CN206500139U - A kind of new ammonification ureaformaldehyde dual control reactor - Google Patents

A kind of new ammonification ureaformaldehyde dual control reactor Download PDF

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Publication number
CN206500139U
CN206500139U CN201720106976.6U CN201720106976U CN206500139U CN 206500139 U CN206500139 U CN 206500139U CN 201720106976 U CN201720106976 U CN 201720106976U CN 206500139 U CN206500139 U CN 206500139U
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China
Prior art keywords
ureaformaldehyde
dog
house
reative cell
ammonification
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Expired - Fee Related
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CN201720106976.6U
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Chinese (zh)
Inventor
高建国
王恒涛
王广照
胡顺强
张生华
孙运宏
王顶强
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Individual
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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fertilizers (AREA)

Abstract

The utility model provides a kind of new ammonification ureaformaldehyde dual control reactor, belong to chemical reaction engineering device technique field, including shell, ureaformaldehyde reative cell and aminating reaction room, described enclosure is provided with ureaformaldehyde reative cell and aminating reaction room, the top of described ureaformaldehyde reative cell is provided with motor one and dog-house, motor one is connected with agitating shaft by shaft coupling, shaft coupling is provided with distributing disc, the bottom of described aminating reaction room is provided with motor two and discharging opening, top is provided with dog-house three, coil pipe is respectively equipped between described shell and reative cell, one end of opening is connected with air inlet, the other end respectively with upper gas outlet, lower gas outlet is connected.The beneficial effects of the utility model are:Using the design method of dual control integrated form, ureaformaldehyde and aminating reaction kettle are merged so that two procedures can be carried out continuously, improve production efficiency and product quality, simultaneously using identical steam heating passage, auxiliary equipment is reduced, production cost has been saved.

Description

A kind of new ammonification ureaformaldehyde dual control reactor
Technical field
The utility model is related to chemical reaction engineering device technique field, more particularly to a kind of new ammonification ureaformaldehyde dual control reaction Device.
Background technology
In the production of ureaformaldehyde ammonification composite fertilizer, it is necessary first to which urea and formaldehyde hybrid reaction are generated in the middle of ureaformaldehyde Body, is then granulated by aminating reaction, and existing production equipment is mainly free-standing reactor, does not possess continuous life mostly Production capacity power, i.e. ureaformaldehyde and aminating reaction need to carry out interruption transfer, undoubtedly cause production efficiency reduction, and reaction speed is slow, influence The raising of product quality.
Utility model content
The utility model provides a kind of new ammonification ureaformaldehyde dual control reactor, using the design method of dual control integrated form, Organically ureaformaldehyde reactor and aminating reaction kettle are merged so that two procedures can be carried out continuously, and be substantially increased Production efficiency and product quality, while heating passage using identical steam, reduce auxiliary equipment, have saved production cost.
In order to solve the above technical problems, the embodiment of the present application provides a kind of new ammonification ureaformaldehyde dual control reactor, including Shell, ureaformaldehyde reative cell and aminating reaction room, it is characterised in that described enclosure is sequentially provided with ureaformaldehyde reaction from top to bottom Room and aminating reaction room, centre were connected provided with dividing plate and by communicating pipe, and the top of described ureaformaldehyde reative cell is provided with driving electricity Machine one and dog-house one, dog-house two, described motor one are connected with agitating shaft by shaft coupling, and shaft coupling is provided with Distributing disc, the other end of agitating shaft is provided with upper agitator, and the bottom of described aminating reaction room is provided with motor two and discharging Mouthful, driving electronic two is connected by shaft coupling with lower agitator, and the top of aminating reaction room is provided with dog-house three, and described is outer Be respectively equipped with coil pipe between shell and ureaformaldehyde reative cell and aminating reaction room, coil pipe be divided into above and below two parts, one end passes through three-way pipe It is connected with air inlet, the other end is connected with upper gas outlet, lower gas outlet respectively.
As the preferred embodiment of this programme, described dog-house one, dog-house two and dog-house three is respectively that urea is thrown Material mouth, formaldehyde dog-house and ammoniacal liquor dog-house, wherein dog-house two are located in the diameter range of distributing disc, and dog-house one, which is located at, to be divided Outside cloth disk.
As the preferred embodiment of this programme, the surface of described distributing disc is circumferentially uniformly provided with some through holes.
As the preferred embodiment of this programme, described communicating pipe is provided with solenoid electric valve one.
As the preferred embodiment of this programme, the triple valve that described air inlet is connected with coil pipe is provided with Electromagnetic Control Valve two.
As the preferred embodiment of this programme, outside described ureaformaldehyde reative cell and aminating reaction room wall in axial direction on Provided with temperature sensor, at least provided with three temperature sensors on each reative cell.
The one or more technical schemes provided in the embodiment of the present application, have at least the following technical effects or advantages:
Using the design method of dual control integrated form, organically ureaformaldehyde reactor and aminating reaction kettle are merged, made Obtaining two procedures can be carried out continuously, and substantially increase production efficiency and product quality, while being heated using identical steam logical Road, reduces auxiliary equipment, has saved production cost.
Brief description of the drawings
, below will be to embodiment in order to illustrate more clearly of the utility model embodiment or technical scheme of the prior art Or the accompanying drawing used required in description of the prior art is briefly described, it should be apparent that, drawings in the following description are only Some embodiments of the present utility model, for those of ordinary skill in the art, are not paying the premise of creative labor Under, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the structural representation of the embodiment of the present application.
In Fig. 1:1st, shell, 2, shaft coupling, 3, coil pipe, 4, dog-house three, 5, solenoid electric valve one, 6, communicating pipe, 7, on Agitator, 8, agitating shaft, 9, distributing disc, 10, dog-house one, 11, dog-house two, 12, motor one, 13, ureaformaldehyde reative cell, 14th, upper gas outlet, 15, temperature sensor, 16, air inlet, 17, solenoid electric valve two, 18, aminating reaction room, 19, lower outlet Mouthful, 20, lower agitator, 21, motor two, 22, discharging opening.
Embodiment
The utility model provides a kind of new ammonification ureaformaldehyde dual control reactor, using the design method of dual control integrated form, Organically ureaformaldehyde reactor and aminating reaction kettle are merged so that two procedures can be carried out continuously, and be substantially increased Production efficiency and product quality, while heating passage using identical steam, reduce auxiliary equipment, have saved production cost.
In order to be better understood from above-mentioned technical proposal, below in conjunction with Figure of description and specific embodiment to upper Technical scheme is stated to be described in detail.
As shown in figure 1, a kind of new ammonification ureaformaldehyde dual control reactor, including shell 1, ureaformaldehyde reative cell 13 and aminating reaction Ureaformaldehyde reative cell 13 and aminating reaction room 18 are sequentially provided with inside room 18, described shell 1 from top to bottom, centre is provided with dividing plate simultaneously It is connected by communicating pipe 6, the top of described ureaformaldehyde reative cell 13 is provided with motor 1 and dog-house 1, dog-house two 11, described motor 1 is connected with agitating shaft 8 by shaft coupling 2, and shaft coupling 2 is provided with distributing disc 9, agitating shaft 8 The other end be provided with upper agitator 7, the bottom of described aminating reaction room 18 is provided with motor 2 21 and discharging opening 22, driving Electronic 2 21 are connected by shaft coupling 2 with lower agitator 20, and the top of aminating reaction room 18 is provided with dog-house 34, described Coil pipe 3 is respectively equipped between shell 1 and ureaformaldehyde reative cell 13 and aminating reaction room 18,3 points of coil pipe is two parts up and down, and one end leads to Cross three-way pipe with air inlet 16 to be connected, the other end is connected with upper gas outlet 14, lower gas outlet 19 respectively.
Wherein, in actual applications, described dog-house 1, dog-house 2 11 and dog-house 34 are respectively that urea is thrown Material mouth, formaldehyde dog-house and ammoniacal liquor dog-house, wherein dog-house 2 11 are located in the diameter range of distributing disc 9, dog-house 1 Outside distributing disc 9.
Wherein, in actual applications, the surface of described distributing disc 9 is circumferentially uniformly provided with some through holes, from throwing Material mouth 1 and dog-house 2 11 put into urea and formaldehyde in proportion respectively, and the formaldehyde of input falls directly into ureaformaldehyde reative cell 13 Bottom, the urea of input is fallen into distributing disc 9, and is thrown away urea by the centrifugal force of rotation, uniform unrestrained so that urea and Formaldehyde mixing is more uniform.
Wherein, in actual applications, described communicating pipe 6 is provided with solenoid electric valve 1, Electromagnetic Control after the completion of reaction Valve 1 is automatically opened up so that ureaformaldehyde obtains twice work by being flowed into progress next step reaction in aminating reaction room 18 communicating pipe 6 Sequence can be carried out continuously, and substantially increase production efficiency and product quality.
Wherein, in actual applications, the triple valve that described air inlet 16 is connected with coil pipe 3 is provided with solenoid electric valve 2 17, by adjusting the solenoid electric valve 2 17 in each branch, the intake of steam can be adjusted, so as to adjust two reative cells Interior temperature, makes it have optimal reaction temperature respectively.
Wherein, in actual applications, described ureaformaldehyde reative cell 13 and the outside wall surface of aminating reaction room 18 in axial direction on Provided with temperature sensor 15, at least provided with three temperature sensors 15, the temperature positioned at different height of setting on each reative cell Spending sensor 15 is used for the temperature detection to the material in different height, and temperatures above output cannot be only used for technological parameter prison Control, while the adjustment of agitator 7 and the lower gradient of agitator 20 can be instructed in process, with to be applied to different material and Different process index.
It is described above, only it is preferred embodiment of the present utility model, not makees any formal to the utility model Limitation, although the utility model is disclosed above with preferred embodiment, but is not limited to the utility model, any ripe Professional and technical personnel is known, is not being departed from the range of technical solutions of the utility model, when in the technology using the disclosure above Hold the equivalent embodiment made a little change or be modified to equivalent variations, as long as without departing from technical solutions of the utility model Hold, any simple modification, equivalent variations and the modification made according to technical spirit of the present utility model to above example, still Belong in the range of technical solutions of the utility model.

Claims (6)

1. a kind of new ammonification ureaformaldehyde dual control reactor, including shell (1), ureaformaldehyde reative cell (13) and aminating reaction room (18), Characterized in that, ureaformaldehyde reative cell (13) and aminating reaction room (18) are sequentially provided with from top to bottom inside described shell (1), in Between be connected provided with dividing plate and by communicating pipe (6), the top of described ureaformaldehyde reative cell (13) provided with motor one (12) and Dog-house one (10), dog-house two (11), described motor one (12) are connected with agitating shaft (8) by shaft coupling (2), Shaft coupling (2) is provided with distributing disc (9), and the other end of agitating shaft (8) is provided with upper agitator (7), described aminating reaction room (18) bottom is provided with motor two (21) and discharging opening (22), and motor two (21) passes through shaft coupling (2) and lower stirring Device (20) is connected, and the top of aminating reaction room (18) is provided with dog-house three (4), described shell (1) and ureaformaldehyde reative cell (13) be respectively equipped with coil pipe (3) between aminating reaction room (18), coil pipe (3) be divided into above and below two parts, one end passes through three-way pipe It is connected with air inlet (16), the other end is connected with upper gas outlet (14), lower gas outlet (19) respectively.
2. a kind of new ammonification ureaformaldehyde dual control reactor according to claim 1, it is characterised in that described dog-house one (10), dog-house two (11) and dog-house three (4) are respectively urea dog-house, formaldehyde dog-house and ammoniacal liquor dog-house, wherein throwing Material mouth two (11) is located in the diameter range of distributing disc (9), and dog-house one (10) is located at outside distributing disc (9).
3. a kind of new ammonification ureaformaldehyde dual control reactor according to claim 1, it is characterised in that described distributing disc (9) surface is circumferentially uniformly provided with some through holes.
4. a kind of new ammonification ureaformaldehyde dual control reactor according to claim 1, it is characterised in that described communicating pipe (6) it is provided with solenoid electric valve one (5).
5. a kind of new ammonification ureaformaldehyde dual control reactor according to claim 1, it is characterised in that described air inlet (16) triple valve being connected with coil pipe (3) is provided with solenoid electric valve two (17).
6. a kind of new ammonification ureaformaldehyde dual control reactor according to claim 1, it is characterised in that described ureaformaldehyde reaction Room (13) and aminating reaction room (18) outside wall surface are in axial direction provided with temperature sensor (15), each reative cell and at least set There are three temperature sensors (15).
CN201720106976.6U 2017-02-04 2017-02-04 A kind of new ammonification ureaformaldehyde dual control reactor Expired - Fee Related CN206500139U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201720106976.6U CN206500139U (en) 2017-02-04 2017-02-04 A kind of new ammonification ureaformaldehyde dual control reactor

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CN206500139U true CN206500139U (en) 2017-09-19

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109046210A (en) * 2018-09-05 2018-12-21 惠州市丰源钢结构有限公司 A kind of steel construction chemical reaction kettle
CN112691633A (en) * 2021-01-28 2021-04-23 盐城仁恒化工有限公司 Equipment and method for producing ethylenediamine tetraacetic acid by using hydrocyanic acid and ethylenediamine as raw materials

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109046210A (en) * 2018-09-05 2018-12-21 惠州市丰源钢结构有限公司 A kind of steel construction chemical reaction kettle
CN112691633A (en) * 2021-01-28 2021-04-23 盐城仁恒化工有限公司 Equipment and method for producing ethylenediamine tetraacetic acid by using hydrocyanic acid and ethylenediamine as raw materials

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170919

Termination date: 20220204

CF01 Termination of patent right due to non-payment of annual fee