CN205850310U - The oxime water separation tank that a kind of diacetylmonoxime produces - Google Patents
The oxime water separation tank that a kind of diacetylmonoxime produces Download PDFInfo
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- CN205850310U CN205850310U CN201620845781.9U CN201620845781U CN205850310U CN 205850310 U CN205850310 U CN 205850310U CN 201620845781 U CN201620845781 U CN 201620845781U CN 205850310 U CN205850310 U CN 205850310U
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- oxime
- baffle
- solvent column
- column tower
- tank body
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Abstract
nullThe utility model discloses the oxime water separation tank that a kind of diacetylmonoxime of chemical production device technical field produces，Including tank body、Solvent column tower body and the drawing liquid water pump being arranged on solvent column tower body intracavity bottom，The inner chamber bottom right side of described tank body is provided with product exit，The intracavity bottom right-to-left of described tank body is respectively arranged with the first vertical baffle plate、Second baffle and third gear plate，The left side of described first baffle plate is provided with pure water inlet，The left side of described second baffle and third gear plate is provided with mixture export，Described mixture export connects connecting tube，This utility model utilizes extractant to be extracted into the dissolubility of oxime in oil phase from oxime aqueous solution by oxime，And be layered by oxime water separation tank，Thus realize the separation of oxime water，And whole apparatus structure is simple，Separation efficiency is high，The mixed liquor separated can also be sent back in solvent column，And then again separate.
Description
Technical field
This utility model relates to chemical production device technical field, and the oxime water that a kind of diacetylmonoxime produces separates
Tank.
Background technology
Diacetylmonoxime is generally colourless or faint yellow oily transparency liquid, and diacetylmonoxime is due to low toxicity, oligosaprobic characteristic, extensively
Being applied in the anti skinning agent of coating, ink, paint, meanwhile, diacetylmonoxime is also a class oxygen scavenging chemical, have low toxicity, efficiently,
Rapidly, the feature of tool passivation protection effect, additionally, diacetylmonoxime is also the raw material of neutral cross-linking agent.
In the production process of diacetylmonoxime, need oxime water is separated, but existing oxime water separation tank structure be complicated,
Oxime water can not be efficiently separated, the inefficiency of separation.
Utility model content
The purpose of this utility model is the oxime water separation tank providing a kind of diacetylmonoxime to produce, to solve above-mentioned background skill
The problem proposed in art.
For achieving the above object, this utility model provides following technical scheme: the oxime water that a kind of diacetylmonoxime produces separates
Tank, including tank body, solvent column tower body and the drawing liquid water pump being arranged on solvent column tower body intracavity bottom, on the right side of the inner chamber of described tank body
Bottom is provided with product exit, vertical the first baffle plate of the intracavity bottom right-to-left of described tank body being provided with respectively, second
Baffle plate and third gear plate, the left side of described first baffle plate is provided with pure water inlet, described second baffle and the left side of third gear plate
Being provided with mixture export, described pure water inlet and mixture export are arranged at the intracavity bottom of tank body, described mixed liquor
Outlet connection has connecting tube, and the other end of described connecting tube is connected to the right side of water pump, and the left side outfan of described water pump passes through
Pipeline is connected to the inner chamber left bottom of solvent column tower body, and the inner chamber of described solvent column tower body is provided with agitating device, described molten
The inner chamber right hand top of agent tower tower body is provided with material inlet, and the left side top of described tank body is provided with liquidometer, described tank body
Inner chamber left bottom connect and have oxime water inlet pipe, the other end of described oxime water inlet pipe is through the bottom of solvent column tower body and connects
It is connected on the bottom outfan of drawing liquid water pump.
Preferably, the half of a length of second baffle of described first baffle plate, a length of third gear of described second baffle
The half of plate.
Preferably, described first baffle plate, second baffle and third gear plate are the intracavity bottom being set in qually spaced in tank body.
Preferably, it is provided with valve in described product exit, pure water inlet and mixture export.
Preferably, described agitating device is impeller, and impeller welds with impeller axle, and impeller axle is arranged on solvent column tower body
Front and back on inwall.
Compared with prior art, the beneficial effects of the utility model are: this utility model utilizes the extractant dissolving to oxime
Oxime is extracted in oil phase from oxime aqueous solution by property, and is layered by oxime water separation tank, thus realizes the separation of oxime water, and whole
Individual apparatus structure is simple, and separation efficiency is high, additionally it is possible to is sent back in solvent column by the mixed liquor separated, and then again separates.
Accompanying drawing explanation
Fig. 1 is this utility model structural representation.
In figure: 1 tank body, 2 product exit, 3 first baffle plates, 4 pure water inlets, 5 second baffles, 6 mixture exports,
7 third gear plates, 8 connecting tubes, 9 water pumps, 10 oxime water inlet pipes, 11 drawing liquid water pumps, 12 solvent column tower bodies, 13 stirring dresses
Put, 14 material inlets, 15 liquidometers.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is carried out
Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of this utility model rather than whole
Embodiment.Based on the embodiment in this utility model, those of ordinary skill in the art are not under making creative work premise
The every other embodiment obtained, broadly falls into the scope of this utility model protection.
Fig. 1, a kind of technical scheme of this utility model offer: the oxime water separation tank that a kind of diacetylmonoxime produces, bag are provided
Include tank body 1, solvent column tower body 12 and be arranged on the drawing liquid water pump 11 of solvent column tower body 12 intracavity bottom, the inner chamber of described tank body 1
Bottom right side is provided with product exit 2, the intracavity bottom right-to-left of described tank body 1 respectively be provided with the first vertical baffle plate
3, second baffle 5 and third gear plate 7, the left side of described first baffle plate 3 is provided with pure water inlet 4, described second baffle 5 and the 3rd
The left side of baffle plate 7 is provided with mixture export 6, and described pure water inlet 4 and mixture export 6 are arranged at the inner chamber of tank body 1
Bottom, described mixture export 6 connects connecting tube 8, and the other end of described connecting tube 8 is connected to the right side of water pump 9, described water
The left side outfan of pump 9 is connected to the inner chamber left bottom of solvent column tower body 12 by pipeline, described solvent column tower body 12 interior
Chamber is provided with agitating device 13, and the inner chamber right hand top of described solvent column tower body 12 is provided with material inlet 14, described tank body 1
Left side top is provided with liquidometer 15, and the inner chamber left bottom of described tank body 1 connects oxime water inlet pipe 10, described oxime water inlet
The other end of pipe 10 passes the bottom of solvent column tower body 12 and is connected on the bottom outfan of drawing liquid water pump 11.
Wherein, the half of a length of second baffle 5 of described first baffle plate 3, a length of third gear of described second baffle 5
The half of plate 7, in order to preferably separate oxime water, described first baffle plate 3, second baffle 5 and third gear plate 7 are for being set in qually spaced in
The intracavity bottom of tank body 1, is provided with valve in described product exit 2, pure water inlet 4 and mixture export 6, in order to control liquid
The uninterrupted that body is released, described agitating device 13 is impeller, and impeller welds with impeller axle, and impeller axle is arranged on solvent column tower
Before and after body 12 on inwall, the oxime water in solvent column tower body 12 is made to be fully contacted with extractant.
Operation principle: during work, first oxime water and extractant enter in solvent column tower body 12, then by material inlet 14
It is sufficiently stirred for by the agitating device 13 in solvent column tower body 12 again, and mix homogeneously, then taking out bottom solvent column tower body 12
Oxime water containing extractant is sent in oxime water inlet pipe 10 by liquid water pump 11, during then oxime water enters the inner chamber of tank body 1, because extraction
Take agent can be extracted in oil phase from oxime aqueous solution by oxime, so oxime aqueous solution can divide in the leftward space of third gear plate 7
Layer, the oil phase containing oxime is on upper strata, and aqueous phase is in lower floor, the aqueous phase mixing so the oil phase containing oxime can cross the 3rd dividing plate 7, containing oxime
Liquid is flowed out by mixture export 6, and then the oil phase containing oxime is assembled, by last step in the leftward space of second baffle 5
May not separate the clean oil phase containing oxime to be further layered, the oil phase containing oxime can cross second baffle 5, and containing oxime
Aqueous phase mixed liquor flows out from mixture export 6, and the purest can be in the leftward space of the first baffle plate 3 containing oxime oil phase
Assemble, and the oil phase containing oxime the purest in last step is further layered, pure can cross the containing oxime oil phase
One baffle plate 3, and flow out from product exit 2, the aqueous phase after three times separate is pure, and pure aqueous phase can be from only
Flowing out in water out 4, during this, connecting tube 8 sends into water pump 9 by flow out in mixture export 6 containing oxime aqueous phase mixed liquor
In, and by water pump 9 pressure-raising in solvent column tower body 12 sent into by pipeline.
Embodiment the most of the present utility model, for the ordinary skill in the art,
It is appreciated that in the case of without departing from principle of the present utility model and spirit and these embodiments can be carried out multiple change, repair
Changing, replace and modification, scope of the present utility model is defined by the appended claims and the equivalents thereof.
Claims (5)
1. the oxime water separation tank that diacetylmonoxime produces, including tank body (1), solvent column tower body (12) be arranged on solvent column tower
The drawing liquid water pump (11) of body (12) intracavity bottom, it is characterised in that: the inner chamber bottom right side of described tank body (1) is provided with product and goes out
Mouthful (2), the intracavity bottom right-to-left of described tank body (1) be respectively arranged with vertical the first baffle plate (3), second baffle (5) and
Third gear plate (7), the left side of described first baffle plate (3) is provided with pure water inlet (4), described second baffle (5) and third gear plate
(7) left side is provided with mixture export (6), described pure water inlet (4) and mixture export (6) and is arranged at tank body (1)
Intracavity bottom, described mixture export (6) connect have connecting tube (8), the other end of described connecting tube (8) to be connected to water pump
(9) right side, the left side outfan of described water pump (9) is connected to the inner chamber left bottom of solvent column tower body (12) by pipeline,
The inner chamber of described solvent column tower body (12) is provided with agitating device (13), and the inner chamber right hand top of described solvent column tower body (12) sets
Being equipped with material inlet (14), the left side top of described tank body (1) is provided with liquidometer (15), on the left of the inner chamber of described tank body (1)
Bottom connects oxime water inlet pipe (10), and the other end of described oxime water inlet pipe (10) passes the bottom of solvent column tower body (12) also
It is connected on the bottom outfan of drawing liquid water pump (11).
The oxime water separation tank that a kind of diacetylmonoxime the most according to claim 1 produces, it is characterised in that: described first baffle plate
(3) half of a length of second baffle (5), the half of a length of third gear plate (7) of described second baffle (5).
The oxime water separation tank that a kind of diacetylmonoxime the most according to claim 1 produces, it is characterised in that: described first baffle plate
(3), second baffle (5) and third gear plate (7) are the intracavity bottom being set in qually spaced in tank body (1).
The oxime water separation tank that a kind of diacetylmonoxime the most according to claim 1 produces, it is characterised in that: described product exit
(2), it is provided with valve in pure water inlet (4) and mixture export (6).
The oxime water separation tank that a kind of diacetylmonoxime the most according to claim 1 produces, it is characterised in that: described agitating device
(13) being impeller, and impeller welds with impeller axle, impeller axle is arranged on before and after solvent column tower body (12) on inwall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620845781.9U CN205850310U (en) | 2016-08-05 | 2016-08-05 | The oxime water separation tank that a kind of diacetylmonoxime produces |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620845781.9U CN205850310U (en) | 2016-08-05 | 2016-08-05 | The oxime water separation tank that a kind of diacetylmonoxime produces |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205850310U true CN205850310U (en) | 2017-01-04 |
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ID=57657727
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620845781.9U Active CN205850310U (en) | 2016-08-05 | 2016-08-05 | The oxime water separation tank that a kind of diacetylmonoxime produces |
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| CN (1) | CN205850310U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107670336A (en) * | 2017-11-10 | 2018-02-09 | 大丰鑫源达化工有限公司 | A kind of continous way oily-water seperating equipment |
-
2016
- 2016-08-05 CN CN201620845781.9U patent/CN205850310U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107670336A (en) * | 2017-11-10 | 2018-02-09 | 大丰鑫源达化工有限公司 | A kind of continous way oily-water seperating equipment |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Oxime water separating tank for producing butanone oxime Effective date of registration: 20220125 Granted publication date: 20170104 Pledgee: Bank of China Limited Xiantao branch Pledgor: HUBEI XIANLIN CHEMICAL CO.,LTD. Registration number: Y2022420000029 |