CN206143101U - Used high -efficient environmental protection reation kettle in pyraclostrobin production process - Google Patents
Used high -efficient environmental protection reation kettle in pyraclostrobin production process Download PDFInfo
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- CN206143101U CN206143101U CN201621144849.7U CN201621144849U CN206143101U CN 206143101 U CN206143101 U CN 206143101U CN 201621144849 U CN201621144849 U CN 201621144849U CN 206143101 U CN206143101 U CN 206143101U
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- kettle
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- environment friendly
- puddler
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
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Abstract
The utility model provides an used high -efficient environmental protection reation kettle in pyraclostrobin production process, include: the cauldron body, its upper end are equipped with inlet pipe, an installation through -hole, and the discharging pipe is established to the lower extreme, and the sampling tube is established to lower part one side, pressing from both sides and overlapping, the external side of cauldron is located to the cover, and forms a cavity between the external wall of cauldron, and it has anticorrosive coating, heat preservation and waterproof layer by lower supreme coating in proper order to press from both sides the cover internal surface, the stirring unit is including motor, puddler, stirring rake, the heating unit includes to add the hot -fluid storage tank and set up in the heat -insulating material that adds who adds hot -fluid storage tank inboard, cooling unit, including cooling fluid storage tank and refrigerating coil, refrigerating coil sets up on the puddler. Reation kettle can effectively prevent the cross contamination of raw materials, and the heating, the cooling method environmental protection is controllable and control is accurate, and thermal insulation performance is good, does benefit to the intensive mixing of pyraclostrobin raw materials, and reaction condition control accurately, does benefit to to improve productivity and yield, and is energy -concerving and environment -protective, improvement economic benefits.
Description
Technical field
This utility model is related to high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process.
Background technology
Pyraclostrobin is a kind of methoxy acrylic new type bactericide, is new-type wide-spectrum bactericide, the mechanism of action
For mitochondrial respiratory inhibitor, prevent mitochondrion from producing and providing the energy needed for cell homergy, ultimately result in cell
It is dead.
It can suppress fungus-caused most of diseases such as crop Ascomycetes, Basidiomycetess, deuteromycetes, Oomycete.
Growth to spore germination and mycelia has very strong inhibitory action, with protection and therapeutic activity.With in permeability and local
Activity is inhaled, the lasting period is long, resistance of rainwater washing against.It is widely used in preventing and treating Semen Tritici aestivi, Oryza sativa L., Semen arachidis hypogaeae, Fructus Vitis viniferae, vegetable, Rhizoma Solani tuber osi, perfume (or spice)
Disease on any of several broadleaf plants, Fructus Citri Limoniae, coffee, fruit tree, Semen Juglandiss, Camellia sinensis, Nicotiana tabacum L. and ornamental plant, lawn and other field crops.
Not only toxicity is low for the antibacterial, to non-target organism safety and friendly to user and environment safety, by
U.S. EPA Environmental Protection Agency is classified as " Candidate Agents for reducing risk ".
Reactor is combined reaction container, according to design of the reaction condition to reactor structure function and configuration adnexa.From
Charging-reaction-the discharging of beginning can complete pre-set reactions steps with higher automaticity, to reacting
Temperature, pressure, mechanics control in journey（Stirring, air blast etc.）, the important parameter such as reactant/product concentration carry out strict tune
Control.Its structure is typically made up of kettle, actuating device, agitating device, heater, chiller, sealing device.
Important container of the reactor as raw material mixing, reaction in pyraclostrobin production process, the quality of its performance are straight
Connecing affects the yield and yield of pyraclostrobin, however, existing pyraclostrobin production reactor, and not according to pyrazoles ether bacterium
The production technology of ester is made to measure, and charge door is very few, causes raw material just to occur mixing during charging, affects yield and pure
Degree, temperature control are inaccurate, and fluctuating margin is big, affect larger to reaction.
It is for pyraclostrobin production reactor, more rare, and for reactor, the current country is primarily present as follows
Patent documentation：
Chinese patent Authorization Notice No.：CN205127931U, discloses a kind of water of 2- chloro-5-chloromethyl thiazoles reactor
Cycle heating device, including reactor, the inside of reactor have heating rod mounting bracket, are provided with heating rod mounting bracket
One circle electrically heated rod；An external kettle body is provided with the outside of the kettle wall of reactor, the upper end of reactor is provided with steam outlet interface, described
Steam outlet interface upper end is connected with a solid-liquid separator, and solid-liquid separator is connected with U-shaped exhaust gas heat exchanging pipe, and U-shaped aerofluxuss are changed
The outer helical of heat pipe is provided with recuperated cycle pipe, and the two ends of recuperated cycle pipe are by pipeline communication in the external kettle body
Water valve and circulating pump are installed in portion, and recuperated cycle pipe, liquid supplementation pipe on the downside of external kettle body, is provided with.The water that this utility model is adopted
Cycle heating device can be to carrying out isothermal holding in reactor, and the recirculated water of external kettle body is by producing with reactor operation
Raw steam is exchanged heat, and substantially increases energy utilization rate, improves the work efficiency of reactor.However, the patent is provided
The water circulation attemperator of reactor be to be incubated by water circulation, exchanged heat to following by the steam produced with kettle
Ring water is heated, however, the water-cycling mode is to the control of temperature and inaccurate, no cooling measure, and heat-insulating property has
Wait to discuss.
Utility model content
To solve above-mentioned problem, the purpose of this utility model is to provide in a kind of pyraclostrobin production process
High-efficiency environment friendly reactor used, the reactor can effectively prevent the cross-contamination of raw material, heating, type of cooling environmental protection it is controllable and
Control is accurate, good heat insulating, and beneficial to being sufficiently mixed for pyraclostrobin raw material, reaction condition control is accurate, produces beneficial to improving
Rate and yield, energy-conserving and environment-protective are increased economic efficiency.
To reach above-mentioned purpose, the technical solution of the utility model is：
High-efficiency environment friendly reactor used in a kind of pyraclostrobin production process, including：Kettle, its upper end are provided with least one
Individual feed pipe is simultaneously provided with an installation through-hole, and lower end sets out expects pipe, and bottom side sets probe tube；Chuck, is sheathed on outside the kettle
Side, and a cavity is formed between kettle outer wall, offer on chuck and kettle feed pipe, installation through-hole, discharge nozzle and sampling
The corresponding through hole of pipe, chuck inner surface are sequentially coated with anticorrosive coat, heat-insulation layer and waterproof layer from the bottom to top；Agitating unit,
The puddler connected including motor, one end and motor output shaft, the stirring paddle for being arranged at the puddler other end, the motor are located at
Above kettle, puddler is stretched on the inside of kettle by installation through-hole with respect to the other end of motor, stirring paddle be located at kettle on the inside of
Stirring boom end connection；Heating unit, is arranged at kettle side, including heats fluid reservoir and be arranged at heating fluid reservoir
The heating member of inner side, its liquid outlet and liquid return hole connect to form circulation with the cavity by pipeline respectively；Cooling unit, is arranged
Connected with cooling fluid storage tank liquid outlet, liquid return hole by pipeline in kettle side, including cooling fluid storage tank and two ends respectively
Refrigerating coil, the refrigerating coil is arranged on the agitating unit puddler on the inside of kettle.
Further, the quantity of the enterprising expects pipe of the kettle is 2 ~ 3.
Separately, it is additionally provided with the kettle for monitoring the temperature measurement unit of kettle internal temperature.
Separately have, the anticorrosive coat is epoxy composite material coating or epoxy novolac coating.
Again, the waterproof layer is vaseline primer coating.
Further, the heat-insulation layer is sprayed by ZS-1 thermostable heat-isolating coatings being formed.
And, the pipeline between the heating fluid reservoir liquid outlet and cavity is provided with first flow valve and first flow
Pump, the pipeline between liquid return hole and cavity are provided with first time liquid pump, and the heating fluid in the heating fluid reservoir is for originally
Water.
Separately, second flow valve and second flow pump are set on the pipeline between the cooling fluid storage tank liquid outlet and kettle,
Pipeline between liquid return hole and kettle is provided with second time liquid pump, and the cooling fluid in the cooling fluid storage tank is freezing salt
Water.
Again, the refrigerating coil spirals along puddler length direction and is arranged on puddler.
Further, the feed pipe is provided with inlet valve, discharge nozzle is provided with outlet valve, and probe tube is provided with sampling valve.
The beneficial effects of the utility model are：
The reactor arranges multiple feed pipes, can effectively prevent the cross-contamination of raw material；Probe tube is set, can be taken at any time
Sample is analyzed, beneficial to raising yield；Using add water into the cavity between chuck and kettle mode is heated to kettle, meet
Heating-up temperature in pyraclostrobin production process needs, and water reusable edible, energy-conserving and environment-protective；Using refrigerating coil to kettle
Interior mixed solution is cooled down, and, used as cooling medium, type of cooling environmental protection is controllable for chilled brine；Temperature is set and surveys material part,
Monitoring kettle internal temperature change in time, by first, second flow valve, first, second flow pump control hot water, cold water stream
Amount, control are accurate；Jackets inner wall sets gradually anticorrosive coat, heat-insulation layer and waterproof layer, and anti-corrosion, insulation and water resistance are good, have
Effect lifts reactor service life, coordinates agitating unit, beneficial to being sufficiently mixed for pyraclostrobin raw material, reaction condition control essence
Really, beneficial to yield and yield, energy-conserving and environment-protective are improved, be conducive to increasing economic efficiency, reduce production cost.
Description of the drawings
Fig. 1 is the knot of high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process provided by the utility model
Structure schematic diagram.
Specific embodiment
This utility model is described further below by specific embodiment, but embodiment is not intended to limit this practicality newly
The protection domain of type.
With reference to Fig. 1, high-efficiency environment friendly reactor used, bag in a kind of pyraclostrobin production process described in the utility model
Include：Kettle 1, its upper end are provided with least one feed pipe 11 and are provided with an installation through-hole 12, and lower end sets out expects pipe 13, bottom side
If probe tube 14；Chuck 2, is sheathed on the outside of the kettle 1, and a cavity 3 is formed between 1 outer wall of kettle, opens up on chuck 2
There is the through hole corresponding with 1 feed pipe 11 of kettle, installation through-hole 12, discharge nozzle 13 and probe tube 14（It is not shown）, table in chuck 2
Face is sequentially coated with anticorrosive coat 21, heat-insulation layer 22 and waterproof layer 23 from the bottom to top；Agitating unit 4, including motor 41, one end with
The puddler 42 of 41 output shaft of motor connection, the stirring paddle 43 for being arranged at 42 other end of puddler, the motor 41 are located at kettle 1
Top, the other end of the relative motor 41 of puddler 42 are stretched on the inside of kettle 1 by installation through-hole 12, stirring paddle 43 with positioned at kettle
42 end of puddler connection on the inside of 1；Heating unit 5, is arranged at 1 side of kettle, including heats fluid reservoir 51 and be arranged at
Heating member 52 on the inside of heating fluid reservoir 51, its liquid outlet 53 and liquid return hole 54 are connected with the cavity 3 by pipeline respectively
Form circulation；Cooling unit 6, is arranged at 1 side of kettle, including cooling fluid storage tank 61 and two ends respectively by pipeline and cooling
61 liquid outlet 62 of fluid reservoir, the refrigerating coil 64 of the connection of liquid return hole 63, the refrigerating coil 64 are arranged on the inside of kettle 1
4 puddler 42 of agitating unit on.
Further, the quantity of 1 enterprising expects pipe 11 of the kettle is 2 ~ 3.
Separately, it is additionally provided with the kettle 1 for monitoring the temperature measurement unit 15 of 1 internal temperature of kettle.
Separately have, the anticorrosive coat 21 is epoxy composite material coating or epoxy novolac coating.
Again, the waterproof layer 23 is vaseline primer coating.
Further, the heat-insulation layer 22 is sprayed by ZS-1 thermostable heat-isolating coatings being formed.
And, the pipeline between heating 51 liquid outlet 53 of fluid reservoir and cavity 3 is provided with first flow valve 55 and the
One flow pump 56, the pipeline between liquid return hole 54 and cavity 3 are provided with first time liquid pump 57, in the heating fluid reservoir 51
Heating fluid is tap water.
Separately, second flow valve 65 and second is set on the pipeline between 61 liquid outlet 62 of the cooling fluid storage tank and kettle 1
Flow pump 66, the pipeline between liquid return hole 63 and kettle 1 are provided with second time liquid pump 67, cold in the cooling fluid storage tank 61
But fluid is chilled brine.
Again, the refrigerating coil 64 spirals along 42 length direction of puddler and is arranged on puddler 42.
Further, the feed pipe 11 is provided with inlet valve 111, discharge nozzle 13 is provided with outlet valve 131, sets on probe tube 14
There is sampling valve 141.
High-efficiency environment friendly reactor used, the reactor in a kind of pyraclostrobin production process described in the utility model
Multiple feed pipes are set, the cross-contamination of raw material can be effectively prevented；Using into the cavity between chuck and kettle adding water square
Formula is heated to kettle, meets the heating-up temperature needs in pyraclostrobin production process, and water reusable edible, energy-saving ring
Protect；The mixed solution in kettle is cooled down using refrigerating coil, used as cooling medium, type of cooling environmental protection can for chilled brine
Control；Temperature is set and surveys material part, in time the change of monitoring kettle internal temperature, by first, second flow valve, first, second stream
Amount pump control hot water, cold water flow, control are accurate；Jackets inner wall sets gradually anticorrosive coat, heat-insulation layer and waterproof layer, anti-corrosion,
Insulation and water resistance are good, effectively lift reactor service life, coordinate agitating unit, beneficial to the abundant of pyraclostrobin raw material
Mixing, reaction condition control are accurate, beneficial to yield and yield, energy-conserving and environment-protective are improved, are conducive to increasing economic efficiency, and reduce production
Cost.
It should be noted that above example is only to illustrate the technical solution of the utility model and unrestricted.Although ginseng
This utility model is described in detail according to preferred embodiment, it will be understood by those within the art that, can be to reality
Modified with new technical scheme or equivalent, without deviating from the scope of technical solutions of the utility model, which all should
Cover in right of the present utility model.
Claims (10)
1. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process, it is characterised in that include：
Kettle, its upper end are provided with least one feed pipe and are provided with an installation through-hole, and lower end sets out expects pipe, and bottom side sets sampling
Pipe；
Chuck, is sheathed on the outside of the kettle, and a cavity is formed between kettle outer wall, offers and feed with kettle on chuck
The corresponding through hole of pipe, installation through-hole, discharge nozzle and probe tube, chuck inner surface are sequentially coated with anticorrosive coat from the bottom to top, protect
Warm layer and waterproof layer；
Agitating unit, including motor, one end and motor output shaft puddler for connecting, the stirring for being arranged at the puddler other end
Oar, the motor are located above kettle, and puddler is stretched on the inside of kettle by installation through-hole with respect to the other end of motor, stirring paddle
It is connected with the stirring boom end on the inside of kettle；
Heating unit, is arranged at kettle side, including heating fluid reservoir and the heating member being arranged on the inside of heating fluid reservoir,
Its liquid outlet and liquid return hole connect to form circulation with the cavity by pipeline respectively；
Cooling unit, is arranged at kettle side, including cooling fluid storage tank and two ends respectively by pipeline and cooling fluid storage tank
Liquid outlet, the refrigerating coil of liquid return hole connection, the refrigerating coil are arranged on the agitating unit puddler on the inside of kettle.
2. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In the quantity of the enterprising expects pipe of the kettle is 2 ~ 3.
3. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In being additionally provided with the kettle for monitoring the temperature measurement unit of kettle internal temperature.
4. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In the anticorrosive coat is epoxy composite material coating or epoxy novolac coating.
5. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In the waterproof layer is vaseline primer coating.
6. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In the heat-insulation layer is sprayed by ZS-1 thermostable heat-isolating coatings and formed.
7. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In the pipeline between the heating fluid reservoir liquid outlet and cavity is provided with first flow valve and first flow pump, liquid return hole
Pipeline between cavity is provided with first time liquid pump, and the heating fluid in the heating fluid reservoir is tap water.
8. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In, set second flow valve and second flow pump on the pipeline between the cooling fluid storage tank liquid outlet and kettle, liquid return hole with
Pipeline between kettle is provided with second time liquid pump, and the cooling fluid in the cooling fluid storage tank is chilled brine.
9. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In the refrigerating coil spirals along puddler length direction and is arranged on puddler.
10. high-efficiency environment friendly reactor used in a kind of pyraclostrobin production process according to claim 1, its feature exist
In the feed pipe is provided with inlet valve, and discharge nozzle is provided with outlet valve, and probe tube is provided with sampling valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621144849.7U CN206143101U (en) | 2016-10-21 | 2016-10-21 | Used high -efficient environmental protection reation kettle in pyraclostrobin production process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621144849.7U CN206143101U (en) | 2016-10-21 | 2016-10-21 | Used high -efficient environmental protection reation kettle in pyraclostrobin production process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206143101U true CN206143101U (en) | 2017-05-03 |
Family
ID=58621873
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621144849.7U Expired - Fee Related CN206143101U (en) | 2016-10-21 | 2016-10-21 | Used high -efficient environmental protection reation kettle in pyraclostrobin production process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206143101U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107348826A (en) * | 2017-09-22 | 2017-11-17 | 太仓市林港农场专业合作社 | A kind of durable mill of black garlic anti-corrosion |
| CN111530400A (en) * | 2020-05-16 | 2020-08-14 | 巫仁科 | Environment-friendly chemical production cooling reation kettle |
-
2016
- 2016-10-21 CN CN201621144849.7U patent/CN206143101U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107348826A (en) * | 2017-09-22 | 2017-11-17 | 太仓市林港农场专业合作社 | A kind of durable mill of black garlic anti-corrosion |
| CN111530400A (en) * | 2020-05-16 | 2020-08-14 | 巫仁科 | Environment-friendly chemical production cooling reation kettle |
| CN111530400B (en) * | 2020-05-16 | 2020-12-22 | 宁夏宏民生物科技有限公司 | Environment-friendly chemical production cooling reation kettle |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20181219 Address after: 224500 Kaitai Road, Coastal Industrial Park, Binhai County Development Zone, Yancheng City, Jiangsu Province Patentee after: JIANGSU TUOQIU AGRICULTURE CHEMICAL Co.,Ltd. Address before: No. 32 Renmin Road, Dongkan Town, Binhai County, Yancheng City, Jiangsu Province Co-patentee before: Liu Bin Patentee before: Pan Hong |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170503 Termination date: 20211021 |