CN206549609U - The continuous charging system of solid polyolefin hydrocarbon catalyst with online switching system - Google Patents

The continuous charging system of solid polyolefin hydrocarbon catalyst with online switching system Download PDF

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CN206549609U
CN206549609U CN201621413506.6U CN201621413506U CN206549609U CN 206549609 U CN206549609 U CN 206549609U CN 201621413506 U CN201621413506 U CN 201621413506U CN 206549609 U CN206549609 U CN 206549609U
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line
valve
catalyst
high pressure
gases
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Inventor
王登飞
任合刚
郭峰
何书艳
姜艳峰
李�瑞
国海峰
孙彬彬
赵增辉
韦德帅
杜威
高宇新
宋磊
杨国兴
付义
王斯晗
姜进宪
王熺
王立明
闫磊磊
吕红丽
何贵磊
李峰
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China Petroleum and Natural Gas Co Ltd
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China Petroleum and Natural Gas Co Ltd
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Abstract

A kind of continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of band, including:Tank body to hold catalyst, tank body top is provided with safety attachment, pressurized gas inlet pipeline, counterbalance valve, catalyst inlet line, and bottom valve is provided with tank base, and bottom valve is connected with outlet line, and outlet line is provided with baiting valve;Scavenging conduit group, including the first gases at high pressure blow line, the second gases at high pressure blow line, two blow lines are arranged on outlet line and positioned at the two ends of baiting valve, and the second gases at high pressure blow line draws sampling by-pass line, pressurized gas inlet branch line;Clean pipe group, including cleaning agent suction line, cleaning agent outlet line, low-pressure gas suction line, cleaning agent suction line is drawn from the second gases at high pressure blow line, and cleaning agent outlet line is drawn from outlet line, and low-pressure gas suction line is connected with tank body top;Agitating device, is connected and extends in tank body with tank body top;Temperature control system, is covered on tank body outer surface.

Description

The continuous charging system of solid polyolefin hydrocarbon catalyst with online switching system
Technical field
The utility model is related to field of olefin polymerisation, more particularly, to a kind of charging of granular solids polyolefin catalyst System.
Background technology
The catalyst majority applied to olefinic polyreaction industrial at present is solid particle type, and this solid particle type is urged The charging of agent is generally added using the catalyst feeding device of particular design, such as is used on Unipol polyethylene devices Solid catalysis agent feeding device;It is also a kind of by complicated process for preparation, by catalyst preparation into certain density slurries or Paste, then send into reactor with metering system.Both the above method, the former equipment investment is very high, and adition process is easily blocked up, The amount of catalyst in catalyst feeder is known without accurately and effectively method.The process for preparation of the latter is extremely complex, single The preparation of catalyst is accomplished by ten more than hour, and catalyst brings slurries or paste into reaction system, to reaction system Have an impact.
Polyolefin catalyst generally has very high activity, requires catalyst with sufficiently stable and accurate in practical operation The minimum flow of control is added in polymer reactor, and it is unstable otherwise to will result in polymerisation, causes product quality to fluctuate Or the caking in reactor.Therefore, it is the key for needing to solve how catalyst to be added into polymerization reaction system uniformly, exactly Problem.In addition the poor fluidity of solid olefins polymerization catalyst, cohesive easily in catalyst storage tank to unite or formed bridge formation, is catalyzed Agent can not be added in feeding line by automatic valve, cause catalyst can not continuous feed, reaction be forced stop.
Chinese patent CN101786552A discloses a kind of powder material autoweighting feeder, including charging hopper, plus The outlet of funnel connects the entrance of metering ball valve, measures in the material channel of ball valve provided with determination capacity and rotary storage Expect room, the outer wall of storage compartment is against the inwall of the material channel of metering ball valve, and in storage compartment's rotation process, material import and export can It is connected with the entrance or outlet for measuring ball valve.The utility model can realize the powder feed of low dose, but material is easily in thing Expect the inwall deposition of passage, cause error in dipping.
Chinese patent CN101811011A discloses a kind of automatic catalyst-feeding method, set fluidisation conveying airduct line to It is continually fed into feeder on fluidisation conveying wind, fluidisation conveying airduct line and fluidisation conveying wind regulating valve and flowmeter, charging is set Charging regulating valve is set on pipe, sets one to connect between the pipeline section of outlet valve near exit with discharge nozzle at the top of feeder Valve and blast regulating valve are communicated with pipe, communicating pipe, fluidisation conveying wind is constantly passed through into feeder, catalyst is in charging Circulated in connection circulation loop at the top of device, reduce the deposition blocking during catalyst transport, feed unstable asks Topic, but the EGR of the equipment is arranged on feeder top, and very strong fluidisation conveying wind, the device one are needed in cyclic process As use compressed air as fluidisation and convey wind, therefore equipment cost is higher, and the utility model is also required by fluidizing conveying Wind ensures that pressure is constant less than or equal to catalyst storage tank pressurising pressure, higher than regenerator pressure, so to equipment in feeder Requirement it is higher, add production cost.
Chinese patent CN102993342 A provide a kind of charging system of powdery polyolefin catalyst.The system includes urging Agent storage tank, pans and blower fan, catalyst storage tank are connected by pipeline with pans, and an automatic valve, wind are set on pipeline The gateway of machine at the top and bottom of pipeline and pans respectively with being connected to form on circulation loop, pipeline at the top of the pans Position sets outlet, is connected by pipeline with rear system.The automatic valves of two series connection are set above the line under the overall leadership being connected with rear system, One quantity tube is set between automatic valve;One gas blow line is set respectively in the outlet of two automatic valves.The practicality is new Solid catalyst can be added continuously in reaction system by type at ambient pressure, but due to lacking the metering device of catalyst, be urged The addition of agent is uncontrollable.And this charging system uses a catalyst storage tank and a pans, catalyst charging Long flow path, catalyst is easily enriched with and remained in pans, causes the waste of catalyst.
Different types of catalyst often poisonous substance each other.If device need switching the trade mark when, it is necessary to thoroughly remove catalyst Charging system, is now accomplished by dismantling catalyst feed systems.Polyolefin catalyst is former using poisonous and hazardous transition metal Son is as the activated centre of catalyst, the alkyl aluminium component often not waited containing quantity in solid polyolefin hydrocarbon catalyst in addition, Meeting can vigorous combustion after air.When switching catalyst, it is enriched with such as in catalyst storage tank, not only results in environmental pollution, also Operating personnel can be caused with personal injury, trigger serious accident.Existing catalyst addition system is pressure vessel, is torn open Unload process cumbersome and time-consuming.The usual residence time of polyolefin catalyst in the reactor is 30 minutes to 2 hours, and this just anticipates Taste must complete as early as possible in the unloading process of catalyst feed systems.And in existing gas-phase polythene commercial plant, The raw materials such as ethene, co-monomer, nitrogen and solid catalyst need to be continuously added into gas-phase fluidized-bed reactor, if feed system Take-down time is long, will result in a series of serious consequences such as reactor superpressure, raw material are largely vented, device stops.And it is industrial Device is big due to scale, and the loss that each driving and parking is caused is also millions of levels.And the key for switching the trade mark is exactly two kinds of catalysis The Rapid replacement in charging system of agent system.Therefore in the urgent need to one kind catalysis can be switched fast without stopping polymerisation The catalyst addition system of agent system.
In addition, the existing high-end trade mark or temperature sensitive type solid polyolefin hydrocarbon catalyst are in fill process, feeding temperature needs dimension Hold at 0~30 DEG C.The fluctuation of feeding temperature can influence the performance of catalyst and its polymerizate, cause polymerizate quality ripple It is dynamic, and then influence the benefit of manufacturing enterprise.And the charging system of existing solid polyolefin hydrocarbon catalyst is without temperature regulating device.Cause This is in the urgent need to a kind of continuous charging of solid polyolefin hydrocarbon catalyst and online switching system.The utility model utility model is consolidated The charging system of body polyolefin catalyst, increases by an agitator on catalyst storage tank, one temperature regulating device of outside increase, both can be with The blanking temperature of stability contorting catalyst, can avoid catalyst from bonding and unite or formed bridge formation again.It is real using the utility model With the charging system of new solid polyolefin hydrocarbon catalyst, simple in equipment, catalyst charging flow is short;Per depot siding and valve Door is purged and conveyed by gases at high pressure, enrichment and residual in the absence of catalyst;Both being produced into for polyolefin had been saved This, is easy to the maintenance maintenance of equipment again.The utility model also helps different types of catalyst and switched online, saves polyolefin The driving cost of commercial plant, it is to avoid the generation of Transition Materials.
Utility model content
For the defect of above-mentioned prior art, there is provided the continuous charging of the solid polyolefin hydrocarbon catalyst with online switching system System, the present apparatus adds on-line cleaning pipe group, switches online beneficial to different types of catalyst, saves polyolefin industry device Production cost, it is to avoid the generation of Transition Materials, and the material system can solve the problem that on the premise of equipment cost is not increased it is existing The problem of easily deposition, blocking etc. cause to feed unstable in systems during pellet type catalyst charging in technology.To realize Above-mentioned purpose, utility model can take following technical proposals:
A kind of continuous charging system of the solid polyolefin hydrocarbon catalyst for the online switching system of band that the utility model is provided, its It is characterised by, including:
One tank body to hold catalyst, tank body top provided with safety attachment, pressurized gas inlet pipeline, counterbalance valve, Catalyst inlet line, bottom valve is provided with tank base, and bottom valve is connected with an outlet line, and the outlet line is provided with Baiting valve;
One scavenging conduit group, including the first gases at high pressure blow line, the second gases at high pressure blow line, first high pressure Gas blow line, the second gases at high pressure blow line are drawn from the outlet line and positioned at the two ends of baiting valve, institute The second gases at high pressure blow line is stated close to the bottom valve, the second gases at high pressure blow line draws one and samples by-pass line, one Pressurized gas inlet branch line;
One cleaning pipe group, including cleaning agent suction line, cleaning agent outlet line, low-pressure gas suction line, it is described clear Lotion suction line is drawn from the second gases at high pressure blow line, and the cleaning agent outlet line is drawn from outlet line, And the cleaning agent outlet line is located at after the first gases at high pressure blow line, on the low-pressure gas suction line and tank body Portion is connected;
One agitating device, is connected and extends in the tank body with tank body top;
One temperature control system, is covered on tank body outer surface.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that described Temperature control system is an electric heater unit.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that described Safety attachment includes a safety valve and a rupture disk.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that described Bottom valve is closed when being a normally opened ball valve, cleaning tank body or filling catalyst.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that high pressure Gas access branch line is provided with the second valve, and sampling by-pass line is provided with sampling valve, and cleaning pipeline is provided with cleaning inlet valve.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that described Agitating device includes a motor and the agitator with motor connection, and the agitator is helix(ribbon type) agitator, magnetic stirring apparatus, magnetic Power heating stirrer, hinging type agitator, frequency conversion double layer agitator, propeller mixer, turbine agitator, paddle stirring One of which in device, anchor agitator.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that described First gases at high pressure blow line is provided with the 3rd valve.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that described The first gases at high pressure blow line or the second gases at high pressure blow line in used gas not occur chemistry with catalyst The gas of reaction.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that described Rotating blanking valve is automatic rotary valve, and the volume of automatic rotary valve is fixed.
The continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of described band, it is characterised in that catalysis Agent suction line is provided with inlet valve, and pressurized gas inlet pipeline is provided with the first valve, provided with clear on cleaning agent outlet line Outlet valve is washed, low-pressure gas suction line is provided with the 4th valve, and outlet valve is provided with outlet line end, and outlet valve is set It is placed between baiting valve and polymer reactor.
Whole system flow of the present utility model is short, and simple in equipment, maintenance maintenance is convenient.Can using the utility model To avoid, because bonding is united or arch formation in catalyst storage tank caused by the poor fluidity of solid olefins polymerization catalyst, solving Catalyst can not continue the problem of charging, solid polyolefin catalyst granules can continuously, it is steady and be precisely added and gather Close in reactor;Simultaneously catalyst is avoided to deposit, block on pipeline and everywhere valve.In addition with beneficial to different types of Catalyst switches online, saves the production cost of polyolefin industry device, it is to avoid the generation of Transition Materials,
Brief description of the drawings
Fig. 1 is the continuous charging system structure diagram of the solid polyolefin hydrocarbon catalyst with online switching system.
Wherein reference is:
1 tank body
Agitating device 11
Motor 111
Agitator 112
Counterbalance valve 12
Safety attachment 13
Pressurized gas inlet pipeline 14
First valve 141
Catalyst inlet line 15
Inlet valve 151
Bottom valve 16
Outlet line 17
Outlet valve 171
Baiting valve 18
First gases at high pressure blow line 19
3rd valve 191
Second gases at high pressure blow line 20
Sample by-pass line 201
Sampling valve 2011
Pressurized gas inlet branch line 202
Second valve 2021
Cleaning agent suction line 203
Clean inlet valve 2031
Cleaning agent outlet line 21
Washing outlet valve 211
Low-pressure gas suction line 22
4th valve 221
Temperature control system 2
Embodiment
Structural principle of the present utility model and operation principle are described in detail below in conjunction with the accompanying drawings:
The utility model provides a kind of continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of band, is System includes:Tank body 1, scavenging conduit group, cleaning pipe group, a temperature control system 2, agitating device 11.
Tank body 1 is catalyst storage tank, and the top of tank body 1 is provided with agitating device 11, safety attachment 13, provided with inlet valve 151 Catalyst inlet line 15, the pressurized gas inlet pipeline 14 provided with the first valve 141, counterbalance valve 12, safety attachment 13 are included One safety valve 131 and a rupture disk (not shown), the pressure of catalyst storage tank are provided by pressurized gas inlet pipeline 14, by Counterbalance valve 12 is controlled.The bottom of tank body 1 is provided with bottom valve 16, and bottom valve 16 is connected with an outlet line 17, connected on outlet line 17 It is connected to baiting valve 18.
Scavenging conduit group includes the first gases at high pressure blow line 19, the second gases at high pressure blow line 20, and described first is high Calm the anger body blow line 19, the second gases at high pressure blow line 20 is arranged on the outlet line 17 and positioned at baiting valve 18 two ends, the second gases at high pressure blow line 20 draws close to the bottom valve 16, the second gases at high pressure blow line 20 Go out a sampling by-pass line 201, a pressurized gas inlet branch line 202.
Clean pipe group, including cleaning agent suction line 203, cleaning agent outlet line 21, low-pressure gas suction line 22, institute State cleaning agent suction line 203 to draw from the second gases at high pressure blow line 20, the cleaning agent outlet line 21 goes out certainly Mouth pipeline is drawn, and the cleaning agent outlet line 21 is located at after the first gases at high pressure blow line 19, the low-pressure gas Suction line 22 is connected with the top of tank body 1;
Catalyst inlet line 203 is provided with inlet valve, and pressurized gas inlet pipeline is provided with the first valve, gone out in cleaning agent Mouth pipeline 21 is provided with washing outlet valve, and low-pressure gas suction line 22 is provided with the 4th valve, set in the end of outlet line 17 There is outlet valve, outlet valve is arranged between baiting valve and polymer reactor.Pressurized gas inlet branch line 202 is provided with the second valve Door 2021, sampling by-pass line 201 is provided with sampling valve 2011, and the pressure of catalyst storage tank is by from pressurized gas inlet pipeline 14 Gases at high pressure provide, the pressure in catalyst storage tank is controlled by counterbalance valve 12, the pressure of catalyst storage tank and from high pressure gas The pressure of the inner high voltage gas of body suction line 14 is identical.
The temperature control system 2 is covered on the outer surface of tank body 1, and the outside of tank body 1 temperature is controlled by the temperature of temperature-controlling system 2 Degree, temperature-controlling system can be electric heater unit.In present embodiment, described temperature regulating device 2 provides 0~30 DEG C for agent storage tank Temperature.
Agitating device, is connected and extends in the tank body 1 with the top of tank body 1;Agitating device be connected with the top of tank body 1 and Extend in the tank body 1, agitating device 11 includes a motor 111 and the agitator 112 being connected with motor 111, agitator 112 Extend in tank body 1, agitator and the connection of catalyst storage tank seal.
Sampling valve 2011 is only opened when catalyst is sampled, and solid catalyst particle is added through catalyst inlet line 203 To after catalyst storage tank, the sampling valve 2011 on sampling by-pass line 201 is opened, sample analysis chemical examination, sampling analysis chemical examination is extracted Catalyst could be added after qualified into polymer reactor.
When charging system is run, the inertia of setting pressure is passed through into catalyst storage tank by pressurized gas inlet pipeline 14 After gas, the pressure of counterbalance valve 12 is set.Motor 111 and agitator 112 are opened, bottom valve 16 is opened, bottom valve 16 is one Normally opened ball valve, is only closed, rotating blanking valve 18 rotates up splicing, necessarily in cleaning catalyst storage tank or filling catalyst The second valve 2021 on pressurized gas inlet branch line 202 is opened after time, gases at high pressure is purged into catalyst storage tank, prevents The clogging baiting valve 18 in catalyst whereabouts.Rotating blanking valve 18 is rotated down discharging simultaneously, opens the 3rd valve 191 and outlet Outlet valve 171 on line 17, solid particle catalyst is defeated via the gases at high pressure at the first gases at high pressure blow line 19 It is fed into polymer reactor, catalyst storage tank external temperature is controlled by the temperature of temperature regulating device 2, by controlling baiting valve 18 speed controls the inlet amount with metered catalyst.
The baiting valve 18 that the utility model is provided is automatic rotary valve, and its valve body volume is fixed, when baiting valve 18 revolves upwards During transfer material, the second valve 2021 closed on pressurized gas inlet branch line 202 stops purging, pressurized gas inlet branch line 202 It is mainly used in purging into catalyst storage tank, prevents baiting valve 18 to solid catalyst particle during bottom discharge from bottom valve 16 flow out and clogging baiting valve 18.When baiting valve 18 rotates up splicing, the on pressurized gas inlet branch line 202 is opened Two valves 2021, open purging.When baiting valve 18 is rotated down discharging, the on the first gases at high pressure blow line 19 is opened Gases at high pressure are conveyed to outlet line 17 by three valves 191, and the first gases at high pressure blow line 19 and the 3rd valve 191 are main For solid catalyst particle to be delivered into polymer reactor, the pressure from the first gases at high pressure blow line 19 is higher than Catalyst storage tank or the pressure from pressurized gas inlet pipeline 14.
When baiting valve 18 is rotated down discharging, the 3rd valve 191 closed on the first gases at high pressure blow line 19 stops Only purge.In the present embodiment, the pressure phase on the pressure and pressurized gas inlet branch line 202 of the first gases at high pressure blow line 19 Together.Gas used is that the gas not chemically reacted with solid polyolefin hydrocarbon catalyst is for example smart in gases at high pressure blow line One kind in nitrogen or rare gas processed.
Agitator 112 used in the utility model is the helix(ribbon type) agitator with motor, the heating of magnetic stirring apparatus, magnetic force Agitator, hinging type agitator, frequency conversion double layer agitator, propeller mixer, turbine agitator, dasher, anchor formula One kind in agitator.
A specific embodiment explanation is lifted below:
Embodiment 1, such as Fig. 1,500 grams of solid catalyst particles are added into catalyst storage tank, open sampling by-pass line 201 On sampling valve 2011 take out sample, sampling analysis chemical examination it is qualified.The first valve 141 is opened, passes through pressurized gas inlet pipeline 14 are passed through after 2.0MPa purified nitrogen into catalyst storage tank, set the pressure of counterbalance valve 12 as 2.0Mpa, temperature control system Temperature control is at 20 DEG C..The propeller mixer of catalyst storage tank is opened, rotating speed is 20rpm.Bottom valve 16 is opened, using valve Body volume is 0.2L, and rotating blanking valve 18 rotates up splicing.After certain time, open on pressurized gas inlet branch line 202 Second valve 2021, gases at high pressure are purged into catalyst storage tank, prevent the clogging baiting valve 18 in catalyst whereabouts.Rotate simultaneously Baiting valve 18 opens the outlet valve 171 on the 3rd valve 191 and outlet line 17 to bottom discharge, solid particle catalyst via Gases at high pressure at the first gases at high pressure blow line 19 are delivered into polymer reactor, wherein pressurized gas inlet branch Gases at high pressure used are 2.5MPa purified nitrogen (polymer reactor in the gases at high pressure blow line 19 of line 202 and first Pressure 2.0MPa).The 3rd valve 191 and outlet valve 171 are finally closed, a catalyst charge is completed.By controlling baiting valve 18 speed controls the inlet amount with metered catalyst.
Cleaning pipe group is used for cleaning operation when solid polyolefin hydrocarbon catalyst switches online, needs first by catalyst storage tank Catalyst emission displacement is clean, is cleaned with hexane, and new solid polyolefin hydrocarbon catalyst is added again after drying.Clean charging system When, close the 3rd valve 191 and outlet valve.The sampling valve 2011 opened on sampling by-pass line 201 will be remaining in catalyst storage tank After catalyst treatment is clean, stop charging system operating.By counterbalance valve 12 by the Stress control of catalyst storage tank into normal pressure.It is logical Cross hexane and add mouth and valve (15) to catalyst storage tank (12) addition hexane, motor 111, agitator 112 are opened, in agitator Stirring action under carry out cleaning 2~5 minutes after, open the washing outlet valve 211 on cleaning agent outlet line 21, pass through cleaning Hexane in system is emitted into specified containers by agent outlet line 21.Then the 4th valve on low-pressure gas suction line 22 is opened Door 221, is passed through low-pressure nitrogen into catalyst storage tank by low-pressure gas suction line 22 and carries out purging displacement.To ensure cleaning Quality, the above-mentioned cleaning operation of repetition 5~10 times.After cleaning is finished, you can carry out the handover operation of catalyst.
The utility model advantage is:This is new available for the high-end trade mark or temperature sensitive type solid polyolefin catalyst charge, The performance of temperature fluctuations affect catalyst is avoided, cleaning pipe group is added, is easy to line to avoid urging originally when switching new catalyst The pollution that agent is brought;The catalyst stored in catalyst storage tank is stirred using agitator, it is to avoid solid catalyst is bonded and united Or build bridge, catalyst smoothly can be added in feed system;Set on catalyst storage tank bottom pipeline under the rotation of fixed volume Expect valve, the FREQUENCY CONTROL that catalyst charge amount can be rotated by rotating blanking valve, it is ensured that charging system is in running It is middle that the sufficiently stable and accurate control of solid catalyst is added in polymer reactor.Originally it is new in addition to add in each depot siding Fill gases at high pressure blow line, it is to avoid the problem of catalyst deposit on pipeline and everywhere valve, blocked, it is ensured that whole pipeline It is unobstructed, catalyst is stablized, is accurately added in polymer reactor.

Claims (10)

1. a kind of continuous charging system of the solid polyolefin hydrocarbon catalyst of the online switching system of band, it is characterised in that including:
One tank body to hold catalyst, tank body top is provided with safety attachment, pressurized gas inlet pipeline, counterbalance valve, catalysis Agent suction line, bottom valve is provided with tank base, and bottom valve is connected with an outlet line, and the outlet line is provided with blanking Valve;
One scavenging conduit group, including the first gases at high pressure blow line, the second gases at high pressure blow line, first gases at high pressure Blow line, the second gases at high pressure blow line are drawn from the outlet line and positioned at the two ends of baiting valve, described the Two gases at high pressure blow lines are close to the bottom valve, and the second gases at high pressure blow line draws one and samples by-pass line, a high pressure Gas access branch line;
One cleaning pipe group, including cleaning agent suction line, cleaning agent outlet line, low-pressure gas suction line, the cleaning agent Suction line is drawn from the second gases at high pressure blow line, and the cleaning agent outlet line is drawn from outlet line, and institute Cleaning agent outlet line is stated after the first gases at high pressure blow line, the low-pressure gas suction line connects with tank body top It is logical;
One agitating device, is connected and extends in the tank body with tank body top;
One temperature control system, is covered on tank body outer surface.
2. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature It is, the temperature control system is an electric heater unit.
3. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature It is, the safety attachment includes a safety valve and a rupture disk.
4. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature It is, the bottom valve is closed when being a normally opened ball valve, cleaning tank body or filling catalyst.
5. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature Be, pressurized gas inlet branch line be provided with the second valve, sampling by-pass line be provided with sampling valve, cleaning pipeline provided with clean into Mouth valve.
6. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature It is, the agitating device includes a motor and the agitator with motor connection, the agitator is helix(ribbon type) agitator, magnetic force Agitator, magnetic force heating stirrer, hinging type agitator, frequency conversion double layer agitator, propeller mixer, turbine agitator, One of which in dasher, anchor agitator.
7. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature It is, the first gases at high pressure blow line is provided with the 3rd valve.
8. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature Be, in the first described gases at high pressure blow line or the second gases at high pressure blow line gas used be with catalyst not The gas chemically reacted.
9. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature It is, the baiting valve is automatic rotary valve, the volume of automatic rotary valve is fixed.
10. the continuous charging system of the solid polyolefin hydrocarbon catalyst as claimed in claim 1 with online switching system, its feature It is, catalyst inlet line is provided with inlet valve, and pressurized gas inlet pipeline is provided with the first valve, in cleaning agent outlet line Washing outlet valve is provided with, low-pressure gas suction line is provided with the 4th valve, is provided with outlet valve in outlet line end, goes out Mouth valve is arranged between baiting valve and polymer reactor.
CN201621413506.6U 2016-12-21 2016-12-21 The continuous charging system of solid polyolefin hydrocarbon catalyst with online switching system Active CN206549609U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113828188A (en) * 2021-09-10 2021-12-24 中石化石油工程技术服务有限公司 Uniform discharging device for online cleaning of drilling oil-based drilling cuttings feeding device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113828188A (en) * 2021-09-10 2021-12-24 中石化石油工程技术服务有限公司 Uniform discharging device for online cleaning of drilling oil-based drilling cuttings feeding device

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