CN205575972U - Hydrogenated vegetable oil midbody sorbitol acid anhydride monostearate apparatus for producing - Google Patents
Hydrogenated vegetable oil midbody sorbitol acid anhydride monostearate apparatus for producing Download PDFInfo
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- CN205575972U CN205575972U CN201620338407.XU CN201620338407U CN205575972U CN 205575972 U CN205575972 U CN 205575972U CN 201620338407 U CN201620338407 U CN 201620338407U CN 205575972 U CN205575972 U CN 205575972U
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- storage tank
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- delivery pump
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- vegetable oil
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Abstract
The utility model provides a hydrogenated vegetable oil midbody sorbitol acid anhydride monostearate apparatus for producing mainly includes: sorbitol storage tank, alkali lye storage tank, hydrogen peroxide solution storage tank, feedstock pump, enamel reactor, purification and separation jar, delivery pump, bleaching jar, the hydrogen peroxide solution storage tank is connected with feedstock pump, and feedstock pump is connected with enamel reactor, and the alkali lye storage tank is connected with feedstock pump, and feedstock pump is connected with enamel reactor, and enamel reactor is connected with the delivery pump, and the delivery pump is connected with the purification and separation jar, and the purification and separation jar is connected with the delivery pump, and the delivery pump is connected with enamel reactor, wherein, sorbitol storage tank full volume 10.03 10.35m3, diameter of drum 1650 - 1790mm, 3500 - 4100mm of length, head thickness 8.5 9.6mm, the feedstock pump flow 759 782m3h, lift 79 88m, rotational speed 1550 does 1590rmin inhale journey 5.5 5.7m, shaft power 219 243kw, enamel reactor nominal volume 2100 does 2900L press from both sides cover capacity 760 1010L, the outer pot diameter 1550 1680mm, power of motor 8 10kw, agitation speed 65 75rmin.
Description
Technical field
The present invention relates to a kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units.
Background technology
Sorbitan monostearate can be used for vegetable protein beverage, juice-type beverage, Lac Bovis seu Bubali, toffee, ice cream, face
Bag, cake, solid beverage, chocolate, maximum usage amount is 3.0g/kg；Butter, instant coffee, dry yeast, hydrogenated vegetable oil,
10.0g/kg.It is dissolved in ethanol, ether, methanol and the carbon tetrachloride of heat, is scattered in warm water and benzene, insoluble in cold water and acetone.
Freezing point 50～52 DEG C, HLB value 4.7.For cheese, maximum usage amount is 10.0g/kg.For bread, in bread making process
In, this product is directly added in dough after dissolving, it is possible to and shortening mixture, consumption is the 0.35%～0.5% of flour.After addition
Bread can be made soft, delaying aging.Owing to oils and fats is dispersed, bubble uniforms, it will be apparent that improve baked goods quality.For
Cake, use compounding with other emulsifying agents, the moisture in cake raw material, butter equal distribution can be made uniform, form fine and closely woven pore
Structure, improves the quality of cake.Ice cream making adds this product of 0.2%～0.3%, ice-cream products can be made hard, become
Shape is stable, occurs without " change soup " phenomenon.Chocolate adds the 0.1% of total material～this product of 0.3%, adipic crystals can be prevented
Float on surface and form " frosting " phenomenon, cause surface staining, the most also prevent spoiled by rancid oil or fat, improve gloss, strengthen wind
Taste and flexibility.Sorbitan monostearate is as hydrogenated vegetable oil intermediate, and its process units is good and bad for improving product
Quality, reduces by-products content and has Important Economic meaning.
Summary of the invention
It is an object of the invention to provide a kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units, main
Including: Sorbitol storage tank (F101), alkali liquor storage tank (F102), hydrogen peroxide storage tank (F103), raw material pump (J101, J102,
J103), enamel reaction still (D101), purification separation tank (F104), delivery pump (J104, J105), bleaching tank (D102)；This production
Annexation between device ingredient is: hydrogen peroxide storage tank (F103) is connected with raw material pump (J103), raw material pump
(J103) being connected with enamel reaction still (D101), alkali liquor storage tank (F102) is connected with raw material pump (J102), raw material pump
(J102) being connected with enamel reaction still (D101), enamel reaction still (D101) is connected with delivery pump (J104), delivery pump
(J104) being connected with purification separation tank (F104), purification separation tank (F104) is connected with delivery pump (J105), delivery pump
(J105) it is connected with enamel reaction still (D101)；Wherein, Sorbitol storage tank (F101) total volume 10.03--10.35m3, cylinder
Body diameter 1650 1790mm, length 3500 4100mm, head thickness 8.5--9.6mm；Raw material pump (J101) flow 759--
782m3/h, lift 79--88m, rotating speed 1550--1590r/min, suction 5.5--5.7m, shaft power 219--243kw；Enamel
Reactor (D101) nominal volume 2100--2900L, chuck capacity 760--1010L, outer pot diameter 1550--1680mm, motor
Power 8--10kw, speed of agitator 65-75r/min；Wherein, described Sorbitol storage tank (F101) cylinder wall thickness 6.1
6.9mm；Described enamel reaction still (D101) interior pot diameter 1310--1680mm.
A kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units, production principle is: sorbitol is with hard
Fat acid generation dehydration esterification reacts and obtains.Reaction equation is as follows:
A kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units, concrete production procedure is:
Sorbitol in F101 is pumped in reactor D101 by metering, digs vesicle in decompression dehydration to still, then add
Enter stearic acid, add 30% alkali liquor 5 8kg, at reduced pressure conditions；140 150 DEG C it are warming up to, the most slowly in two hours
It is further continued for heating up after being warming up to 160 170 DEG C of insulations 4--5 hour, until 190 DEG C, then it is incubated 2--3 hour at a temperature of this, take out
Acid number surveyed by sample, when acid number terminates to about 8mgKOH/g esterification.Pump in F104 and stand, cool overnight, remove bottom burnt
Compound.Material is transported in D102, adds appropriate hydrogen peroxide for decoloration, is finally warming up to about 90--100 DEG C, cools down molding, bag
Fill to obtain finished product.
The invention has the advantages that: decrease reaction intermediate link, reduce reaction temperature and response time, improve reaction
Yield.
Accompanying drawing explanation
Fig. 1 is a kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units figure
Specifically include that Sorbitol storage tank (F101), alkali liquor storage tank (F102), hydrogen peroxide storage tank (F103), raw material pump
(J101, J102, J103), enamel reaction still (D101), purification separation tank (F104), delivery pump (J104, J105), bleaching tank
(D102)；
Detailed description of the invention
Below in conjunction with being embodied as example, the invention will be further described:
A kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units
Example 1:
Raw materials for production and consumption
Sorbitol in F101 is pumped in reactor D101 by metering, digs vesicle in decompression dehydration to still, then add
Enter stearic acid, add 30% alkali liquor 6kg, at reduced pressure conditions；It is warming up to 140 DEG C in two hours, is then to slowly warm up to 160
DEG C insulation was further continued for heating up after 4 hours, until 190 DEG C, then was incubated 2 hours at a temperature of this, and acid number is surveyed in sampling, when acid number arrives
About 8mgKOH/g esterification terminates.Pump in F104 and stand, cool overnight, remove bottom carbonizing matter.Material is transported to
In D102, add appropriate hydrogen peroxide for decoloration, be finally warming up to about 90 DEG C, cool down molding, pack to obtain finished product 1.
Finished product 1 character
| Outward appearance | Brown wax | Saponification number | 165mgKOH/g |
| Hydroxyl value | 280mgKOH/g | Moisture | < 1.3% |
| Acid number | <7mgKOH/g |
Example 2:
Raw materials for production and consumption
Sorbitol in F101 is pumped in reactor D101 by metering, digs vesicle in decompression dehydration to still, then add
Enter stearic acid, add 30% alkali liquor 6kg, at reduced pressure conditions；It is warming up to 145 DEG C in two hours, is then to slowly warm up to 165
DEG C insulation was further continued for heating up after 4.5 hours, until 190 DEG C, then was incubated 2.5 hours at a temperature of this, and acid number is surveyed in sampling, when acid number arrives
About 8mgKOH/g esterification terminates.Pump in F104 and stand, cool overnight, remove bottom carbonizing matter.Material is transported to
In D102, add appropriate hydrogen peroxide for decoloration, be finally warming up to about 95 DEG C, cool down molding, pack to obtain finished product 2.
Finished product 2 character
| Outward appearance | Brown wax | Saponification number | 175mgKOH/g |
| Hydroxyl value | 290mgKOH/g | Moisture | < 1.2% |
| Acid number | <6mgKOH/g |
Example 3:
Raw materials for production and consumption
Sorbitol in F101 is pumped in reactor D101 by metering, digs vesicle in decompression dehydration to still, then add
Enter stearic acid, add 30% alkali liquor 8kg, at reduced pressure conditions；It is warming up to 150 DEG C in two hours, is then to slowly warm up to 170
DEG C insulation was further continued for heating up after 5 hours, until 190 DEG C, then was incubated 3 hours at a temperature of this, and acid number is surveyed in sampling, when acid number arrives
About 8mgKOH/g esterification terminates.Pump in F104 and stand, cool overnight, remove bottom carbonizing matter.Material is transported to
In D102, add appropriate hydrogen peroxide for decoloration, be finally warming up to about 100 DEG C, cool down molding, pack to obtain finished product 3.
Finished product 3 character
| Outward appearance | Brown wax | Saponification number | 185mgKOH/g |
| Hydroxyl value | 310mgKOH/g | Moisture | < 1.1% |
| Acid number | <5mgKOH/g |
Claims (3)
1. a hydrogenated vegetable oil intermediate sorbitan monostearate process units, it is characterised in that specifically include that Pyrusussuriensis
Sugar alcohol storage tank (F101), alkali liquor storage tank (F102), hydrogen peroxide storage tank (F103), raw material pump (J101, J102, J103), enamel are anti-
Answer still (D101), purification separation tank (F104), delivery pump (J104, J105), bleaching tank (D102)；This process units ingredient
Between annexation be: hydrogen peroxide storage tank (F103) is connected with raw material pump (J103), and raw material pump (J103) reacts with enamel
Still (D101) is connected, and alkali liquor storage tank (F102) is connected with raw material pump (J102), raw material pump (J102) and enamel reaction still
(D101) being connected, enamel reaction still (D101) is connected with delivery pump (J104), delivery pump (J104) and purification separation tank
(F104) being connected, purification separation tank (F104) is connected with delivery pump (J105), delivery pump (J105) and enamel reaction still
(D101) it is connected；Wherein, Sorbitol storage tank (F101) total volume 10.03--10.35m3, barrel diameter 1650
1790mm, length 3500 4100mm, head thickness 8.5--9.6mm；Raw material pump (J101) flow 759--782m3/h, lift
79--88m, rotating speed 1550--1590r/min, suction 5.5--5.7m, shaft power 219--243kw；Enamel reaction still (D101) is public
Claim volume 2100--2900L, chuck capacity 760--1010L, outer pot diameter 1550--1680mm, power of motor 8--10kw, stir
Mix rotating speed 65-75r/min.
A kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units, its feature
It is, described Sorbitol storage tank (F101) cylinder wall thickness 6.1 6.9mm.
A kind of hydrogenated vegetable oil intermediate sorbitan monostearate process units, its feature
It is, described enamel reaction still (D101) interior pot diameter 1310--1680mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620338407.XU CN205575972U (en) | 2016-04-20 | 2016-04-20 | Hydrogenated vegetable oil midbody sorbitol acid anhydride monostearate apparatus for producing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620338407.XU CN205575972U (en) | 2016-04-20 | 2016-04-20 | Hydrogenated vegetable oil midbody sorbitol acid anhydride monostearate apparatus for producing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205575972U true CN205575972U (en) | 2016-09-14 |
Family
ID=56863499
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620338407.XU Expired - Fee Related CN205575972U (en) | 2016-04-20 | 2016-04-20 | Hydrogenated vegetable oil midbody sorbitol acid anhydride monostearate apparatus for producing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205575972U (en) |
-
2016
- 2016-04-20 CN CN201620338407.XU patent/CN205575972U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160914 Termination date: 20170420 |