CN205907046U - Apparatus for preparing silicon oxygen compound's manufacturing - Google Patents
Apparatus for preparing silicon oxygen compound's manufacturing Download PDFInfo
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- CN205907046U CN205907046U CN201620290949.4U CN201620290949U CN205907046U CN 205907046 U CN205907046 U CN 205907046U CN 201620290949 U CN201620290949 U CN 201620290949U CN 205907046 U CN205907046 U CN 205907046U
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- tank body
- opening
- heating furnace
- collector
- manufacturing equipment
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Abstract
The utility model discloses an apparatus for preparing silicon oxygen compound's manufacturing. The manufacture equipment includes the heating furnace and the vertical jar body of placing, and a jar body top is equipped with the opening, and the bottom of jar body is equipped with originally and is set up in adding the stove, is equipped with collector and connection for vacuum pump on the jar body between heating furnace and opening. Through the utility model discloses a manufacture equipment, the industrialization preparation that can mechanize, automatic realizes silicon oxygen compound.
Description
Technical field
The utility model is related to chemical field and in particular to a kind of manufacturing equipment preparing silicon oxide compound.
Background technology
Sio is used as preparing the important source material of optical glass, semi-conducting material and lithium ion battery negative material.
Because the working condition of sio is harsh, its yield can not meet the market demand.The presently disclosed mode of production is usually
Make si and sio2 reaction produce sio gas under vacuum and hot conditions, and make sio cryogenic temperature condensation.
The production equipment of industrial sio is by reative cell and collecting chamber all in vacuum cylinder at present, in reative cell and very
Heating wire is placed, this equipment can not be effectively increased reaction chamber size, lead to product yield relatively low, also in cavity between empty cylinder
The material Homogenizing of composition also resulting in product all directions is poor.Because heater members are in vacuum cylinder it is impossible to adopt combustion
Burn heating, thus energy resource consumption is larger；Because reative cell and collecting chamber are all in vacuum cylinder, the sio taking out in collecting chamber needs
Cooling whole equipment, it is impossible to realize continuous production, greatly causes the waste of the energy.
Therefore, the production equipment of existing industrial production sio cannot carry out industrialized production sio well.
Content of the invention
The utility model is mainly solving the technical problems that provide a kind of manufacturing equipment preparing silicon oxide compound, Neng Gouji
Tool, the preparation of industrialization realizing silicon oxide compound of automation.
In a first aspect, the embodiment of the present invention provides a kind of manufacturing equipment of silicon oxide compound, described manufacturing equipment includes adding
Hot stove and vertical at least one tank body placed, described tank body top is provided with opening, and described tank body built with raw material and is arranged at
In heating furnace, the tank body between described heating furnace and described opening is provided with collector and vacuumizes interface.
Wherein, the tank body between described heating furnace and described opening is additionally provided with cooling device.
Wherein, described cooling device is coolant jacket, and described coolant jacket is set on described tank body, is circulated by cooling medium
Cooling.
Wherein, described tank body bottom is at least partially disposed at outside described heating furnace, and described tank body bottom is provided with deslagging
Mouthful.
Wherein, described heating furnace is electric furnace or combustion heating furnace.
Wherein, described collector is the tubular structure of at least one end open.
Wherein, described collector is the different tubular structure of two ends size, and wherein, described collector is towards the one of opening
End is smaller in size than the other end.
Wherein, described tank body is additionally provided with the cover for opening or closing described opening.
The beneficial effects of the utility model are: be different from the situation of prior art, the system of the utility model silicon oxide compound
Manufacturing apparatus include heating furnace and the vertical tank body placed, and tank body top is provided with opening, and the bottom of tank body equipped with raw material and is arranged at
Add in stove, the tank body between heating furnace and opening is provided with collector and vacuumizes interface.By system of the present utility model
Manufacturing apparatus, can load problem by effectively solving raw material, increase charge and increase heat utilization rate.And adopted based on manufacturing equipment
The design of perpendicular tank, the equipment of being more beneficial for realizes mechanization, automation, thus better meet silicon oxide compound industrialized production and
Ensure product quality.
Brief description
Fig. 1 is a kind of manufacturing equipment structural representation of silicon oxide compound that the utility model first embodiment provides；
Fig. 2 is a kind of manufacturing equipment structural representation of silicon oxide compound that the utility model second embodiment provides；
Fig. 3 is a kind of manufacturing equipment structural representation of silicon oxide compound that the utility model 3rd embodiment provides；
Fig. 4 is a kind of method indicative flowchart preparing silicon oxide compound.
Specific embodiment
Refer to Fig. 1-Fig. 3, Fig. 1-Fig. 3 is the manufacturing equipment structure of the silicon oxide compound that the utility model embodiment provides
Schematic diagram, as illustrated, the manufacturing equipment in the present embodiment includes heating furnace 1 and vertical at least one tank body 2 (its placed
In, Fig. 1 show 1 tank body, and Fig. 3 show 3 tank bodies, and certainly, the number of tank body is not limited with illustrating, can be according to need
Increased and decreased), tank body 2 top is provided with opening 3, and tank body 2 built with raw material and is arranged in heating furnace 1, in heating furnace 1 with open
Tank body between mouth 3 is provided with collector 4 and vacuumizes interface 5.
When raw material in tank body is reacted, need tank body 2 is sealed, then by vacuumizing interface 5 to tank
Body is vacuumized so that being in vacuum state in tank body.Wherein it is possible to by sealing device, sealing dress are arranged on tank body
Put for opening or closing opening 3, wherein, the sealing device in the embodiment of the present invention can be heat-resisting piston, by heat-resisting work
Extracting or filling in realization of plug opens or closes opening 3, and sealing device can also be the hard plate of other heat-resisting airtight materials
Material, can with opening 3 realize fit tightly, by person's opening 3 place hard plate material or take off sheet material realize close to tank body 2
Seal or open.
Wherein, in the embodiment of the present invention, put into raw material for convenience and take out final product, by also setting on tank body 2
It is equipped with the cover 7 for opening or closing opening 3.Wherein, cover 7 can be connected by any of which with tank body 2, such as
Revolving type connects, and buckle-type connects, hinged, threaded etc..
Wherein, collector 4 is the tubular structure of at least one end open.Wherein, one end of collector 4 opening is towards tank body 2
Bottom.Thus convenient collect product and taking and placing collector 4.The such as cylindrical structural of one or both ends opening or one end
Or the taper of both ends open etc..
Wherein in a kind of implementation, collector 4 is the different tubular structure of two ends size, wherein, collector 4 court
One end to opening 3 is smaller in size than the other end.I.e. collector 4 is the tubular structure with certain taper, the little one end court of size
To opening 3, facilitate taking out and putting into of collector 4.
Wherein, collector 4 can using heat resisting steel, sus, iron sheet, quartz, graphite, leaf, carborundum, aluminum oxide and
One or more of c/c composite material is made.
In the utility model embodiment, it is reacting part that tank body 2 is placed in part in heating furnace, heating furnace 1 and opening 3 it
Between part be collection portion, reacting part is used for inserting raw material and being placed in heating furnace 1, and collection portion is used for inserting collector 4, collects
Device 4 is placed in the upper end of tank body 2, that is, place the reacting part upper end of raw material, collection portion and opening 3 may be contained within outside heating furnace 1, tank body
2 are vacuumized by interface 5.
It is additionally provided with cooling device 6 on tank body 2 between heating furnace 1 and opening 3.
Wherein, cooling device 6 can be arranged on the External Internal of tank body 2, is such as arranged on the outer surface of tank body 2,
Or it is arranged on collector 4 outer surface within tank body 2.
Cooling device 6 is used for the tank body 2 between heating furnace 1 and opening 3 being cooled down, specifically to tank body 2
Collection portion is cooled down.Cooling device 6 can select the type of cooling by required cooling requirement, for faster cooling down collection portion.
Wherein in an embodiment, cooling device is coolant jacket, and coolant jacket is set on tank body 2, by cooling medium
Circulating cooling.Can be using water, air, inert gas, coolant as cooling medium.In one of which embodiment, adopt
It is cooled with circulating water, can effectively reduce cooling cost.
In another kind of implementation, as shown in Fig. 2 the bottom of tank body 2 is at least partially disposed at outside heating furnace 1, and tank
Body 2 bottom is provided with slag-drip opening 8.
Lower end deslagging be can achieve by slag-drip opening 8, on the premise of ensureing good seal, preparation can be improved further and produce
The speed of product and production efficiency.
During reaction, by interface 5, tank body 2 is vented, so that the vacuum in tank body 2 is met the requirements, heating furnace 7 is to reacting part
Interior raw material heating, raw material after chemical reaction generates product steam, because collection portion is located at outside heating furnace 1, positioned at collection portion
The air themperature of periphery is far below heating furnace 1, the cooling medium heat exchange of product steam and tank body 2 extraneous air or cooling device 6,
It is condensate in formation solid product on collector 4, after the production cycle, opens cover 7, take out collector 4, dress from opening 3
Entering new raw material, change to new collector 4, close cover 7, repeating said process until completing this production, in this process
In, heating furnace 1, without blowing out, keeps production status, thus realizing semi-successive cultivation, greatly improving efficiency, having saved energy
Source.
Wherein, in the utility model embodiment, heating furnace 1 can be electric furnace or combustion heating furnace.And heat
Stove 1 connects air, thus realizing electrical heating or combustion heating, electrical heating can be medium-high frequency sensing heating, heating using microwave
And resistance heating, resistance heating can be Elema, Si-Mo rod, graphite resistance heating, and the fuel that combustion heating adopts includes
Natural gas, coal gas, device in Gas, biogas or manufactured gas, manufactured fuel gas.Wherein, combustion heating, can be to a great extent compared with electrical heating
Energy saving.
Due to the vacuum state in tank body 2, atmospheric pressure can be unfavorable for the service life of tank body 2, for ensureing the use of tank body 2
In the life-span, in the present embodiment, tank body 2 is from one or more of heat resisting steel, pottery, corundum, carborundum and carbon materials material
Expect the tank body made, for ensureing sealing, workability and processing cost, preferably heat resisting steel, and preferred tank body 2 is a diameter of
100mm to 1000mm, the preferably length of tank body 2 are 300mm to 5000mm.
In addition, as shown in figure 3, multiple tank bodies 2 (being illustrated as 3) can be arranged the size based on heating furnace 1, can be more preferable
Utilization heating furnace 1 heat, carry out in multiple tank bodies simultaneously raw material reaction produce silicon oxide compound product.
Wherein, in one of which implementation of the present utility model, silicon oxide compound is silicon monoxide.
The manufacturing equipment of above-mentioned silicon oxide compound of the present utility model, by being arranged at heating furnace by the reacting part of tank body
Interior, collection portion and opening are placed in outside heating furnace, take out collector by opening opening, close opening after putting into new collector,
Whole equipment need not be cooled down, heating furnace can continuously work, efficiency high.Due to the shaft designs of equipment, can be had using Action of Gravity Field
Effect avoids product to be contaminated, and improves product quality, and improves equipment charge, improves heat utilization rate.And using perpendicular
Tank designs, and the equipment of being more beneficial for realizes mechanization, automation.
Wherein, refer to Fig. 4, Fig. 4 is that a kind of method preparing silicon oxide compound that the utility model embodiment provides is shown
Meaning property flow chart, it should be noted that the method preparing silicon oxide compound of the present embodiment is based on the above-mentioned reality of the utility model
Apply the manufacturing equipment described in example to realize, therefore, in the present embodiment, be related to the relative position between manufacturing equipment all parts
Put relation or implement form, refer to the related description of above-described embodiment, repeat no more in the present embodiment.
As shown in figure 4, the method preparing silicon oxide compound of the present embodiment comprises the following steps:
S101: Si powder and silica are mixed and is pressed into the bottom putting into described tank body after block as raw material, put
Enter collector, tank body is closed.
In one of which specific implementation, by opening cover, by Si powder and SiO 2 powder mixing after and press
It is placed in the reacting part of tank body as raw material after becoming block, the collection portion of tank body is put into collector, close cover.
S102: tank body is vacuumized by vacuumizing interface.
When implementing, vacuumized so that vacuum in tank body meets by vacuumizing interface tank body being exhausted
Reaction requires.Wherein, in a kind of possible implementation, by after vacuumizing interface tank body being vacuumized so that tank body
Vacuum remain 0.01-10000pa.
S103: open heating furnace and raw material is heated so that raw material carries out reaction produces steam.
Wherein, when unlatching heating furnace is heated, open cooling device simultaneously and cooled down.It should be noted that opening
Heating furnace and open the execution of cooling device it is also possible to before above-mentioned steps s101.
The condensation of s104: steam forms solid silicon oxide compound product on the collector, takes out collector to collect from opening
Silicon oxide compound product.
After the raw material reaction in tank body finishes, keep the operation of heating furnace and cooling device, open cover and take out collection
Device, loads new raw material in reacting part, puts into new collector in collection portion, closes cover, by interface, tank body is taken out
Vacuum, starts next round reaction, and silicon oxide compound product is peeled off from the collector taking out.So repeatedly, until preparing
Terminate.
Wherein, for realizing higher production efficiency and relatively low production cost, in the utility model embodiment, the dress of tank body
Carrying capacity is designed as 2-200kg, during the course of the reaction, controls the temperature of heating furnace to remain 1100-1400 DEG C, controls the reaction time
For 2-60 hour (putting into new collector to the time taken out between this collector).The temperature control of cooling device is 100-
900℃.
By preparing silicon oxide compound using the manufacturing equipment of the utility model embodiment, do not need to stop in preparation process
Only heating stove heat, it is achieved that the semi-continuous working of equipment, drastically increases production efficiency, it is to avoid heating furnace heats up repeatedly
The energy waste causing in temperature-fall period.
The foregoing is only embodiment of the present utility model, not thereby limit the scope of the claims of the present utility model, every
The equivalent structure made using the utility model specification and accompanying drawing content or equivalent flow conversion, or be directly or indirectly used in
Other related technical fields, are all included in the same manner in scope of patent protection of the present utility model.
Claims (6)
1. a kind of manufacturing equipment of silicon oxide compound is it is characterised in that described manufacturing equipment includes heating furnace and vertical placement
At least one tank body, described tank body top is provided with opening, and described tank body built with raw material and is arranged in heating furnace, adds described
Tank body between hot stove and described opening is provided with collector and vacuumizes interface；
Described tank body bottom is at least partially disposed at outside described heating furnace, and described tank body bottom is provided with slag-drip opening；.
Cover for opening or closing described opening is additionally provided with described tank body.
2. manufacturing equipment according to claim 1 is it is characterised in that tank body between described heating furnace and described opening
On be additionally provided with cooling device.
3. manufacturing equipment according to claim 2 it is characterised in that described cooling device be coolant jacket, described coolant jacket
It is set on described tank body, by cooling medium circulating cooling.
4. manufacturing equipment according to claim 1 is it is characterised in that described heating furnace is electric furnace or combustion heating
Stove.
5. manufacturing equipment according to claim 1 is it is characterised in that described collector is the tubular knot of at least one end open
Structure.
6. manufacturing equipment according to claim 1 is it is characterised in that described collector is the different tubular of two ends size
Structure, wherein, described collector is smaller in size than the other end towards one end of opening.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620290949.4U CN205907046U (en) | 2016-04-08 | 2016-04-08 | Apparatus for preparing silicon oxygen compound's manufacturing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620290949.4U CN205907046U (en) | 2016-04-08 | 2016-04-08 | Apparatus for preparing silicon oxygen compound's manufacturing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205907046U true CN205907046U (en) | 2017-01-25 |
Family
ID=57814978
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620290949.4U Active CN205907046U (en) | 2016-04-08 | 2016-04-08 | Apparatus for preparing silicon oxygen compound's manufacturing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205907046U (en) |
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2016
- 2016-04-08 CN CN201620290949.4U patent/CN205907046U/en active Active
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| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190829 Address after: 516227 High Temperature Calcination Workshop of Huyangkeng Section, Huangdong Village, Zhenlong Town, Huiyang District, Huizhou City, Guangdong Province Patentee after: Huizhou Dingyuan New Energy Technology Co., Ltd. Address before: 518107 Xitian Community High-tech Industrial Park, Gongming Office, Guangming New District, Shenzhen City, Guangdong Province, 1, 2, 3, 4, 5, 6, 7 A, 7 B and 8 Patentee before: Shenzhen BTR New Energy Material Co., Ltd. |