CN206127177U - Extraction device of tetrahexose monosialogandlioside sodium of high -purity - Google Patents
Extraction device of tetrahexose monosialogandlioside sodium of high -purity Download PDFInfo
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- CN206127177U CN206127177U CN201621103533.3U CN201621103533U CN206127177U CN 206127177 U CN206127177 U CN 206127177U CN 201621103533 U CN201621103533 U CN 201621103533U CN 206127177 U CN206127177 U CN 206127177U
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Abstract
The utility model provides an extraction device of tetrahexose monosialogandlioside sodium of high -purity, including condenser, extraction bottle and the solvent bottle who connects gradually, extract the bottle bottom through the pipeline with solvent bottle connects, it is equipped with the steam pipe to extract bottle one side, be equipped with level sensor on the extraction bottle inside wall, be equipped with the check valve in the pipeline, be equipped with the controller on the extraction bottle lateral wall, the check valve level sensor all with the communication of controller looks, the bottom transversely is equipped with at a distance from the net in extracting the bottle, be equipped with the round platform on the inner wall of extraction bottle bottom, it is in along the overlap joint to separate the selvage on the round platform. The utility model provides an extraction device simple structure has saved the structure of siphon, and cooperation through using solenoid valve and level sensor can realize automatic recovered solvent, has effectively avoided siphon jam problem, has effectively improved the extraction efficiency, and the practicality is strong.
Description
Technical field
This utility model belongs to medical equipment technical field, more particularly to a kind of highly purified monosialyl tetrahexose nerve
The extraction device of section glycosides fat sodium.
Background technology
The preparation method of GM1 is generally divided into extraction and two steps of purification, wherein extracting step
Rapid is usually to smash to pieces fresh Medulla sus domestica, using acetone treatment, is precipitated, and is dried under conditions of temperature is for 70-90 degree Celsius
It is roasting, acetone powder is obtained, then acetone powder is extracted 2-5 time with chloroform methanol mixed solution, that is, extract is obtained, extract is passed through
Crude product dry powder is obtained after fo lch distribution, virus-free and acid hydrolysis inactivation of virus, crude product dry powder is single through being obtained after purification
Sialic acid tetrahexose ganglioside sodium.Extraction equipment for fat is generally used in total fat extraction process is organized, extraction equipment for fat is again
Claim fat extractor, it is a kind of liquid-solid extraction device.
At present, existing extraction equipment for fat is generally apparatus,Soxhlet'ses, and it is to solid in biology, medicine, chemical industry
Material carries out a kind of traditional means of solvent extraction purification.Such as a kind of rope disclosed in existing patent ZL201420688416.2
Family name's extractor, it is made up of solvent bottle, extractor, the part of condenser three, and there are respectively siphon and steam in extractor both sides
Pipe, during extraction, the heating evaporation of solvent is drenched into the material to be extracted of extractor Jing after steam pipe flow to condenser condensation,
Lipid material in extraction sample, device internal solvent liquid level to be extracted reach a certain height, dissolved with the solvent Jing siphons of crude fat
Solvent bottle is flowed into, meanwhile, the solvent in inflow solvent bottle continues to be heated gasification, rises, condenses, and instills in extractor, so
Move in circles, till extracting is completely.Although the device can play the purpose for reclaiming a large amount of solvents, the device passes through
Siphon realizes backflow, and structure is more complicated, using highly inconvenient, especially in high volume production process, and the thing of non-solvent
Material is easy to block siphon, so as to cause solvent to flow in solvent bottle, and then causes material extracting to be forced to terminate, this
Outward, all the time in static state when the material in extractor is extracted, extraction efficiency is relatively low, causes extraction times longer or extracting is not filled
Point, for this purpose, it is a kind of using extraction device that is fairly simple and being automatically obtained solvent recovery to be badly in need of exploitation.
Utility model content
Can not accomplish that recycle heat is utilized to solve extraction device of the prior art, not only heated solvent bottle needs consumption
Take larger heat, and the heat of the outlet in condenser is not reclaimed, additionally, when the material in extractor is extracted
All the time in static state, extraction efficiency is relatively low, and the problems such as causing extraction times longer or extract insufficient, this utility model is provided
A kind of extraction device of highly purified GM1.
This utility model concrete technical scheme is as follows：
This utility model provides a kind of extraction device of highly purified GM1, including
Condenser, extracting bottle and the solvent bottle being sequentially connected, the extracting top of bottle is hinged with closure, and the extracting bottom of bottle portion passes through
Pipeline is connected with the solvent bottle, and the extracting bottle side is provided with steam pipe, described steam pipe one end and solvent bottle top
Side connects, and its other end is connected with extractor top, and the extracting bottle medial wall is provided with liquid level sensor, the pipe
Be provided with check valve in road, the extracting bottle lateral wall is provided with controller, the check valve, the liquid level sensor with it is described
Controller communicates；
The extracting bottle inner bottom part is transversely provided with the filter for placing material to be extracted, in the extracting bottle bottom interior wall
Round platform is provided with, on the round platform, the filter edge is provided with handle to the filter overlapping edges.
Further, the through hole for installing the condenser is provided with the closure, in the through hole first is provided with
Female thread, the condenser bottom is provided with the first external screw thread being adapted to first female thread, and the condenser is by described
First female thread and the first externally threaded cooperation are threadedly coupled with the extracting top of bottle.
Further, solvent bottle top is provided with the second female thread, the duct bottom be provided with described second in spiral shell
Second external screw thread of stricture of vagina adaptation, the extracting bottle is threadedly coupled by the pipeline with the solvent bottle.
Further, the extracting bottle bottom side is provided with discharging tube, and the discharging tube is provided with valve.
Further, agitating device is provided with the extracting bottle, the agitating device includes being fixed on the sealing caping
The rotating shaft of the motor in portion and the motor connection and the mixing component being connected with the rotating shaft, the mixing component stretches to institute
State extracting bottom of bottle portion and be located at filter top.
Preferably, the mixing component includes the swivel base being connected with the rotating shaft bottom and some is arranged on the swivel base side
The stirring paddle of wall, the length of some stirring paddles gradually increases from top to bottom.
Preferably, the steam pipe lateral wall is provided with interlayer, the interlayer and is filled with heat-preservation cotton.
The beneficial effects of the utility model are as follows：The extraction device simple structure provided in the technical program, eliminates rainbow
The structure of suction pipe, by using the cooperation of electromagnetic valve and liquid level sensor, can realize automatic recycling design, effectively prevent rainbow
Suction pipe blockage problem, the suitable extensive material of improvement of the device extracts production, effectively increases extraction efficiency, practical.
Description of the drawings
Fig. 1 is the extraction device of a kind of highly purified GM1 described in embodiment 1
Structural representation；
Fig. 2 is the extraction device of a kind of highly purified GM1 described in embodiment 2
Structural representation；
Fig. 3 is the extraction device of a kind of highly purified GM1 described in embodiment 3
Structural representation.
Wherein：1st, condenser；2nd, bottle is extracted；3rd, solvent bottle；4th, closure；5th, pipeline；6th, steam pipe；7th, sensor；8、
Check valve；9th, controller；10th, filter；11st, round platform；12nd, handle；13rd, through hole；14th, discharging tube；15th, valve；16th, motor；17、
Rotating shaft；18th, swivel base；19th, stirring paddle；20th, interlayer.
Specific embodiment
Below in conjunction with the accompanying drawings this utility model is described in further detail with following examples.
Embodiment 1
As shown in figure 1, this utility model embodiment 1 provides a kind of highly purified Monostalotetrahexosylgangliside
The extraction device of sodium, including the condenser 1, extracting bottle 2 and solvent bottle 3 that are sequentially connected, the top of extracting bottle 2 is hinged with sealing
Lid 4, extracting bottle 2 bottom is connected by pipeline 5 with the solvent bottle 3, and extracting bottle 2 side is provided with steam pipe 6, described
The one end of steam pipe 6 connects with the top side of the solvent bottle 3, and its other end is connected with the top of extracting bottle 2, the extracting bottle
2 medial walls are provided with liquid level sensor 7, the pipeline 5 and are provided with check valve 8, and extracting bottle 2 lateral wall is provided with controller
9, the check valve 8, the liquid level sensor 7 communicate with the controller 9.
Controller 9 can control the unlatching of check valve 8, when the solvent liquid level in extracting bottle 2 reaches the position of liquid level sensor 7
Put, liquid level sensor 7 sends detection signal to controller 9, and the control electromagnetic valve of controller 9 is opened, and is realized in extracting bottle 2
Solvent is flowed in solvent bottle 3, and then circulates extracting, and the structure design is fairly simple.
In order to prevent feed blocking pipeline 5, define in the technical program it is described extracting the inner bottom part of bottle 2 be transversely provided with for
The filter 10 of material to be extracted is placed, the extracting bottom interior wall of bottle 2 is provided with round platform 11, and the overlapping edges of the filter 10 are in institute
State on round platform 11, the edge of the filter 10 is provided with handle 12.Material is placed on filter 10, can be prevented effectively from feed blocking pipe
Road 5, and filter 10 ridden upon on round platform 11, installs firm, handle 12 can conveniently extract filter 10, convenient to place material, real
It is strong with property.
Embodiment 2
As shown in Fig. 2 this utility model embodiment 2 is on the basis of embodiment 1, the closure 4 is further defined
On be provided with through hole 13 for installing the condenser 1, the through hole 13 and be provided with the first female thread, the bottom of the condenser 1
The first external screw thread being adapted to first female thread is provided with, the condenser 1 passes through first female thread and described first
Externally threaded cooperation is connected with the extracting screw top of bottle 2.The through hole 13 at the top of closure 4 is used to install condenser 1, condenses
The bottom of device 1 is threadedly coupled with through hole 13, connects more firm and convenient.
The top of the solvent bottle 3 is provided with the second female thread, and the bottom of the pipeline 5 is provided with what is be adapted to second female thread
Second external screw thread, the extracting bottle 2 is threadedly coupled by the pipeline 5 with the solvent bottle 3.The top of solvent bottle 3 and extracting bottle 2
The pipeline 5 of bottom is threadedly coupled, and facilitates device to install, and connection is more firmly, more safe and reliable in operation.
As shown in Fig. 2 it should be noted that it is described extracting the bottom side of bottle 2 be provided with discharging tube 14, on the discharging tube 14
It is provided with valve 5.Discharging tube 14 is used to discharge the material in extracting bottle 2, convenient cleaning extracting bottle 2.
Embodiment 3
As shown in figure 3, in order to improve extraction efficiency, the extracting bottle 2 that embodiment 3 is limited on the basis of embodiment 1
Agitating device is inside provided with, the agitating device includes that the motor 16 and the motor 16 that are fixed on the top of the closure 4 connect
Rotating shaft 17 and the mixing component that is connected with the rotating shaft 17, the mixing component stretches to the extracting bottom of bottle 2 and is located at
The top of the filter 10.Motor 16 is connected with controller 9, and motor 16 drives rotating shaft 17 to rotate, band of the mixing component in rotating shaft 17
Dynamic lower rotation, realizes stirring, effectively improves extraction efficiency, the total fat in cerebral tissue is substantially dissolved in solvent.
As shown in Figure 3, it is preferred that the mixing component includes the transposase 11 8 being connected with the bottom of the rotating shaft 17 and some sets
The stirring paddle 19 in the side wall of the transposase 11 8 is put, the length of some stirring paddles 19 gradually increases from top to bottom.
As shown in Figure 3, it is preferred that the lateral wall of the steam pipe 6 is provided with interlayer 20, the interlayer 20 filled with insulation
Cotton.When ambient temperature is relatively low, in order to prevent steam condensation in steam pipe 6, define in the technical program in the outside of steam pipe 6
Wall arranges the interlayer 20 filled with heat-preservation cotton, effectively prevents steam condensation in steam pipe 6, prevents solvent refluxing, is effectively ensured
Extraction efficiency.
This utility model is not limited to above-mentioned preferred forms, and anyone can draw under enlightenment of the present utility model
Other various forms of products, however, make any change in its shape or structure, it is every with same as the present application or phase
Approximate technical scheme, all falls within protection domain of the present utility model.
Claims (7)
1. a kind of extraction device of highly purified GM1, including the condenser being sequentially connected
(1), bottle (2) and solvent bottle (3) are extracted, it is characterised in that extracting bottle (2) top is hinged with closure (4), the extracting
Bottle (2) bottom is connected by pipeline (5) with the solvent bottle (3), and extracting bottle (2) side is provided with steam pipe (6), the steaming
Steam pipe (6) one end connects with the solvent bottle (3) top side, and its other end is connected with extracting bottle (2) top, described to take out
Carry bottle (2) medial wall and be provided with liquid level sensor (7), the pipeline (5) is interior to be provided with check valve (8), extracting bottle (2) outside
Wall is provided with controller (9), and the check valve (8), the liquid level sensor (7) communicate with the controller (9)；
Extracting bottle (2) inner bottom part is transversely provided with the filter (10) for placing material to be extracted, extracting bottle (2) bottom
Inwall is provided with round platform (11), and on the round platform (11), filter (10) edge is provided with filter (10) overlapping edges
Handle (12).
2. the extraction device of highly purified GM1 as claimed in claim 1, its feature exists
In, the through hole (13) for installing the condenser (1) is provided with the closure (4), the through hole (13) is interior to be provided with first
Female thread, condenser (1) bottom is provided with the first external screw thread being adapted to first female thread, and the condenser (1) is led to
Cross first female thread and the first externally threaded cooperation is connected with extracting bottle (2) screw top.
3. the extraction device of highly purified GM1 as claimed in claim 1, its feature exists
In solvent bottle (3) top is provided with the second female thread, and pipeline (5) bottom is provided with what is be adapted to second female thread
Second external screw thread, the extracting bottle (2) is threadedly coupled by the pipeline (5) with the solvent bottle (3).
4. the extraction device of highly purified GM1 as claimed in claim 1, its feature exists
In extracting bottle (2) bottom side is provided with discharging tube (14), and the discharging tube (14) is provided with valve (15).
5. the extraction device of highly purified GM1 as claimed in claim 1, its feature exists
In, agitating device is provided with extracting bottle (2), the agitating device includes being fixed on the motor at the top of the closure (4)
(16) and the motor (16) connection rotating shaft (17) and the mixing component that is connected with the rotating shaft (17), the mixing component
Stretch to extracting bottle (2) bottom and be located at the filter (10) top.
6. the extraction device of highly purified GM1 as claimed in claim 5, its feature exists
Include the swivel base (18) being connected with the rotating shaft (17) bottom in, the mixing component and some be arranged on the swivel base (18) side
The stirring paddle (19) of wall, the length of some stirring paddles (19) gradually increases from top to bottom.
7. the extraction device of highly purified GM1 as claimed in claim 1, its feature exists
In steam pipe (6) lateral wall is provided with interlayer (20), the interlayer (20) and is filled with heat-preservation cotton.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621103533.3U CN206127177U (en) | 2016-09-30 | 2016-09-30 | Extraction device of tetrahexose monosialogandlioside sodium of high -purity |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621103533.3U CN206127177U (en) | 2016-09-30 | 2016-09-30 | Extraction device of tetrahexose monosialogandlioside sodium of high -purity |
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| Publication Number | Publication Date |
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| CN206127177U true CN206127177U (en) | 2017-04-26 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201621103533.3U Active CN206127177U (en) | 2016-09-30 | 2016-09-30 | Extraction device of tetrahexose monosialogandlioside sodium of high -purity |
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| CN (1) | CN206127177U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115487536A (en) * | 2022-10-25 | 2022-12-20 | 湖南农业大学 | Large Soxhlet extraction equipment and method for extracting materials |
-
2016
- 2016-09-30 CN CN201621103533.3U patent/CN206127177U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115487536A (en) * | 2022-10-25 | 2022-12-20 | 湖南农业大学 | Large Soxhlet extraction equipment and method for extracting materials |
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Address after: 519015 west side of the second floor of Everbright International Trade Center, 47 Haibin South Road, Jida, Zhuhai City, Guangdong Province Patentee after: Sailong Pharmaceutical Group Co.,Ltd. Address before: 519015 west side of 2nd floor, Everbright International Trade Center, No. 47, Jida Haibin South Road, Xiangzhou District, Zhuhai City, Guangdong Province Patentee before: ZHUHAI SAILONG PHARMACEUTICAL Co.,Ltd. |
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