CN206509303U - Nuclear-magnetism can washing apparatus - Google Patents

Nuclear-magnetism can washing apparatus Download PDF

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Publication number
CN206509303U
CN206509303U CN201621216922.7U CN201621216922U CN206509303U CN 206509303 U CN206509303 U CN 206509303U CN 201621216922 U CN201621216922 U CN 201621216922U CN 206509303 U CN206509303 U CN 206509303U
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CN
China
Prior art keywords
nuclear
magnetism
washing
rinse bath
nuclear magnetic
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Active
Application number
CN201621216922.7U
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Chinese (zh)
Inventor
卞福江
袁永坤
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Suzhou Yacoo Science Co Ltd
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Suzhou Yacoo Science Co Ltd
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Priority to CN201621216922.7U priority Critical patent/CN206509303U/en
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Abstract

The utility model discloses a kind of nuclear-magnetism can washing apparatus, for cleaning nuclear magnetic tube, the nuclear-magnetism can washing apparatus includes a rinse bath, one sealing-plug, if a waste liquid bottle and dry-cleaning liquid conduit, the sealing-plug is fixed between the rinse bath and waste liquid bottle, each washing lotion conduit is fixed on the rinse bath and extends to the waste liquid bottle through the rinse bath and the sealing-plug, the waste liquid bottle is provided with a gas outlet, the nuclear magnetic tube back-off in the washing lotion conduit and forms a gap with the washing lotion conduit, the air in the nuclear-magnetism can washing apparatus is extracted out from the gas outlet, cleaning fluid in the rinse bath flow to the waste liquid bottle along the gap and the washing lotion conduit, the nuclear magnetic tube inner wall washing is clean.Because washing lotion conduit quantity is multiple, therefore nuclear-magnetism can washing apparatus once can both clean many nuclear magnetic tubes, can also clean a nuclear magnetic tube.

Description

Nuclear-magnetism can washing apparatus
Technical field
The utility model is related to cleaning device, more particularly to a kind of nuclear-magnetism can washing apparatus.
Background technology
Nuclear magnetic resonance technique is widely used in respectively such as organic chemistry, pharmaceutical chemistry, biochemistry and polymer chemistry The Structural Identification of section's chemical substance, has become one of most important detection technique of chemical field.Examined using nuclear magnetic resonance technique Need the testing sample of milligram level being placed in nuclear magnetic tube when surveying compound and dissolve, then be placed in NMR and surveyed It is fixed.Because NMR is extremely sensitive, the sample size of detection is generally all micro milligram level, the quality of nuclear magnetic tube and cleaning Degree influences very big to analysis result, it is necessary to assure nuclear magnetic tube is reused after fully cleaning.Nuclear magnetic tube is one kind by quartz glass Elongated thin-walled straight tube, the diameter about 5mm for the end closure being made, length about 153~226mm, cleaning up can be repeatedly Use, but be due to that the thin-walled and slim-lined construction of nuclear magnetic tube causes nuclear magnetic tube easily to crush, cleans difficult.Conventional cleaning now Method has following several:1st, directly scrubbed with elongated hairbrush or swab stick the insertion nuclear magnetic tube for being moistened with cleaning fluid, this mode is cleaned Cleannes are higher afterwards, but can only once clean one, waste time and energy, and easily cause nuclear-magnetism inside pipe wall to produce cut influence inspection Survey result or directly crush and scratch experimenter;2nd, nuclear magnetic tube is placed in supersonic wave cleaning machine and is cleaned by ultrasonic with cleaning fluid, Such a mode can once clean many nuclear magnetic tubes, but such a method need to repeatedly be replaced and cleaned liquid, waste a large amount of solvents, in addition It is concussion cleaning at a high speed due to being cleaned by ultrasonic, also easily causes nuclear magnetic tube to crack broken;3rd, partial monopoly report passes through letter Easy device negative pressure or malleation flush clean nuclear magnetic tube, but this kind equipment is only applicable to ease of solubility material under cleaning normal temperature, for difficulty Soluble substance can not be cleaned, and such negative pressure device usually easily cause nuclear magnetic tube by negative-pressure adsorption it is closed live, it is impossible to suction is clear Washing lotion, causes cleaning not thorough;4th, cleaned using commercially available special nuclear magnetic tube washer, this kind equipment once cleans many Root, but single can not clean, the single cleaning for temporary needs is impracticable, and equipment price is expensive, and inconvenience is mobile quick, Few laboratories are equipped with this kind equipment.
Utility model content
In order to overcome the deficiencies in the prior art, the purpose of this utility model be to provide one kind can once clean many or The nuclear-magnetism can washing apparatus of single nuclear magnetic tube.
The purpose of this utility model is realized using following technical scheme:
A kind of nuclear-magnetism can washing apparatus, for cleaning nuclear magnetic tube, the nuclear-magnetism can washing apparatus includes a rinse bath, one close It is each described to wash if blocking, a waste liquid bottle and dry-cleaning liquid conduit, the sealing-plug are fixed between the rinse bath and waste liquid bottle Fluid catheter is fixed on the rinse bath and extends to the waste liquid bottle, the waste liquid bottle through the rinse bath and the sealing-plug Provided with a gas outlet, the nuclear magnetic tube back-off in the washing lotion conduit and with one gap of washing lotion conduit formation, from it is described go out Gas port extracts the air in the nuclear-magnetism can washing apparatus out, and the cleaning fluid in the rinse bath is along the gap and the washing lotion Conduit flow to the waste liquid bottle, and the nuclear magnetic tube inner wall washing is clean.
It is preferred that, each washing lotion conduit includes a body and an interlayer, and the interlayer is surrounded on the body, described Cleaning fluid is along the bulk flow.
It is preferred that, the interlayer is used for the solution for housing heat, to heat the cleaning fluid in the rinse bath.
It is preferred that, the rinse bath is provided with some grooves, to prevent the nuclear magnetic tube seamless right with the bottom of rinse bath Connect.
Compared with prior art, the beneficial effects of the utility model are:
The nuclear magnetic tube back-off of the utility model nuclear-magnetism can washing apparatus in washing lotion conduit and forms a gap with washing lotion conduit, The air in nuclear-magnetism can washing apparatus is extracted out from gas outlet, the cleaning fluid in rinse bath flow to waste liquid along gap and washing lotion conduit Bottle, nuclear magnetic tube inner wall washing is clean, and because washing lotion conduit quantity is multiple, therefore nuclear-magnetism can washing apparatus once both can be clear Many nuclear magnetic tubes are washed, a nuclear magnetic tube can also be cleaned.
Brief description of the drawings
Fig. 1 is a structural representation of the utility model nuclear-magnetism can washing apparatus.
Fig. 2 is a top view of the utility model nuclear-magnetism can washing apparatus.
Fig. 3 is a use state schematic diagram of the utility model nuclear-magnetism can washing apparatus.
In figure:100th, nuclear-magnetism can washing apparatus;10th, rinse bath;12nd, groove;20th, sealing-plug;30th, waste liquid bottle;32nd, outlet Mouthful;40th, washing lotion conduit;42nd, body;44th, interlayer;200th, nuclear magnetic tube.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the utility model, rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made The every other embodiment obtained, belongs to the scope of the utility model protection.
It should be noted that when component is referred to as " being fixed on " another component, it can be directly on another component Or can also have component placed in the middle.When a component is considered as " connection " another component, it can be directly connected to To another component or it may be simultaneously present component placed in the middle.When a component is considered as " being arranged at " another component, it Can be set directly on another component or may be simultaneously present component placed in the middle.Term as used herein is " vertical ", " level ", "left", "right" and similar statement for illustrative purposes only.
Unless otherwise defined, all of technologies and scientific terms used here by the article is led with belonging to technology of the present utility model The implication that the technical staff in domain is generally understood that is identical.It is herein to be in term used in the description of the present utility model The purpose of description specific embodiment, it is not intended that in limitation the utility model.Term as used herein " and/or " include The arbitrary and all combination of one or more related Listed Items.
Fig. 1 is referred to Fig. 3, a kind of nuclear-magnetism can washing apparatus 100 includes a rinse bath 10, a sealing-plug 20, a waste liquid If bottle 30 and dry-cleaning liquid conduit 40.
The bottom of rinse bath 10 is provided with some grooves 12.The waste liquid bottle 30 is provided with a gas outlet 32.Washed described in each Fluid catheter 40 includes a body 42 and an interlayer 44, and the interlayer 44 is surrounded on the body 42.
When assembling the nuclear-magnetism can washing apparatus 100, the sealing-plug 20 is fixed on the rinse bath 10 and the waste liquid Between bottle 30 and the waste liquid bottle 30 is sealed.The body 42 of the washing lotion conduit 40 runs through the rinse bath 10 and the sealing Plug 20, and extend to the waste liquid bottle 30.The interlayer 44 extends to the bottom of rinse bath 10 and is fixed on the rinse bath 10 bottoms.
During using the nuclear-magnetism can washing apparatus 100, the back-off of a nuclear magnetic tube 200 in washing lotion conduit 40 described in one and with it is described One gap of the formation of washing lotion conduit 40, is extracted out the air in the nuclear-magnetism can washing apparatus 100 by the gas outlet 32, described Body 42 of the cleaning fluid along gap and the washing lotion conduit 40 in rinse bath 10 flow to the waste liquid bottle 30, by the nuclear magnetic tube 200 inner wall washings are clean, and because the quantity of washing lotion conduit 40 is multiple, therefore the nuclear-magnetism can washing apparatus 100 was once both The many nuclear magnetic tubes 200 can be cleaned, a nuclear magnetic tube 200 can also be cleaned.The interlayer 44 is used to house heat Solution, to heat the cleaning fluid in the rinse bath 10.The groove 12 of the rinse bath 10 can make the nuclear magnetic tube 200 and institute State the bottom of rinse bath 10 and leave gap, to prevent the washing lotion conduit 40 can not be drawn onto cleaning fluid.
It will be apparent to those skilled in the art that technical scheme that can be as described above and design, make other various It is corresponding to change and deformation, and all these change and deformation should all belong to the protection of the utility model claim Within the scope of.

Claims (4)

1. a kind of nuclear-magnetism can washing apparatus, for cleaning nuclear magnetic tube, the nuclear-magnetism can washing apparatus includes a rinse bath, its feature It is:If the nuclear-magnetism can washing apparatus also includes a sealing-plug, a waste liquid bottle and dry-cleaning liquid conduit, the sealing-plug is fixed on Between the rinse bath and waste liquid bottle, each washing lotion conduit is fixed on the rinse bath and runs through the rinse bath and described Sealing-plug extends to the waste liquid bottle, and the waste liquid bottle is provided with a gas outlet, the nuclear magnetic tube back-off in the washing lotion conduit simultaneously With one gap of washing lotion conduit formation, the air in the nuclear-magnetism can washing apparatus is extracted out from the gas outlet, it is described clear Cleaning fluid in washing trough flow to the waste liquid bottle along the gap and the washing lotion conduit, and the nuclear magnetic tube inner wall washing is done Only.
2. nuclear-magnetism can washing apparatus according to claim 1, it is characterised in that:Each washing lotion conduit includes a body And an interlayer, the interlayer is surrounded on the body, and the cleaning fluid is along the bulk flow.
3. nuclear-magnetism can washing apparatus according to claim 2, it is characterised in that:The interlayer is used for the solution for housing heat, To heat the cleaning fluid in the rinse bath.
4. nuclear-magnetism can washing apparatus according to claim 1, it is characterised in that:The rinse bath is provided with some grooves, with Prevent the nuclear magnetic tube and the bottom of rinse bath slitless connection.
CN201621216922.7U 2016-11-11 2016-11-11 Nuclear-magnetism can washing apparatus Active CN206509303U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621216922.7U CN206509303U (en) 2016-11-11 2016-11-11 Nuclear-magnetism can washing apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621216922.7U CN206509303U (en) 2016-11-11 2016-11-11 Nuclear-magnetism can washing apparatus

Publications (1)

Publication Number Publication Date
CN206509303U true CN206509303U (en) 2017-09-22

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Application Number Title Priority Date Filing Date
CN201621216922.7U Active CN206509303U (en) 2016-11-11 2016-11-11 Nuclear-magnetism can washing apparatus

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113695304A (en) * 2020-05-22 2021-11-26 兰州大学 Nuclear magnetic pipe cleaner and cleaning method
CN113798294A (en) * 2021-09-15 2021-12-17 苏州源展材料科技有限公司 Apparatus and method for cleaning reaction vessel

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113695304A (en) * 2020-05-22 2021-11-26 兰州大学 Nuclear magnetic pipe cleaner and cleaning method
CN113695304B (en) * 2020-05-22 2023-03-14 兰州大学 Nuclear magnetic pipe cleaner and cleaning method
CN113798294A (en) * 2021-09-15 2021-12-17 苏州源展材料科技有限公司 Apparatus and method for cleaning reaction vessel

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GR01 Patent grant
GR01 Patent grant
CP02 Change in the address of a patent holder
CP02 Change in the address of a patent holder

Address after: 215000 No. 388 Shui Shui Road, Suzhou Industrial Park, Jiangsu

Patentee after: SUZHOU YACOO SCIENCE Co.,Ltd.

Address before: 215000 Changyang street, Suzhou Industrial Park, Jiangsu, China, No. 415, No.

Patentee before: SUZHOU YACOO SCIENCE Co.,Ltd.