CN205874600U - Big silk bundle polyacrylonitrile wet process spinning compression roller device - Google Patents
Big silk bundle polyacrylonitrile wet process spinning compression roller device Download PDFInfo
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- CN205874600U CN205874600U CN201620630617.6U CN201620630617U CN205874600U CN 205874600 U CN205874600 U CN 205874600U CN 201620630617 U CN201620630617 U CN 201620630617U CN 205874600 U CN205874600 U CN 205874600U
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- compression roller
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Abstract
The utility model provides a big silk bundle polyacrylonitrile wet process spinning compression roller device, including driving roller (1), pressure roller adjustment device and sulfoxide solution catcher (4), pressure roller adjustment device is by hand wheel (3), hand wheel connecting rod (5), mount (6) and compression roller (2) are constituteed, hand wheel connecting rod (5) top is fixed in in hand wheel (3), it has mount (6) to control between two hand wheel connecting rod (5), threaded connection is passed through with mount (6) in hand wheel connecting rod (5), hand wheel connecting rod (5) lower part has compression roller pivot (7), mount (6) are located compression roller pivot (7) top, install compression roller (2) in compression roller pivot (7), compression roller (2) below has driving roller (1), and make compression roller (2) parallel with driving roller (1), sulfoxide solution collection device (4) is located driving roller (1) below. The utility model has the advantages of reduce the washing load of follow -up washing technology, reduce the sulfoxide loss, reduce wet process spinning cost.
Description
Technical field
This utility model relates to a kind of big tow polyacrylonitrile wet spinning press-roller device.
Background technology
Carbon fiber has the characteristics such as high specific strength, high ratio modulus, heat-resisting, corrosion-resistant, endurance, creep resistant, is a kind of high
Performance fibers material, has been widely used for Aero-Space, national defense construction, Leisure Sport articles for use, medical apparatus and instruments and building trade.
Carbon fiber can be divided into polyacrylonitrile-radical, asphaltic base, viscose-based carbon fiber, and wherein polyacrylonitrile-based carbon fibre purposes is the widest, consumption
Maximum, with the fastest developing speed, have overwhelming superiority in carbon fiber produces.
Polyacrylonitrile-based carbon fibre is prepared through pre-oxidation, carbonization process by polyacrylonitrile fibre.Polyacrylonitrile fibre
Cost accounts for the 50～60% of carbon fiber totle drilling cost.Low cost, the polyacrylonitrile fibre of high-quality are commercial production high-performance polypropylenes
The basis of itrile group carbon fiber.At present, domestic more main flow is that polyacrylonitrile fibre is prepared in spinning in a wet process, full-bodied poly-third
The dimethyl sulphoxide solution (polymer fluid) of alkene nitrile successively through multistage coagulating bath molding, washing, hot water drawing-off, oil, be dried densification
Change, steam drafting, relaxation heat setting technique prepare polyacrylonitrile fibre.
During polymer fluid coagulation forming, solvent dimethyl sulfoxide separates send out simultaneously with coagulator water double diffusion and solidifying phase
Raw, tow solidification is from outward appearance to inner essence gradually completing, fiber surface and the asynchronism of solidified inside, causes fibrous inside to produce a large amount of
Hole.Tow washing step mainly completes fiber surface and pore interior carries the washing work of dimethyl sulfoxide, to ensure silk
The internal dimethyl sulfoxide content of bundle is reduced to less than 0.09%.Under the conditions of certain washing process, the dimethyl that tow carries is sub-
Sulfone is the most, and water rinses water loss is the biggest, and wastewater discharge also can increase accordingly, and dimethyl sulfoxide waste increases, and poly-third
Alkene nitrile fiber production cost rises.
Big tow (12K, 24K, 48K etc., term " 12K " represents that every bundle fiber contains 12000 ultimate fibres) polyacrylonitrile
During wet spinning, go out coagulating bath tow because carrying the dimethyl sulphoxide solution of a large amount of high concentration containing a large amount of holes, go out
After coagulating bath tow enters follow-up washing process, because carrying a large amount of sulfoxide solution, washing load is relatively big, and water consumption is relatively big, simultaneously
The water lotion overwhelming majority is discharged with sewage form, and therefore dimethyl sulfoxide loss is more, and spinning cost is bigger.
Summary of the invention
The purpose of this utility model patent is to provide a kind of big tow polyacrylonitrile wet spinning press-roller device, and this device can
Polyacrylonitrile wet spinning is gone out the substantial amounts of high-concentration dimethyl sulfoxide aqueous solution carried in coagulating bath tow surface and hole
Extrusion, centralized recovery, reduces the cleaning load of follow-up washing process, reduces sulfoxide loss, reduce wet spinning cost.
This utility model be the technical scheme is that
A kind of big tow polyacrylonitrile wet spinning press-roller device, it includes that live-roller, press roll adjusting device and sulfoxide are molten
Collection, it is characterised in that press roll adjusting device is that handwheel is fixed on by handwheel, handwheel connecting rod, fixed mount and pressure roller composition
Handwheel connecting rod top, has fixed mount, handwheel connecting rod to be threaded connection with fixed mount between the handwheel connecting rod of two, left and right, and handwheel is even
Pressure roller rotating shaft is arranged at bar bottom, and fixed mount is positioned at above pressure roller rotating shaft, is provided with pressure roller in pressure roller rotating shaft, has transmission below pressure roller
Roller, and make pressure roller parallel with live-roller, sulfoxide solution collection device is positioned at below live-roller.
The uni-drive gear box that live-roller is connected by one end is rotated, and press roll adjusting device is fixing even by fixed mount 6
It is connected on above driving roller gear case.
The material of pressure roller is metallic substrates, plated surface polyurethane, top layer polyurethane shore hardness: 30-70HS；Live-roller
Material is metallic substrates, plated surface pottery.
This utility model is by rotating handwheel, making handwheel connecting rod be moved up and down by screw thread, drives the pressure on fixed mount
Roller moves up and down, and reaches to adjust the gap between pressure roller and live-roller, and operating tow is implemented suitably extruding, the height of extrusion
Concentration dimethyl sulphoxide aqueous solution flows into sulfoxide solution collection device, it is achieved centralized recovery.
This utility model is particularly suitable for application to big tow (12K-48K) polyacrylonitrile fibre and produces, and term " 12K " is every
Containing 12000 ultimate fibres in bundle fiber.
In actual production, dimethyl sulfoxide water can be carried according in yarn counts (12K, 24K, 48K etc.), tow hole
The size of amount of solution, is adjusted flexibly the pressure roller extruding degree to tow, on the premise of not damaging tow, maximizes recovery highly concentrated
The dimethyl sulphoxide aqueous solution of degree.
The good effect of this utility model patent:
1, in actual production, this press-roller device can be equipped on every gear stage of multistage coagulation forming technique, real
Existing high-concentration dimethyl sulfoxide solution maximizes and reclaims, and reduces the loss of wet spinning dimethyl sulfoxide, reduces production cost；
2, this press-roller device deft design, simple in construction, easy to operate；Can facilitate, flexibly, accurately adjust pressure roller and tow
Gap between live-roller；
3, this press-roller device is modular construction, and locally easily worn part (such as: the pressure roller of plated surface polyurethane) is designed to activity
Connect, can change the most at any time, it is simple to dismounting, maintenance；
4, this press-roller device usability is wide, and promotional value is high.
Accompanying drawing explanation
Fig. 1 is this utility model big tow polyacrylonitrile wet spinning press-roller device.
Fig. 2 is this utility model big tow polyacrylonitrile wet spinning press-roller device side view.
As shown in the figure: 1 is live-roller, 2 is pressure roller, and 3 is handwheel, and 4 is sulfoxide solution catcher, and 5 is handwheel connecting rod, and 6 are
Fixed mount, 7 is pressure roller rotating shaft.
Detailed description of the invention
Below in conjunction with the accompanying drawings this utility model is further illustrated.
Embodiment 1
A kind of big tow polyacrylonitrile wet spinning press-roller device, it includes that live-roller 1, press roll adjusting device and sulfoxide are molten
Collection 4, it is characterised in that press roll adjusting device is to be made up of handwheel 3, handwheel connecting rod 5, fixed mount 6 and pressure roller 2, handwheel 3
It is fixed on handwheel connecting rod 5 top, between the handwheel connecting rod 5 of two, left and right, has fixed mount 6, handwheel connecting rod 5 and fixed mount 6 to pass through screw thread
Connecting, handwheel connecting rod 5 bottom has pressure roller rotating shaft 7, fixed mount 6 to be positioned at above pressure roller rotating shaft 7, is provided with pressure in pressure roller rotating shaft 7
Roller 2, has live-roller 1, and makes pressure roller 2 parallel with live-roller 1 below pressure roller 2, sulfoxide solution collection device 4 is positioned at live-roller 1 time
Side.
The uni-drive gear box that live-roller 1 is connected by one end is rotated, and press roll adjusting device is fixing even by fixed mount 6
It is connected on above driving roller gear case.
This utility model is by rotating handwheel 3, making handwheel connecting rod 5 be moved up and down by screw thread, drives on fixed mount 6
Pressure roller 2 moves up and down, and reaches to adjust the gap between pressure roller 2 and live-roller 1, to the tow of 24K polyacrylonitrile fibre in running
Implementing suitably extruding, the high-concentration dimethyl sulfoxide aqueous solution of extrusion flows into sulfoxide solution catcher 4, it is achieved centralized recovery.
12 are spun position and produce 24k fiber, because of tow compared with big, to spin position more, carries the dimethyl of high concentration in the unit interval
The water-soluble liquid measure of sulfoxide is relatively big, and the material of pressure roller 2 is metallic substrates, the pressure roller selecting top layer polyurethane shore hardness 50HS, transmission
The material of roller 1 is metallic substrates, plated surface pottery.
When using this press-roller device, the handwheel 3 at rotating pressure roller two ends simultaneously, at the bar ensureing that pressure roller 2 is parallel with live-roller 1
Under part, adjust the gap of pressure roller 2 and live-roller 1, notes that observation is all and spin a tow solution extrusion capacity, it is ensured that all spin a tow
Suffered extruding force is identical, is guaranteeing not damage tow, under conditions of not producing fracture of wire, is increasing extruding force as far as possible, maximized
Reclaim dimethyl sulphoxide aqueous solution.Long-term use experience: during pressure roller extruding 24K tow, pressure roller is with live-roller gap 2.5mm relatively
For suitably.By the sulfoxide solution in collection device, by recovery line, send into high-concentration dimethyl sulfoxide purifying aqueous solutions and reclaim
System, purifies and reclaims sulfoxide.
Claims (5)
1. a big tow polyacrylonitrile wet spinning press-roller device, it includes live-roller (1), and press roll adjusting device and sulfoxide are molten
Collection (4), it is characterised in that press roll adjusting device is by handwheel (3), handwheel connecting rod (5), fixed mount (6) and pressure roller (2)
Composition, handwheel (3) is fixed on handwheel connecting rod (5) top, has fixed mount (6), handwheel connecting rod between the handwheel connecting rod (5) of two, left and right
(5) being threaded connection with fixed mount (6), handwheel connecting rod (5) bottom has pressure roller rotating shaft (7), fixed mount (6) to be positioned at pressure roller rotating shaft
(7) top, is provided with pressure roller (2) in pressure roller rotating shaft (7), and there is live-roller (1) pressure roller (2) lower section, and makes pressure roller (2) and transmission
Roller (1) is parallel, and sulfoxide solution collection device (4) is positioned at live-roller (1) lower section.
2. a kind of big tow polyacrylonitrile wet spinning press-roller device as described in claim 1, it is characterised in that live-roller
(1) uni-drive gear box connected by one end is rotated.
3. a kind of big tow polyacrylonitrile wet spinning press-roller device as described in claim 1, it is characterised in that pressure roller regulates
Device is fixedly connected on above driving roller gear case by fixed mount (6).
4. a kind of big tow polyacrylonitrile wet spinning press-roller device as described in claim 1, it is characterised in that pressure roller (2)
Material be metallic substrates, plated surface polyurethane, top layer polyurethane shore hardness is 30-70HS.
5. a kind of big tow polyacrylonitrile wet spinning press-roller device as described in claim 1, it is characterised in that live-roller
(1) material is metallic substrates, plated surface pottery.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620630617.6U CN205874600U (en) | 2016-06-24 | 2016-06-24 | Big silk bundle polyacrylonitrile wet process spinning compression roller device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620630617.6U CN205874600U (en) | 2016-06-24 | 2016-06-24 | Big silk bundle polyacrylonitrile wet process spinning compression roller device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205874600U true CN205874600U (en) | 2017-01-11 |
Family
ID=57692031
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620630617.6U Active CN205874600U (en) | 2016-06-24 | 2016-06-24 | Big silk bundle polyacrylonitrile wet process spinning compression roller device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205874600U (en) |
-
2016
- 2016-06-24 CN CN201620630617.6U patent/CN205874600U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230330 Address after: 030100 Jinyi Village, Yangqu County, Taiyuan City, Shanxi Province Patentee after: SHANXI GANGKE CARBON MATERIALS CO.,LTD. Address before: 030001 No. 27 Taoyuan South Road, Taiyuan City, Shanxi Province Patentee before: INSTITUTE OF COAL CHEMISTRY, CHINESE ACADEMY OF SCIENCES |
|
| TR01 | Transfer of patent right |