201720965114U CN207066126U CN 207066126 U CN207066126 U CN 207066126U CN 201720965114 U CN201720965114 U CN 201720965114U CN 207066126 U CN207066126 U CN 207066126U
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sintering
cabinet
temperature
mini
atmosphere
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CN201720965114.9U
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孙矿
徐炜
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SHANGHAI CHENHUA TECHNOLOGY CO., LTD.
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Zhejiang Morning Technology Co Ltd
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Abstract

The utility model discloses a kind of mini-sintering system, including sintering equipment, vacuum system, atmosphere system, temperature system, and four integrate in a miniature cabinet, the sintering equipment is arranged on the left of miniature cabinet on the vertical cabinet of top, the vertical cabinet side is provided with for controlling sintering equipment, vacuum system, atmosphere system and the control flow of temperature system operation, opposite side is then provided with the temperature monitor for being used for monitoring temperature in temperature system, the vertical cabinet front is provided with the closure of sintering equipment, the vertical cabinet back side is provided with the inflation line for atmosphere system, the external pump housing, the horizontal cabinet for supporting vertical cabinet is provided with below the vertical cabinet.The utility model forms a high and easy to operation mini-sintering system of the small integrated level of floor space by changing the original structure design of sintering system.

Description

A kind of mini-sintering system
Technical field
It the utility model is related to sintering system field, the specially high mini-sintering system of the small integrated level of floor space.
Background technology
Sintering refers to granular material to be changed into dense body, is a traditional technical process.People utilize this very early Individual technique produces ceramics, powder metallurgy, refractory material, hyperthermal material etc..In general, powder passes through after overmolding It is a kind of polycrystalline material to sinter obtained dense body, and its microstructure is made up of crystal, vitreum and stomata.Sintering process is direct Crystallite dimension, pore size and the grain-boundary shape in microstructure and distribution are influenceed, and then influences the performance of material.
And sintering system can be divided into discharge plasma sintering, hot pressing according to the difference of its heating environment and mode of heating Sintering, resistance heating sintering, wherein discharge plasma sintering (Spark Plasma Sintering, abbreviation SPS) technique be by The powder such as metal load graphite etc. made of material in mould, using upper and lower stamping and powered electrode by specific sintering power supply and Pressing pressure puts on sintered powder, completes to produce a kind of new of high performance material through discharge activation, thermoplastic deformation and cooling Powder metallurgy sintered technology, discharge plasma sintering have the characteristics of being sintered in pressure process, waited caused by pulse current from Pressurization in daughter and sintering process advantageously reduces the sintering temperature of powder, and discharge plasma sintering method (SPS) is by pressing Pulse electric energy, the high heat energy of the high-temperature plasma that spark discharge is instantaneously occurred (plasma discharging) are sent into powder base powder gap It is effectively applied to thermal diffusion and electric field diffusion etc., in the case where being warming up to more than 2000 DEG C of superhigh temperature by low temperature, insulation about exists It can complete " to sinter " in 5 to 20min or so short time or " sinter bonded ", be the new technology of new material synthesis processing, this One new technology is different from traditional " discharge sintering method ", and the material category being applicable is very more and extensive, can be used to synthesize bag Include fiber/particle composite, function-graded material, foreign material and be bonded on interior composite, and closed including amorphous state Metal material including gold, magnetic material, intermetallic compound, hard alloy, it is also possible to for the structure control of porous material, Application prospect is quite varied.And hot pressed sintering is that dry powder is filled into model, then from single shaft direction while pressurization while heat, Make shaping and sintering while a kind of sintering method completed.Its feature is that hot pressed sintering is carried out simultaneously due to heating pressurization, powder In hot plastic state, contribute to the contact diffusion of particle, flow the progress of mass transport process, thus briquetting pressure is only what is be cold-pressed 1/10;It can also reduce sintering temperature, shorten sintering time, grown up so as to resist crystal grain, obtain that crystal grain is tiny, consistency is high and machine The good product of tool, electric property.Sintering aid or shaping assistant need not be added, the ceramic product of ultra-high purity can be produced.And Resistance heating sinters
But equipment volume to be present big for said system, causes floor space big, especially to R&D institution and institute of junior college School, its experimental site is smaller, is not suitable for being placed in Routine Test Lab, and place to place needs to redesign, and causes a large amount of waves Take.
Utility model content
The purpose of this utility model is to form a floor space by changing the original structure design of sintering system small The high and easy to operation mini-sintering system of integrated level.
To achieve the above object, the utility model provides following technical scheme:
A kind of mini-sintering system, it is characterised in that including sintering equipment, vacuum system, atmosphere system, temperature system, And four integrate in a miniature cabinet, wherein, the sintering equipment is arranged on the left of miniature cabinet on the vertical cabinet of top, The vertical cabinet side is provided with for controlling sintering equipment, vacuum system, atmosphere system and the control of temperature system operation System screen, opposite side are then provided with the temperature monitor for being used for monitoring temperature in temperature system, and the vertical cabinet front is provided with The closure of sintering equipment, the vertical cabinet back side are provided with the inflation line for atmosphere system, and the external pump housing is described perpendicular To the horizontal cabinet being provided with below cabinet for supporting vertical cabinet, the horizontal cabinet has been internally integrated sintering equipment, true The control circuit of empty set system, atmosphere system and temperature system, and the sintering equipment uses discharge plasma sintering module, its Including pressue device and impulse current generator.
Preferably, the pressue device is arranged at the top of vertical cabinet, including is set in sintering equipment and sintered above module Seaming chuck, and sinter module-external water-cooled vacuum room.
Preferably, the pressue device is provided with pressure controller and displacement control system, wherein the pressure controller The pulse size sent is 0~200kN, and frequency is 0~100Hz, the pressure controller and the driving for driving seaming chuck Element is connected, the displacement control system include be sequentially connected the sensor connect, capture card, host computer, PLC control system and Servo valve, the servo valve is controlling seaming chuck.
Preferably, temperature monitor, PLC control system and the pulse current that the temperature system includes being sequentially connected occur Device, the sintering equipment left side are provided with a through hole for being used for infrared detection temperature.
Preferably, the atmosphere system includes gas handling system and gas extraction system;The gas handling system includes a fast inflation Circuit and a slow inflation line, the fast inflation line include fast charge valve and flowmeter, and the slow inflation line includes trickle charge Valve and flowmeter, the flow velocity of the fast inflation line in 3~30L/mim, the flow velocity of the slow inflation line in 1~10L/min, The gas extraction system includes atmosphere pressures sensor, vacuum meter, air bleeding valve, Manual air-release valves and the regulating valve being sequentially connected, institute The size of valve port can be changed by stating regulating valve, and control electric current scope is connected with filter between 4~20mA after the regulating valve With the direct-connected pump of rotary vane type.
And a kind of sintering method of mini-sintering system, comprise the following steps:
S1, sintering equipment closure in vertical cabinet opened, be sintered thing and be put into sintering equipment, pass through control after sealing System screen control mini-sintering system extracts vacuum to 5pa;
S2, by control flow control pressue device in seaming chuck displacement, to mould apply pressure, pressure limit is in 2- 15kN, voltage stabilizing 1-5min;
S3, pass through the impulse current generator in control flow control temperature system so that temperature is adjusted at 500-2000 DEG C Fluctuation, kept for certain time;
S4, after machining, thing to be sintered be cooled to room temperature taking-up.
Compared with prior art, the beneficial effects of the utility model are as follows:
1st, this mini-sintering system is in its structure optimization, by reasonably arranging so that the occupation of land face of whole sintering system Product is small, and vertical height control is within the specific limits, is easy to laboratory or other research institutions to be used;
2nd, this mini-sintering system has the repertoire of other large scale sintering systems, and intelligent, integrated level height, operation Personnel can directly complete all operationss of sintering system by control flow, and be checked by control flow each in whole sintering process The design parameter at position.
Brief description of the drawings
Fig. 1 is the front view of the utility model mini-sintering system;
Fig. 2 is the schematic diagram of the utility model mini-sintering system;
Fig. 3 is the structural representation of the utility model mini-sintering system.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made The every other embodiment obtained, belong to the scope of the utility model protection.
Fig. 1-3 are referred to, the utility model provides a kind of technical scheme:The mini-sintering system, including sintering equipment 1, Vacuum system, atmosphere system, temperature system, and four integrate in a miniature cabinet 100, wherein, the sintering equipment 1 is set On the vertical cabinet 101 above the miniature left side of cabinet 100, the vertical side of cabinet 101 is provided with for controlling sintering dress The control flow 5 of 1, vacuum system, atmosphere system and temperature system operation is put, opposite side, which is then provided with temperature system, is used for temperature The temperature monitor 4 of monitoring is spent, the vertical front of cabinet 101 is provided with the closure 11 of sintering equipment 1, the vertical cabinet 101 back sides are provided with the inflation line 3 for atmosphere system, and the external pump housing 31, the vertical lower section of cabinet 101, which is provided with, to be used for The horizontal cabinet 102 of vertical cabinet 101 is supported, the horizontal cabinet 102 has been internally integrated sintering equipment 1, vacuum system, atmosphere The control circuit of system and temperature system, the sintering equipment 1 use discharge plasma sintering module, and it includes pressue device 6 and impulse current generator.Electrode 71 is arranged on seaming chuck in wherein described impulse current generator.
The pressue device 6 is arranged on the vertical top of cabinet 101, including sets in sintering equipment 1 and sinter above module Seaming chuck 61, and sinter the water-cooled vacuum room 2 of module-external.
The pressue device 6 is provided with pressure controller and displacement control system, wherein what the pressure controller was sent Pulse size is 0~200kN, and frequency is 0~100Hz, the pressure controller and the driving element for driving seaming chuck 61 It is connected, the driving element can be hydraulic cylinder either cylinder or other mechanical drive modes, and unilateral pressure head is realized with this Pulsed or the pressing of single formula, wherein more pulseds from unilateral pressure head or single formula pressing mode, the pressing effect brought Fruit is more preferable, and stability is higher.The displacement control system includes being sequentially connected the sensor connect, capture card, host computer, PLC controls System processed and servo valve, the servo valve is controlling seaming chuck 61.The sensor includes force snesor and displacement transducer, Force snesor and displacement transducer are arranged at seaming chuck, are easy to the accuracy of sensing.Because the system data volume is more huge, The acquisition module carried using common PLC control system can not be completed to gather, therefore PLC coordinates capture card, host computer to carry out The collection and analysis of data, while capture card uses 10KHz specification, ensures the normal acquisition of data.
The temperature system includes temperature monitor 4, PLC control system and the impulse current generator 71 being sequentially connected, The left side of sintering equipment 1 is provided with a through hole 41 for being used for infrared detection temperature.
The atmosphere system includes gas handling system and gas extraction system;The gas handling system includes a fast inflation line and one The slow inflation line of bar, the fast inflation line include fast charge valve and flowmeter, and the slow inflation line includes trickle charge valve and flow Meter, the flow velocity of the fast inflation line is in 3~30L/mim, and the flow velocity of the slow inflation line is in 1~10L/min, the exhaust System includes atmosphere pressures sensor, vacuum meter, air bleeding valve, Manual air-release valves and the regulating valve being sequentially connected, the regulating valve The size of valve port can be changed, control electric current scope is connected with filter and rotary vane type between 4~20mA after the regulating valve Direct-connected pump.
And a kind of sintering method of mini-sintering system, comprise the following steps:
S1, the closure 11 of sintering equipment 1 in vertical cabinet 101 opened, be sintered thing and be put into sintering equipment 1, sealed Mini-sintering system is controlled to extract vacuum to 5pa by control flow 5 afterwards;
S2, the displacement of seaming chuck 61 in pressue device 6 controlled by control flow 5, pressure is applied to mould, pressure limit exists 2-15kN, voltage stabilizing 1-5min;
S3, pass through the impulse current generator 71 in the control temperature system of control flow 5 so that temperature is adjusted in 500-2000 DEG C fluctuation, keep certain time;
S4, after machining, thing to be sintered be cooled to room temperature taking-up.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art, It is appreciated that these embodiments can be carried out with a variety of changes in the case where not departing from principle of the present utility model and spirit, repaiied Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.

Claims (5)

  1. A kind of 1. mini-sintering system, it is characterised in that including sintering equipment, vacuum system, atmosphere system, temperature system, and Four integrate in a miniature cabinet, wherein, the sintering equipment is arranged on the left of miniature cabinet on the vertical cabinet of top, institute Vertical cabinet side is stated to be provided with for controlling sintering equipment, vacuum system, atmosphere system and the control of temperature system operation Screen, opposite side are then provided with the temperature monitor for being used for monitoring temperature in temperature system, and the vertical cabinet front is provided with burning The closure of device is tied, the vertical cabinet back side is provided with the inflation line for atmosphere system, and the external pump housing is described vertical The horizontal cabinet for supporting vertical cabinet is provided with below cabinet, the horizontal cabinet has been internally integrated sintering equipment, vacuum The control circuit of system, atmosphere system and temperature system, the sintering equipment use discharge plasma sintering module, and it includes Pressue device and impulse current generator.
  2. 2. a kind of mini-sintering system according to claim 1, it is characterised in that the pressue device is arranged on vertical cabinet At the top of body, including the seaming chuck in sintering equipment above sintering module is set, and sinters the water-cooled vacuum room of module-external.
  3. 3. a kind of mini-sintering system according to claim 2, it is characterised in that the pressue device is provided with pressure control Device and displacement control system processed, wherein the pulse size that the pressure controller is sent is 0~200kN, frequency is 0~ 100Hz, with driving the driving element of seaming chuck to be connected, the displacement control system includes being sequentially connected the pressure controller Sensor, capture card, host computer, PLC control system and the servo valve connect, the servo valve is controlling seaming chuck.
  4. 4. a kind of mini-sintering system according to claim 3, it is characterised in that the temperature system includes being sequentially connected Temperature monitor, PLC control system and impulse current generator, be provided with one on the left of the sintering equipment and be used for infrared inspection The through hole of testing temperature.
  5. 5. a kind of mini-sintering system according to claim 4, it is characterised in that the atmosphere system includes gas handling system And gas extraction system;The gas handling system includes fast an inflation line and a slow inflation line, and the fast inflation line includes Fast charge valve and flowmeter, the slow inflation line include trickle charge valve and flowmeter, and the flow velocity of the fast inflation line is in 3~30L/ Mim, for the flow velocity of the slow inflation line in 1~10L/min, the gas extraction system includes the atmosphere pressures sensing being sequentially connected Device, vacuum meter, air bleeding valve, Manual air-release valves and regulating valve, the regulating valve can change the size of valve port, control electric current scope Between 4~20mA, filter and the direct-connected pump of rotary vane type are connected with after the regulating valve.
CN201720965114.9U 2017-08-04 2017-08-04 A kind of mini-sintering system Active CN207066126U (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107314676A (en) * 2017-08-04 2017-11-03 浙江晨华科技有限公司 A kind of mini-sintering system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107314676A (en) * 2017-08-04 2017-11-03 浙江晨华科技有限公司 A kind of mini-sintering system

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Effective date of registration: 20181023

Address after: Room 17006, 1191 East Daming Road, Hongkou District, Shanghai

Patentee after: SHANGHAI CHENHUA TECHNOLOGY CO., LTD.

Address before: 313000 No. 66, eight Li shop, Tian Lu, Wuxing District, Huzhou, Zhejiang.

Patentee before: Zhejiang morning Technology Co., Ltd.