CN205965058U - Purification of high boiling point chemical reagent , filling integral type equipment - Google Patents
Purification of high boiling point chemical reagent , filling integral type equipment Download PDFInfo
- Publication number
- CN205965058U CN205965058U CN201620987087.0U CN201620987087U CN205965058U CN 205965058 U CN205965058 U CN 205965058U CN 201620987087 U CN201620987087 U CN 201620987087U CN 205965058 U CN205965058 U CN 205965058U
- Authority
- CN
- China
- Prior art keywords
- chemical reagent
- boiling point
- high boiling
- evaporator
- lid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a purification of high boiling point chemical reagent, filling integral type equipment, comprising a base plate, the upper surface of bottom plate is equipped with the evaporating pot, and the bottom of evaporating pot is equipped with the heater strip, and the top of heater strip is equipped with the hot plate, the upper end of evaporating pot is equipped with the evaporation lid, and the lower extreme of evaporation lid is equipped with temperature sensor, the by heating silk heats for chemical reagent, it is more even when the by heating board makes heating chemical reagent, temperature sensor and humidity transducer have been set up at the evaporation lid, temperature when evaporating through temperature sensor determine, go out the pressure release in the evaporating pot through the pressure release pipe, prevent the explosion, the by freezing pipe turns into liquid to the gaseous chemical reagent who evaporates, feasible cooling is more convenient, the purification of this high boiling point chemical reagent, equipment structure is simple for the filling integral type, easy for cleaning, purification and the filling efficiency that improves work as an organic whole, lots of energy sources are saved.
Description
Technical field
This utility model is related to chemical reagent technical field, specially a kind of high boiling point chemical reagent purification, fill one
Formula equipment.
Background technology
The chemical reagent of domestic liquid type mainly based on subpackage, due to the strict demand to product index for the chemical reagent,
Many raw materials do not reach the standard of subpackage it is necessary to be purified.The chemical reagent of common liq class can be by way of distillation
To purify, but can run into problems to the purification of high boiling liquid, such as existing mode of heating heats for steam, vapor (steam) temperature
In the evaporating temperature of 120-150 DEG C of difficult to reach material, purchase equipment, and the chemical reagent of liquid type need to be led using electrical heating
It mostly is flammable liquid, equipment safety grade need to be greatly improved；Production lot is little, so laboratory preparation can only be adopted, but experiment
Room preparation method yield is too low and needs that do not catch up with market, chemical reagent wide in variety it is impossible to accomplish that a set of equipment only produces one
Kind, needs one-object-many-purposes, a thing multipotency, and on market, the equipment junction of buying is and is fixedly connected, dismounting inconvenience, is difficult clear
Wash, existing production model is that workshop loads big packaging by after the purification of high boiling liquid chemical reagent, then delivers to packaging car
Between carry out fill, because high boiling liquid chemical reagent freezing point is also high, often just solidified when delivering to packing shop or become
Sticky, can only again be heated to that uniform temperature makes it melt or viscosity reduces and carries out fill again, reduce efficiency, increased energy
Consumption.
Utility model content
The technical problems to be solved in the utility model is to overcome existing defect, provides a kind of high boiling point chemical reagent to carry
Pure, fill integrated equipment, structure is simple, easy and simple to handle, and easy accessibility, easily clean, purification and fill are integrated and carry
The high efficiency of work, saves the substantial amounts of energy, can be with the problem in effectively solving background technology.
For achieving the above object, this utility model provides following technical scheme：A kind of high boiling point chemical reagent purification, fill
Integrated equipment, including base plate, the upper surface of described base plate is provided with evaporator, and the bottom of evaporator is provided with heater strip, heater strip
Top be provided with heating plate, the upper end of described evaporator is provided with evaporation lid, and evaporates the lower end of lid and be provided with temperature sensor, temperature
The side of sensor is provided with humidity sensor, and the upper end of described evaporation lid is provided with relief tube, and relief tube is provided with the first valve, institute
The side stating relief tube is provided with U-shaped conduit, and the upper end of U-shaped conduit and the upper surface of base plate have certain gradient, and on U-shaped conduit
It is provided with cooling tube, the side of described evaporator is provided with water pump, and the outlet of water pump passes through conduit with cooling tube lower end even outside end
Connect, the side of described water pump is provided with water tank, and the lower end of water tank side is connected with water pump by conduit, and the side of water tank upper surface
It is connected with the upper end of cooling tube by conduit, one end of described U-shaped conduit is connected with union joint, and the lower end of union joint is provided with Sheng liquid
Tank, the side of described water tank is provided with controller, and controller electrical connection external power source, and controller electrical connection heater strip, temperature
Degree sensor, humidity sensor and water pump.
As a kind of optimal technical scheme of the present utility model, described evaporation lid is provided with leakproof skin with the junction of evaporator
Pad, and evaporate lid and be connected by junction button with the both sides of evaporator.
As a kind of optimal technical scheme of the present utility model, one end that described U-shaped conduit is connected with evaporation lid is provided with the
Two valves, and the second valve pass through bolt with evaporation cover be connected.
As a kind of optimal technical scheme of the present utility model, described controller arranges display, the lower section of display
It is provided with control button, control button and display electrical connection controller.
As a kind of optimal technical scheme of the present utility model, described union joint is provided with escape pipe, and escape pipe runs through even
The upper and lower side of joint.
Compared with prior art, the beneficial effects of the utility model are：The purification of this high boiling point chemical reagent, fill integral type
Evaporator is provided with equipment, liquid to be evaporated is held by evaporator, be provided with heating plate and heating in evaporator
Silk, is heated to chemical reagent by heater strip, is made by heating plate more uniform during heating chemical reagents, under evaporation lid
End is provided with temperature sensor and humidity sensor, by temperature during temperature sensor detection evaporation, by humidity sensor
Moisture in detection evaporator, is covered in evaporation and is provided with relief tube, discharged the pressure in evaporator by relief tube,
Prevent to explode, water pump is arranged on base plate, will be to be drawn in cooling tube in water tank by water pump, by cooling tube pair
The Gas chemistries flashing to are converted into liquid so that cooling is convenient, the purification of this high boiling point chemical reagent, fill one
Formula device structure is simple, easy and simple to handle, and easy accessibility, easily clean, purification and fill are integrated the effect that improve work
Rate, saves the substantial amounts of energy.
Brief description
Fig. 1 is this utility model structural representation；
Fig. 2 is this utility model cross-sectional view.
In figure：1 escape pipe, 2 U-shaped conduits, 3 cooling tubes, 4 second valves, 5 relief tubes, 6 first valves, 7 evaporation lid, 8
Junction button, 9 evaporators, 10 water tanks, 11 controllers, 12 water pumps, 13 base plates, 14 fluid-containing pots, 15 union joints, 16 temperature sensors,
17 humidity sensors, 18 heating plates, 19 heater strips.
Specific embodiment
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is carried out
Clearly and completely description is it is clear that described embodiment is only a part of embodiment of this utility model rather than whole
Embodiment.Based on the embodiment in this utility model, those of ordinary skill in the art are not under the premise of making creative work
The every other embodiment being obtained, broadly falls into the scope of this utility model protection.
Refer to Fig. 1-2, this utility model provides a kind of technical scheme：A kind of high boiling point chemical reagent purification, fill one
Body formula equipment, including base plate 13, the upper surface of base plate 13 is provided with evaporator 9, holds liquid to be evaporated by evaporator 9,
The bottom of evaporator 9 is provided with heater strip 19, and the top of heater strip 19 is provided with heating plate 18, by heater strip 19 to chemical reagent plus
Heat, is made more uniform during heating chemical reagents by heating plate 18, and the upper end of evaporator 9 is provided with evaporation lid 7, evaporation lid 7 with
The junction of evaporator 9 is provided with leakproof leather packing, and evaporation lid 7 is connected by junction button 8 with the both sides of evaporator 9, by leakproof
Leather packing make evaporation lid 7 and evaporator 9 between be connected even closer, and evaporate lid 7 lower end be provided with temperature sensor 16, temperature
The side of sensor 16 is provided with humidity sensor 17, by temperature during temperature sensor 16 detection evaporation, by humidity sensor
Device 17 detects the moisture in evaporator, and the upper end of evaporation lid 7 is provided with relief tube 5, by relief tube 5 by the pressure in evaporator 9
Discharge, prevent to explode, relief tube 5 is provided with the first valve 6, the side of relief tube 5 is provided with U-shaped conduit 2, U-shaped lead
One end that pipe 2 is connected with evaporation lid 7 is provided with the second valve 4, and the second valve 4 is passed through bolt and is connected with evaporation lid 7, by second
Valve 4 can control debris to enter, and the upper end of U-shaped conduit 2 and the upper surface of base plate 13 have certain gradient, and on U-shaped conduit 2
It is provided with cooling tube 3, the side of evaporator 9 is provided with water pump 12, and the outlet of water pump 12 passes through conduit and cooling tube 3 lower end outside end
Connect, the side of water pump 12 is provided with water tank 10, and the lower end of water tank 10 side is connected with water pump 12 by conduit, and water tank 10 upper table
The side in face is connected with the upper end of cooling tube 3 by conduit, will in water tank 10 be to be drawn in cooling tube 3 by water pump 12,
Liquid is converted into the Gas chemistries flashing to by cooling tube 3 so that cooling is convenient, one end of U-shaped conduit 2 is even
It is connected to union joint 15, union joint 15 is provided with escape pipe 1, escape pipe 1 runs through the upper and lower side of union joint 15, subtracts by escape pipe 1
Pressure in little fluid-containing pot 14, the lower end of union joint 15 is provided with fluid-containing pot 14, holds, by fluid-containing pot 14, the chemical reagent having filtered,
The side of water tank 10 is provided with controller 11, and controller 11 electrical connection external power source, and controller 11 electrical connection heater strip 19,
Temperature sensor 16, humidity sensor 17 and water pump 12, controller 11 arranges display, the lower section of display be provided with control by
Key, control button and display electrical connection controller 11, can more clearly be observed by display, this high boiling point chemistry examination
Agent purification, fill integrated equipment structure are simple, easy and simple to handle, and easy accessibility, easily clean, purification and fill are integrated
Improve the efficiency of work, save the substantial amounts of energy.
When using：First chemical reagent is put in evaporator 9, then by heater strip 19 plate, chemical reagent is heated,
During heating, by temperature during temperature sensor 16 detection evaporation, the moisture in evaporator 9 is detected by humidity sensor 17,
When temperature does not reach the boiling point of chemical reagent, by opening the first valve 6, the pressure in evaporator 9 is shed, when temperature reaches
The boiling point of chemical reagent and when air humidity is big, closes the first valve 6 by opening the second valve 4, allows gas flow into U-shaped conduit
2, then will be to be drawn in cooling tube 3 in water tank 10 by water pump 12, by cooling tube 3, aerochemistry in U-shaped conduit 2 is tried
Agent is converted into liquid, then is flowed in fluid-containing pot 14.
This utility model is provided with heating plate 18 and heater strip 19 in evaporator, by heater strip 19 to chemical reagent plus
Heat, is made more uniform during heating chemical reagents by heating plate 18, is provided with temperature sensor 16 He in the lower end of evaporation lid 7
Humidity sensor 17, by temperature during temperature sensor 16 detection evaporation, is detected in evaporator 9 by humidity sensor 17
Moisture, arranges water pump 12 on base 13, will in water tank 10 be to be drawn in cooling tube 3 by water pump 12, by cooling tube 3
Liquid is converted into the Gas chemistries flashing to so that cooling is convenient, the purification of this high boiling point chemical reagent, fill one
Body formula device structure is simple, easy and simple to handle, and easy accessibility, easily clean, purification and fill are integrated and improve work
Efficiency, saves the substantial amounts of energy.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art,
It is appreciated that these embodiments can be carried out with multiple changes in the case of without departing from principle of the present utility model and spirit, repair
Change, replace and modification, scope of the present utility model is defined by the appended claims and the equivalents thereof.
Claims (5)
1. a kind of high boiling point chemical reagent purification, fill integrated equipment, including base plate（13）It is characterised in that：Described base plate
（13）Upper surface be provided with evaporator（9）, evaporator（9）Bottom be provided with heater strip（19）, heater strip（19）Top be provided with
Heating plate（18）, described evaporator（9）Upper end be provided with evaporation lid（7）, and evaporate lid（7）Lower end be provided with temperature sensor
（16）, temperature sensor（16）Side be provided with humidity sensor（17）, described evaporation lid（7）Upper end be provided with relief tube（5）,
Relief tube（5）It is provided with the first valve（6）, described relief tube（5）Side be provided with U-shaped conduit（2）, U-shaped conduit（2）Upper end
With base plate（13）Upper surface have certain gradient, and U-shaped conduit（2）It is provided with cooling tube outside upper end（3）, described evaporator
（9）Side be provided with water pump（12）, water pump（12）Outlet pass through conduit and cooling tube（3）Lower end connects, described water pump
（12）Side be provided with water tank（10）, water tank（10）Conduit and water pump are passed through in the lower end of side（12）Connect, and water tank（10）On
Conduit and cooling tube are passed through in the side on surface（3）Upper end connect, described U-shaped conduit（2）One end be connected with union joint（15）,
Union joint（15）Lower end be provided with fluid-containing pot（14）, described water tank（10）Side be provided with controller（11）, and controller（11）
Electrical connection external power source, and controller（11）Electrical connection heater strip（19）, temperature sensor（16）, humidity sensor（17）With
Water pump（12）.
2. a kind of high boiling point chemical reagent purification according to claim 1, fill integrated equipment it is characterised in that：Institute
State evaporation lid（7）With evaporator（9）Junction be provided with leakproof leather packing, and evaporate lid（7）With evaporator（9）Both sides pass through even
Connect button（8）Connect.
3. a kind of high boiling point chemical reagent purification according to claim 1, fill integrated equipment it is characterised in that：Institute
State U-shaped conduit（2）With evaporation lid（7）The one end connecting is provided with the second valve（4）, and the second valve（4）By bolt and evaporation
Lid（7）Connect.
4. a kind of high boiling point chemical reagent purification according to claim 1, fill integrated equipment it is characterised in that：Institute
State controller（11）Upper setting display, the lower section of display is provided with control button, and control button and display electrical connection control
Device（11）.
5. a kind of high boiling point chemical reagent purification according to claim 1, fill integrated equipment it is characterised in that：Institute
State union joint（15）It is provided with escape pipe（1）, escape pipe（1）Run through union joint（15）Upper and lower side.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620987087.0U CN205965058U (en) | 2016-08-30 | 2016-08-30 | Purification of high boiling point chemical reagent , filling integral type equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620987087.0U CN205965058U (en) | 2016-08-30 | 2016-08-30 | Purification of high boiling point chemical reagent , filling integral type equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205965058U true CN205965058U (en) | 2017-02-22 |
Family
ID=58040980
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620987087.0U Expired - Fee Related CN205965058U (en) | 2016-08-30 | 2016-08-30 | Purification of high boiling point chemical reagent , filling integral type equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205965058U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117504332A (en) * | 2024-01-04 | 2024-02-06 | 成都金山化学试剂有限公司 | Ultrapure electronic grade chemical reagent purifying device for semiconductor |
-
2016
- 2016-08-30 CN CN201620987087.0U patent/CN205965058U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117504332A (en) * | 2024-01-04 | 2024-02-06 | 成都金山化学试剂有限公司 | Ultrapure electronic grade chemical reagent purifying device for semiconductor |
| CN117504332B (en) * | 2024-01-04 | 2024-03-22 | 成都金山化学试剂有限公司 | Ultrapure electronic grade chemical reagent purifying device for semiconductor |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105327518A (en) | Pentanediamine concentration system and method thereof | |
| CN204943429U (en) | A kind of pure steam generator | |
| CN205965058U (en) | Purification of high boiling point chemical reagent , filling integral type equipment | |
| CN206113444U (en) | Heat pump divides fluidization frost system | |
| CN207532811U (en) | A kind of liquid heating evaporation enrichment facility | |
| CN204746079U (en) | Quick cooling and alkali lye spray purifier | |
| CN204364915U (en) | Thin-film distillation still | |
| CN205627145U (en) | Novel reaction rectifying column | |
| CN205627127U (en) | MVR triple -effect evaporator | |
| CN205973864U (en) | Distilled water machine | |
| CN210787309U (en) | Condensing system | |
| CN208626652U (en) | A kind of alcohol distillation tower | |
| CN204159044U (en) | The cold tank of a kind of sudden strain of a muscle with vapor-recovery system | |
| CN209108628U (en) | A kind of recyclable device applied to nitrating wasting acid | |
| CN209098229U (en) | Dyeing and printing sewage processing equipment | |
| CN205718533U (en) | A kind of steam recycling device | |
| CN207769768U (en) | A kind of naphthalene water reducer condensation reaction equipment | |
| CN206469496U (en) | Sour cycle battery is internalized into system electric heater unit | |
| CN203464774U (en) | Condenser used for producing meropenem branched chains | |
| CN204193534U (en) | A kind of concentration systems of pentanediamine | |
| CN212417026U (en) | Whole skid-mounted equipment of spherical concentrator | |
| CN203944148U (en) | A kind of distillation system | |
| CN207838356U (en) | A kind of paracide production condensing unit | |
| CN202717803U (en) | Isoenthalpy type protection gas humidification device of annealing furnace | |
| CN203190852U (en) | Material condensing device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170222 Termination date: 20170830 |