CN206881692U - A kind of corrosion-and high-temp-resistant Multifunction quartz reactor - Google Patents

A kind of corrosion-and high-temp-resistant Multifunction quartz reactor Download PDF

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Publication number
CN206881692U
CN206881692U CN201720770005.1U CN201720770005U CN206881692U CN 206881692 U CN206881692 U CN 206881692U CN 201720770005 U CN201720770005 U CN 201720770005U CN 206881692 U CN206881692 U CN 206881692U
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China
Prior art keywords
material container
corrosion
temp
quartz reactor
jacket structured
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CN201720770005.1U
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Chinese (zh)
Inventor
刘广卫
贾泽坤
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DONGHAI COUNTY KAIKAI QUARTZ PRODUCTS Co Ltd
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DONGHAI COUNTY KAIKAI QUARTZ PRODUCTS Co Ltd
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Priority to CN201720770005.1U priority Critical patent/CN206881692U/en
Priority to DE202017105610.4U priority patent/DE202017105610U1/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/0066Multi-circuit heat-exchangers, e.g. integrating different heat exchange sections in the same unit or heat-exchangers for more than two fluids
    • F28D7/0083Multi-circuit heat-exchangers, e.g. integrating different heat exchange sections in the same unit or heat-exchangers for more than two fluids with units having particular arrangement relative to a supplementary heat exchange medium, e.g. with interleaved units or with adjacent units arranged in common flow of supplementary heat exchange medium
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/02Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled
    • F28D7/022Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled the conduits of two or more media in heat-exchange relationship being helically coiled, the coils having a cylindrical configuration
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/10Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged one within the other, e.g. concentrically
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/0009Coils
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135Electric resistance heaters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/0015Controlling the temperature by thermal insulation means
    • B01J2219/00153Vacuum spaces
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/025Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0254Glass
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/025Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0263Ceramic
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D1/00Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium is a large body of fluid, e.g. domestic or motor car radiators
    • F28D1/06Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium is a large body of fluid, e.g. domestic or motor car radiators with the heat-exchange conduits forming part of, or being attached to, the tank containing the body of fluid
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D21/00Heat-exchange apparatus not covered by any of the groups F28D1/00 - F28D20/00
    • F28D2021/0019Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for
    • F28D2021/0022Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for for chemical reactors

Abstract

The utility model is a kind of corrosion-and high-temp-resistant Multifunction quartz reactor:The quartz reactor includes the material container as reative cell, it is provided with outside material container jacket structured, material container is provided with some functional interfaces, it is jacket structured to be provided with heat-conducting medium inlet/outlet pipe, material container and it is jacket structured between chuck in be provided with some groups around material container set helix tubes, the helix tube be supported and fixed on material container or it is jacket structured on, the both ends of helix tube pass jacket structured to be connected with supporting peripheral hardware mechanism;The material container, jacket structured, functional interface, heat-conducting medium inlet/outlet pipe and helix tube are made by quartz material and use seamless welding into a single integrated structure.For the utility model due to that provided with some groups of helix tubes, can realize instantaneous switching when needing to be heated or cooled, heat exchange efficiency is high and uniformly.

Description

A kind of corrosion-and high-temp-resistant Multifunction quartz reactor
Technical field
It the utility model is related to reactor technology field, and in particular to a kind of corrosion-and high-temp-resistant Multifunction quartz reaction Device.
Background technology
Reactor is a kind of comprehensive reaction vessel, can be with pre-set from charging-reaction-discharging of beginning Reactions steps carry out.Shortcomings part has traditional reactor in use:
First, for the situation of change for hydrolyzing, neutralize, crystallizing, polymerize, being condensed etc. in chemical reaction process, have no way of learning, It can only by rule of thumb judge or observation window is set, and the range of observation of observation window is smaller, it is difficult to fully understand in chemical reaction process Situation of change;
Second, producing high temperature sometimes in chemical reaction process, reactor made of metal or ceramic material bears chemistry The ability of caused high temperature is worse in course of reaction;Promote to chemically react sometimes for hot environment, the liter of traditional reactor Temperature is slower, influences reaction efficiency.
Third, reactor of the prior art using when be all only to be heated or cooled to carry out material by medium circulation, imitate Rate is low, and the heat exchange uniformity is inadequate.
The content of the invention
Technical problem to be solved in the utility model is in view of the shortcomings of the prior art, there is provided a kind of structure design is more Good, heat exchange is especially uniformly suitable for the corrosion-and high-temp-resistant Multifunction quartz reactor of a variety of chemical reactions.
Technical problem to be solved in the utility model is realized by following technical scheme.The utility model is A kind of corrosion-and high-temp-resistant Multifunction quartz reactor, is characterized in:The quartz reactor includes holding as the material of reative cell Device, is provided with jacket structured outside material container, and material container is provided with some functional interfaces, jacket structured provided with heat conduction Jie Matter inlet/outlet pipe, material container and it is jacket structured between chuck in be provided with some groups around material container set helix tubes, institute State helix tube be supported and fixed on material container or it is jacket structured on, the both ends of helix tube pass jacket structured with supporting peripheral hardware machine Structure connects;The material container, jacket structured, functional interface, heat-conducting medium inlet/outlet pipe and helix tube are made by quartz material It is and into a single integrated structure using seamless welding.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:The jacket structured outside is provided with vacuum interlayer.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:The functional interface includes the vomit pipe for being arranged on material container bottom, and the end of vomit pipe is provided with the spiral shell for installing Line structure.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:Described supporting peripheral hardware mechanism is peripheral hardware cycling mechanism.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:Described peripheral hardware cycling mechanism is circulating water chennel or wind EGR with heating or refrigerating function.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:Electrical heating elements are wherein being provided with one group of helix tube.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:Described electrical heating elements are carbon fiber exothermic part, microwave heater, electromagnetic heating body or resistance heater.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:The quantity of the helix tube is 2-5 groups.
A kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in the utility model, its further preferred technical side Case is:Set between each group helix tube using interaction apart windings, or using arranged side by side up and down, inside and outside arranged side by side, forward-reverse spiral simultaneously A kind of mode in row is distributed.
Compared with prior art, the beneficial effects of the utility model are:
1st, each building block of the utility model reactor is by quartz material, and on the one hand quartz is visual good, The situation of change in course of reaction in reactor can be fully understanded;On the other hand quartz has outstanding corrosion resistance, high temperature resistant Property and resistance to temperature difference irritability, its be adapted to operating temperature range at -50 DEG C -1000 DEG C or so.Therefore material container can be born Caused high temperature and the heat of external heat transmission in chemical reaction process.
2nd, the utility model quartz reactor, by material container and it is jacket structured between chuck in be provided with some groups The helix tube set around material container;Set helix tube can be used for placing electrical heating elements, can also be passed through heat exchange material Heat-conducting medium is exchanged heat, so as to realize the heat exchange to the reaction mass in material container, helix tube does not connect with material container Direct contact heat transfer is touched, but is exchanged heat with heat-conducting medium, then uniform heat exchange is realized by heat-conducting medium.Due to provided with some groups Helix tube, instantaneous switching can be realized when needing to be heated or cooled.Heat exchange efficiency is high.
3rd, material container described in the utility model, jacket structured, functional interface, heat-conducting medium inlet/outlet pipe and helix tube by Quartz material is made and uses seamless welding into a single integrated structure, without seam, thoroughly solves the problems, such as the evaporating, emitting, dripping or leaking of liquid or gas of reactor.
Brief description of the drawings
Fig. 1 is a kind of structural representation of the utility model reactor;
Fig. 2 is a kind of structure distribution schematic diagram of helix tube;
Fig. 3 is another structure distribution schematic diagram of helix tube;
Fig. 4 is the yet another construction distribution schematic diagram of helix tube.
Embodiment
Referring to the drawings, concrete technical scheme of the present utility model described further below, in order to the skill of this area Art personnel are further understood that the utility model, without forming the limitation to its right.
Embodiment 1, reference picture 1, a kind of corrosion-and high-temp-resistant Multifunction quartz reactor:The quartz reactor includes conduct The material container 1 of reative cell, jacket structured 7 being provided with outside material container 1, material container 1 is provided with some functional interfaces 3, Jacket structured 7 are provided with heat-conducting medium inlet/outlet pipe 6, and some groups are provided with the chuck 2 between material container 1 and jacket structured 7 The helix tube 8 set around material container 1, the helix tube 8 are supported and fixed on material container 1 or jacket structured 7, helix tube 8 both ends pass jacket structured 7 and are connected with supporting peripheral hardware mechanism;The material container 1, jacket structured 7, functional interface 3, heat conduction Medium inlet/outlet pipe 6 and helix tube 8 are made by quartz material and use seamless welding into a single integrated structure.
Embodiment 2, in a kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in embodiment 1:Described jacket structured 7 Outside be provided with vacuum interlayer.By set vacuum interlayer, this realizes more preferable heat transfer effect.
Embodiment 3, in a kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in embodiment 1 or 2:The function connects Mouth 3 includes the vomit pipes 4 for being arranged on the bottom of material container 1, and the end of vomit pipe 4 is provided with the helicitic texture 5 for installing.
Embodiment 4, in a kind of any described corrosion-and high-temp-resistant Multifunction quartz reactors of embodiment 1-3:Described Supporting peripheral hardware mechanism is peripheral hardware cycling mechanism, and peripheral hardware cycling mechanism can be that circulating water chennel or wind with heating or refrigerating function follow Loop device, thermal source or low-temperature receiver are provided for helix tube 8, is exchanged heat for being realized with heat transferring medium.
Embodiment 5, in a kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in embodiment 1-4 any one:Institute The quantity for stating helix tube is 1 group, and electrical heating elements are provided with the helix tube.Described electrical heating elements are carbon fiber heating Body, microwave heater, electromagnetic heating body or resistance heater.
Embodiment 6, in a kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in embodiment 1-4 any one:Institute The quantity for stating helix tube is 2 groups, and electrical heating elements are wherein being provided with one group of helix tube.Described electrical heating elements are carbon fiber Heater, microwave heater, electromagnetic heating body or resistance heater.Another group of helix tube be used to inputting circulating air, steam, Hot water or circulation cold air, cold water, set using interaction apart windings between each group helix tube, or using arranged side by side up and down, interior A kind of outer mode side by side, during forward-reverse spiral is arranged side by side is distributed, reference picture 2-4.
Embodiment 7, in a kind of corrosion-and high-temp-resistant Multifunction quartz reactor described in embodiment 1-4 any one:Institute The quantity for stating helix tube is 3 groups, and electrical heating elements are wherein being provided with one group of helix tube.Described electrical heating elements are carbon fiber Heater, microwave heater, electromagnetic heating body or resistance heater.Another two groups of helix tubes be used for input circulating air, steam, Hot water or circulation cold air, cold water, set using interaction apart windings between each group helix tube, or using arranged side by side up and down, interior A kind of outer mode side by side, during forward-reverse spiral is arranged side by side is distributed, reference picture 2-4.
The method that heat exchange reaction is carried out using the corrosion-and high-temp-resistant Multifunction quartz reactor is as follows:Reaction mass enters As the material container of reative cell, heat-conducting medium is passed through into chuck, when reaction needs heating, passes through one group of spiral thereto The one kind inputted in pipe in circulating air, steam, hot water, or start electrical heating elements, the heat-conducting medium in heating jacket is real Now the reaction mass in material container is heated;After the completion of reaction when cooling is needed, one group of helix tube thereto is passed through Middle input circulation cold air, cold water cool down the heat-conducting medium in heating jacket, realize and the reaction mass in material container is carried out Cooling, again by vomit pipe blowing after the completion of cooling, during being heated or cooled, the fluid as heat-conducting medium does not enter in itself Row circulation.

Claims (9)

  1. A kind of 1. corrosion-and high-temp-resistant Multifunction quartz reactor, it is characterised in that:The quartz reactor includes being used as reative cell Material container, be provided with outside material container jacket structured, material container is provided with some functional interfaces, it is jacket structured on set Have heat-conducting medium inlet/outlet pipe, material container and it is jacket structured between chuck in be provided with some groups around material container set spiral shells Coil, the helix tube be supported and fixed on material container or it is jacket structured on, the both ends of helix tube pass jacket structured with matching somebody with somebody Cover the connection of peripheral hardware mechanism;The material container, jacket structured, functional interface, heat-conducting medium inlet/outlet pipe and helix tube are by quartz Material is made and uses seamless welding into a single integrated structure.
  2. A kind of 2. corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 1, it is characterised in that:The chuck The outside of structure is provided with vacuum interlayer.
  3. A kind of 3. corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 1, it is characterised in that:The function Interface includes the vomit pipe for being arranged on material container bottom, and the end of vomit pipe is provided with the helicitic texture for installing.
  4. A kind of 4. corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 1, it is characterised in that:Described matches somebody with somebody It is peripheral hardware cycling mechanism to cover peripheral hardware mechanism.
  5. A kind of 5. corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 4, it is characterised in that:Described is outer If cycling mechanism is circulating water chennel or wind EGR with heating or refrigerating function.
  6. A kind of 6. corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 1, it is characterised in that:Wherein one Electrical heating elements are provided with group helix tube.
  7. A kind of 7. corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 6, it is characterised in that:Described electricity Heating element heater is carbon fiber exothermic part, microwave heater, electromagnetic heating body or resistance heater.
  8. 8. a kind of corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 1-7 any one, its feature exist In:The quantity of the helix tube is 2-5 groups.
  9. A kind of 9. corrosion-and high-temp-resistant Multifunction quartz reactor according to claim 8, it is characterised in that:Each group spiral Between pipe using interaction apart windings set, or using it is arranged side by side up and down, inside and outside side by side, forward-reverse spiral it is arranged side by side in a kind of mode Distribution.
CN201720770005.1U 2017-06-29 2017-06-29 A kind of corrosion-and high-temp-resistant Multifunction quartz reactor Active CN206881692U (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201720770005.1U CN206881692U (en) 2017-06-29 2017-06-29 A kind of corrosion-and high-temp-resistant Multifunction quartz reactor
DE202017105610.4U DE202017105610U1 (en) 2017-06-29 2017-09-15 High Temperature and Corrosion Resistant Multifunction Quartz Reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720770005.1U CN206881692U (en) 2017-06-29 2017-06-29 A kind of corrosion-and high-temp-resistant Multifunction quartz reactor

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107138110A (en) * 2017-06-29 2017-09-08 东海县凯凯石英制品有限公司 A kind of corrosion-and high-temp-resistant Multifunction quartz reactor and heat exchange reaction method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107138110A (en) * 2017-06-29 2017-09-08 东海县凯凯石英制品有限公司 A kind of corrosion-and high-temp-resistant Multifunction quartz reactor and heat exchange reaction method

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