CN206103371U - Spherical concentrator in vacuum - Google Patents
Spherical concentrator in vacuum Download PDFInfo
- Publication number
- CN206103371U CN206103371U CN201621075972.8U CN201621075972U CN206103371U CN 206103371 U CN206103371 U CN 206103371U CN 201621075972 U CN201621075972 U CN 201621075972U CN 206103371 U CN206103371 U CN 206103371U
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- spherical
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- condenser
- liquid
- collecting tank
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Abstract
The utility model discloses a spherical concentrator in vacuum, including spherical concentrated jar, vapour and liquid separator, condenser and collector tube, spherical concentrated jar, vapour and liquid separator, condenser and liquid -collecting tank connect gradually, spherical concentrated tank bottoms portion is equipped with heating jacket and discharge gate, and heating jacket even has the steam pipe, is equipped with the valve on the steam pipe, and spherical concentrated jar of side is equipped with feed inlet and observation window, and even there is the vacuum pump at the liquid -collecting tank top, and liquid -collecting tank and condenser pass through the third pipe connection, are equipped with velocity of flow sensor on the third pipeline, and velocity of flow sensor and valve are connected with the controller respectively. Adopt the utility model discloses a spherical concentrator in vacuum need not the agitator, natural crystallization, and it is concentrated to be particularly useful for a small amount of material, still be equipped with sensing control device, can guarantee that the solvent at the uniform velocity evaporates, it is safe high -efficient.
Description
Technical field
This utility model is related to technical field of biological extraction, more particularly to a kind of vacuum spherical concentrator.
Background technology
At present vacuum-concentrcted device is mainly used in the concentration of the field such as pharmacy, food, chemical industry material, and known normal pressure is dense
Contracting equipment is heated at ambient pressure with steam, and material solution reaches and seethed with excitement after boiling point in concentration kettle, the solvent vapo(u)r Jing pipelines of generation
Import in condenser and proceeded in solvent recovery tank after condensation.The solvent of material solution not engler distillation, enables material solution in tank
Constantly concentration., due to adopting air-distillation, evaporating temperature is high, is not particularly well suited for the concentration of heat-sensitive substance for this kind equipment.Separately
Outward, also there is not solvent boil-up rate sensing and controlling device.
Utility model content
In view of this, this utility model provides a kind of vacuum spherical concentrator, solves of the prior art spherical dense
Solvent flow rate sensing and controlling device is not provided with contracting device.
The technological means that this utility model is adopted are as follows：A kind of vacuum spherical concentrator, including spherical concentration tank, gas-liquid point
From device, condenser and collector tube, spherical concentration tank, gas-liquid separator, condenser and liquid collecting tank are sequentially connected, it is characterised in that：
The spherical concentration pot bottom is provided with heating jacket and discharging opening, and heating jacket is connected with steam pipe, and steam pipe is provided with valve, ball
Shape concentration tank side is provided with charging aperture and observation window, and liquid collecting tank top is connected with vacuum pump, and liquid collecting tank and condenser are by the 3rd pipe
Road connects, and the 3rd pipeline is provided with flow sensor, and flow sensor is connected respectively with valve with controller.
Preferably, gas-liquid separator sidepiece is connected by the first pipeline and spherical concentration tank, and gas-liquid separator bottom passes through
Second pipe and spherical concentration tank connect.
Preferably, condenser is multiple-effect condensing tube.
Preferably, liquid collecting tank is provided with effusion meter.
Using a kind of vacuum spherical concentrator provided by the utility model, without the need for agitator, spontaneous nucleation is especially suitable
In the concentration of a small amount of material；And sensing and controlling device is additionally provided with, and can guarantee that solvent is at the uniform velocity steamed, it is safe and efficient.
Description of the drawings
Fig. 1 is a kind of structural representation of vacuum spherical concentrator of the present utility model.
Specific embodiment
Principle of the present utility model and feature are described below in conjunction with accompanying drawing, example is served only for explaining this practicality
It is new, it is not intended to limit scope of the present utility model.
Such as Fig. 1, a kind of vacuum spherical concentrator, including spherical concentration tank 1, gas-liquid separator 2, condenser 3 and collector tube
4, spherical concentration tank 1, gas-liquid separator 2, condenser 3 and liquid collecting tank 4 are sequentially connected, and the bottom of spherical concentration tank 1 is provided with heating folder
Set 12 and discharging opening 13, the upper left corner of spherical concentration tank 1 is provided with charging aperture 11 and observation window 15, and spherical concentration tank 1 is fixed on support
On 14, the adjustable-height of support 14, the sidepiece of gas-liquid separator 2 is connected by the first pipeline 21 and spherical concentration tank 1, gas-liquid separation
The bottom of device 2 is connected by second pipe 22 and spherical concentration tank 1, and gas-liquid separator 2 can play froth breaking work by the material that flows back
With；Condenser 3 is multiple-effect condensing tube, and condensation efficiency is high.Liquid collecting tank 4 is provided with effusion meter 41, can the intuitive judgment institute steaming liquid scale of construction；Collection
The top of flow container 4 is connected with vacuum pump 5, it is ensured that system is low-pressure state.Heating jacket 12 is connected with steam pipe, and steam pipe is provided with valve
62, condenser 3 and liquid collecting tank 4 are connected by the 3rd pipeline, and the 3rd pipeline is provided with flow sensor 61, flow sensor 61,
Valve 62 is connected respectively with controller 6, when sensor 61 detects the flow velocity of solvent not in threshold range, can send prompting letter
Number, controller 6 receives signal and controls to adjust the size of the valve 62 on steam pipe, so as to control firing rate.
Operation principle：First by concentration tank evacuation, the material solution for intending concentration is poured in concentration tank, open steam, from
Steam inlet enters heating interlayer, and heating concentration is carried out to concentration tank, and residual steam is discharged from steam (vapor) outlet, can in concentration process
The concentration situation observed in tank by observation window, concentration is finished, release, and the material after concentration is released from discharging opening, in concentration tank
The solvent that solution evaporation goes out enters gas-liquid separator, and gas is directly entered condenser, collects liquid collecting tank, and feed liquid is recovered to
Concentration tank.
A kind of new vacuum spherical concentrator is used using this, without the need for agitator, spontaneous nucleation, is particularly suited for a small amount of
Material is concentrated；Sensing and controlling device is additionally provided with, can guarantee that solvent is at the uniform velocity steamed, it is safe and efficient.
Preferred embodiment of the present utility model is the foregoing is only, it is all at this not to limit this utility model
Within the spirit and principle of utility model, any modification, equivalent substitution and improvements done etc. should be included in this utility model
Within the scope of protection.
Claims (4)
1. a kind of vacuum spherical concentrator, including spherical concentration tank, gas-liquid separator, condenser and collector tube, spherical concentration tank,
Gas-liquid separator, condenser and liquid collecting tank are sequentially connected, it is characterised in that：It is described it is spherical concentration pot bottom be provided with heating jacket and
Discharging opening, heating jacket is connected with steam pipe, and steam pipe is provided with valve, and spherical concentration tank side is provided with charging aperture and observation window,
Liquid collecting tank top is connected with vacuum pump, and liquid collecting tank and condenser are connected by the 3rd pipeline, and the 3rd pipeline is provided with flow sensor,
Flow sensor and valve are connected respectively with controller.
2. a kind of vacuum spherical concentrator according to claim 1, it is characterised in that：The gas-liquid separator sidepiece passes through
First pipeline and spherical concentration tank connect, and gas-liquid separator bottom is connected by second pipe and spherical concentration tank.
3. a kind of vacuum spherical concentrator according to claim 1, it is characterised in that：The condenser is multiple-effect condensation
Pipe.
4. a kind of vacuum spherical concentrator according to claim 1, it is characterised in that：The liquid collecting tank is provided with flow
Meter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621075972.8U CN206103371U (en) | 2016-09-23 | 2016-09-23 | Spherical concentrator in vacuum |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621075972.8U CN206103371U (en) | 2016-09-23 | 2016-09-23 | Spherical concentrator in vacuum |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206103371U true CN206103371U (en) | 2017-04-19 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621075972.8U Active CN206103371U (en) | 2016-09-23 | 2016-09-23 | Spherical concentrator in vacuum |
Country Status (1)
| Country | Link |
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| CN (1) | CN206103371U (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107376397A (en) * | 2017-06-19 | 2017-11-24 | 南京紫晶藤节能科技有限公司 | The cold and hot linkage low-temperature evaporation condensing crystallizing system and method for low boiling solution |
| CN107398088A (en) * | 2017-09-18 | 2017-11-28 | 盐城方正医药科技有限公司 | A kind of Simvastatin production enrichment facility |
| CN107569863A (en) * | 2017-08-19 | 2018-01-12 | 安徽泛亚环保科技有限公司 | A kind of tower that is concentrated under reduced pressure for DMF recovery systems |
| CN111003866A (en) * | 2019-12-06 | 2020-04-14 | 安徽晨晰洁净科技有限公司 | Waste salt concentration treatment device |
| CN114832405A (en) * | 2021-02-01 | 2022-08-02 | 朴然熙 | Electric concentration extraction device capable of quickly extracting and concentrating |
-
2016
- 2016-09-23 CN CN201621075972.8U patent/CN206103371U/en active Active
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107376397A (en) * | 2017-06-19 | 2017-11-24 | 南京紫晶藤节能科技有限公司 | The cold and hot linkage low-temperature evaporation condensing crystallizing system and method for low boiling solution |
| CN107569863A (en) * | 2017-08-19 | 2018-01-12 | 安徽泛亚环保科技有限公司 | A kind of tower that is concentrated under reduced pressure for DMF recovery systems |
| CN107398088A (en) * | 2017-09-18 | 2017-11-28 | 盐城方正医药科技有限公司 | A kind of Simvastatin production enrichment facility |
| CN111003866A (en) * | 2019-12-06 | 2020-04-14 | 安徽晨晰洁净科技有限公司 | Waste salt concentration treatment device |
| CN111003866B (en) * | 2019-12-06 | 2024-05-17 | 安徽晨晰洁净科技有限公司 | Waste salt concentration treatment device |
| CN114832405A (en) * | 2021-02-01 | 2022-08-02 | 朴然熙 | Electric concentration extraction device capable of quickly extracting and concentrating |
| CN114832405B (en) * | 2021-02-01 | 2024-01-05 | 朴然熙 | Electric concentrating and extracting device capable of fast extracting and concentrating |
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