CN205091292U - Sodium, potassium, biochemical analysis dry plate of chlorion - Google Patents
Sodium, potassium, biochemical analysis dry plate of chlorion Download PDFInfo
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- CN205091292U CN205091292U CN201520830904.7U CN201520830904U CN205091292U CN 205091292 U CN205091292 U CN 205091292U CN 201520830904 U CN201520830904 U CN 201520830904U CN 205091292 U CN205091292 U CN 205091292U
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- sodium
- potassium
- electrode
- dry plate
- chlorion
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- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 title claims abstract description 51
- 239000011734 sodium Substances 0.000 title claims abstract description 51
- 229910052708 sodium Inorganic materials 0.000 title claims abstract description 51
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 title claims abstract description 37
- 229910052700 potassium Inorganic materials 0.000 title claims abstract description 37
- 239000011591 potassium Substances 0.000 title claims abstract description 37
- 238000012742 biochemical analysis Methods 0.000 title claims abstract description 27
- 241000370738 Chlorion Species 0.000 title claims abstract description 26
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims abstract description 23
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910001414 potassium ion Inorganic materials 0.000 claims abstract description 17
- 150000002500 ions Chemical class 0.000 claims abstract description 16
- 239000012528 membrane Substances 0.000 claims description 26
- 229910052751 metal Inorganic materials 0.000 claims description 14
- 239000002184 metal Substances 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 150000003839 salts Chemical class 0.000 claims description 6
- 239000002904 solvent Substances 0.000 claims description 6
- 239000004094 surface-active agent Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 229920001940 conductive polymer Polymers 0.000 claims description 4
- -1 plastifier Substances 0.000 claims description 4
- 239000003899 bactericide agent Substances 0.000 claims description 2
- 230000002452 interceptive effect Effects 0.000 claims description 2
- 229920005596 polymer binder Polymers 0.000 claims description 2
- 239000002491 polymer binding agent Substances 0.000 claims description 2
- 230000007480 spreading Effects 0.000 claims description 2
- 238000003892 spreading Methods 0.000 claims description 2
- 239000006172 buffering agent Substances 0.000 claims 1
- 238000009413 insulation Methods 0.000 claims 1
- 230000004044 response Effects 0.000 abstract description 10
- 239000007788 liquid Substances 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000012423 maintenance Methods 0.000 abstract description 2
- 238000005259 measurement Methods 0.000 abstract description 2
- 229910001415 sodium ion Inorganic materials 0.000 abstract description 2
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 11
- 229910021607 Silver chloride Inorganic materials 0.000 description 6
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 6
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 5
- 238000001035 drying Methods 0.000 description 5
- 229910052709 silver Inorganic materials 0.000 description 5
- 239000004332 silver Substances 0.000 description 5
- 210000001124 body fluid Anatomy 0.000 description 3
- 239000010839 body fluid Substances 0.000 description 3
- 238000003745 diagnosis Methods 0.000 description 3
- 239000003792 electrolyte Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000523 sample Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 206010011409 Cross infection Diseases 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 206010029803 Nosocomial infection Diseases 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000010876 biochemical test Methods 0.000 description 1
- 210000000476 body water Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- HGAZMNJKRQFZKS-UHFFFAOYSA-N chloroethene;ethenyl acetate Chemical compound ClC=C.CC(=O)OC=C HGAZMNJKRQFZKS-UHFFFAOYSA-N 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000007772 electroless plating Methods 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000002555 ionophore Substances 0.000 description 1
- 230000000236 ionophoric effect Effects 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 230000001575 pathological effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000139 polyethylene terephthalate Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000012088 reference solution Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000001771 vacuum deposition Methods 0.000 description 1
Landscapes
- Investigating Or Analysing Biological Materials (AREA)
Abstract
The utility model relates to a sodium, potassium, biochemical analysis dry plate of chlorion belongs to the biochemical sensor technology field of vim and vigour for sodium in the detecting body liquid, potassium, chlorine ion concentration. The dry plate includes: supporting layer, sodium ion selective electrode, potassium ion selective electrode, chlorine ion selective electrode, intermediate level, salt bridge, top layer. Every sodium, potassium, biochemical analysis dry plate of chlorion has two sodium, potassium, chlorine ion selective electrode, corresponds each other. The utility model discloses the dry plate can overcome that the operation that traditional ion selective electrode exists is complicated, the operation and maintenance is with high costs, low -response, the shortcoming that is difficult for carrying, in the liquid sodium, potassium, chlorine ion concentration but the simultaneous measurement awaits measuring, and easy operation, fast, small, the portable of response speed, and prepare that the process is simple, low in production cost, be fit for big industrial production in batches.
Description
Technical field
The utility model relates to vim and vigour biochemical sensor technologies field, particularly relates to a kind of sodium, potassium, chlorion biochemical analysis dry plate.
Background technology
The development of modern medicine, the particularly rescue of clinical urgent patient, need to test to the electrolyte of human body, and in body fluid, sodium, potassium, chlorine ion concentration are one of important indicator of inspection.Under pathological conditions, bacterium, virus etc. can cause body fluid capacity, composition and potential of hydrogen to change, and cause human body water, electrolyte and disturbance of acid-base balance, thus affect the normal physiological function of human body assembling organ, even jeopardize patient vitals.Therefore, the biochemical test detecting water, electrolyte and acid base equilibrium has become the diagnosis of clinical numerous disease, treatment is assessed and the important evidence of Index for diagnosis.
In current detection body fluid, sodium, potassium, chlorine ion concentration adopt ion-selective electrode.The interior reference solution of conventional ion electrodes selective generally adopts electrolyte solution, can only at lower temperature, pressure operation, its cost of manufacture is higher, operation and maintenance is complicated, not portable, the demand of the occasions such as operation, emergency treatment, field rescue cannot be met, also cannot adapt to the trend of domestic medicine, modern medical service in-vitro diagnosis apparatus pattern.Novel detection means adopts dry ion-selective electrodes to detect, have simple to operate, measure accurately, the time is short, sampling is few, effectively prevent the impact of cross-infection on test result.
Chinese patent CN104316584A discloses and a kind ofly measures sensor of multinomial ion concentration and preparation method thereof, sodium, potassium, chlorine ion concentration can be measured simultaneously, but its ion concentration measurement is limited in scope, and reaction electrode to need wire to be connected with contacting between electrode, technique relative complex.
Summary of the invention
The utility model provides a kind of sodium, potassium, chlorion biochemical analysis dry plate, and measuring accuracy is high, long-time stability good, and the response time is short, and structure is simple, volume is little, and preparation technology is simple, production cost is low, is applicable to producing in enormous quantities.
The utility model sodium, potassium, chlorion biochemical analysis dry plate comprise: supporting layer, sodium selective electrode, potassium ion-selective electrode, Chloride selective electrode, middle layer, top layer and salt bridge.
In the utility model, supporting layer plays protection and supports ion-selective electrode effect, and top layer is provided with inlet and gas port, and middle layer is provided with liquid pool, and salt bridge is sealed between middle layer and top layer.
Supporting layer, middle layer and top layer are selected from polypropylene, Polyvinylchloride, tygon, polyester non-conductive polymer material, and salt bridge is filter paper material.
Sodium, potassium ion-selective electrode comprise: electrode, reference layer, ion-selective membrane.Chloride selective electrode comprises: electrode, polymeric membrane.
Electrode.In the utility model dry plate, electrode comprises metal level and metal salt.Metal salt and metal level form phase boundary potential, have stable electromotive force response.
Electrode metal layer is attached to non-conductive polymer surface, be improve electrode stability, shorten the response time, the utility model can adopt vacuum coating, the mode of electroless plating or plating prepares metal level.Metal salt can adopt the method for chemical oxidation to obtain, and uses iron chloride or liquor potassic permanganate to be oxidized metal level.
Reference layer.Reference layer comprises non-conductive polymer cementing agent, surfactant, bactericidal agent, spreading agent, slaine.
For ensureing the bond strength of reference layer and ion-selective membrane, prevent biochemical analysis dry plate response signal accuracy and long-time stability from reducing, reference layer water cut can not be too high or too low, and reference layer optimum moisture content is 30% ~ 40%.
The utility model by controlling drying time of reference layer, temperature, humidity fixes reference layer slaine proportioning and water cut, optimum drying condition: temperature 25 DEG C, relative humidity 50%, time 40min.
Sodium, potassium ion selective membrane.Sodium, potassium ion selective membrane comprise: high polymer binder, ionophore, carrier solvent, negative ion agent interfering and surfactant.
Chloride selective electrode polymeric membrane.Instead of reference liquid in traditional Chloride selective electrode and ion-selective membrane with polymeric membrane in the utility model, polymeric membrane is uniform cell structure, and 1 ~ 3 μm, aperture, has good longitudinal diffusion coefficient and perviousness, have protective effect simultaneously to electrode.
Polymeric membrane comprises: cementing agent, solvent, volatile solvent, plastifier, surfactant.
The drying condition of polymeric membrane can directly affect membrane micropore size and homogeneity, therefore needs the drying condition controlling polymeric membrane.Preferred drying process: temperature 25 DEG C, relative humidity 25%, time 60min.
Sodium, potassium, Chloride selective electrode that each sodium, potassium, chlorion biochemical analysis dry plate have two panels identical, and position is mutually corresponding.During test, electrode self electromotive force is cancelled out each other, and response potential stability improves.
Be different from existing patent intermediate ion choice electrode, the utility model sodium, potassium, chlorion biochemical analysis dry plate have the following advantages: (1) can measure sodium, potassium, chlorine ion concentration in liquid to be measured simultaneously, simple to operate, greatly improves work efficiency; (2) by controlling reference layer pH and water cut, sodium, the measuring accuracy of potassium ion-selective electrode and long-time stability are improved; (3) with the reference layer in Chloride selective electrode polymeric membrane replacement conventional ion choice electrode and ion-selective membrane, structure is simple; (4) use the metal/metal salt thin electrode of surface uniform, greatly shorten sodium, potassium, chlorion biochemical analysis dry plate response time, can equilibrium establishment within 7s, form stable response electromotive force.
Accompanying drawing explanation
Fig. 1 is sodium, potassium, chlorion biochemical analysis dry plate schematic diagram.
Fig. 2 is sodium, potassium, Chloride selective electrode schematic diagram.
Fig. 3 is sodium, potassium, chlorion biochemical analysis dry plate test concentration known solution response electromotive force.
Embodiment
With embodiment, the utility model is described in detail by reference to the accompanying drawings.
As shown in Figure 1, sodium, potassium, chlorion biochemical analysis dry plate, comprise supporting layer 1, sodium selective electrode 2, potassium ion-selective electrode 3, Chloride selective electrode 4, middle layer 5, salt bridge 6, top layer 7.
As shown in Figure 2, sodium selective electrode comprises: silver layer 21, silver chloride layer 22, reference layer 23, sodion selective membrane 24; Potassium ion-selective electrode comprises: silver layer 31, silver chloride layer 32, reference layer 33, potassium ion selective membrane 34; Chloride selective electrode comprises: silver layer 41, silver chloride layer 42, polymeric membrane 43.
Silver coating 21,31,41 is attached to polyethylene terephthalate surface, silver chloride layer 22,32,42 is obtained by the front 2/3 section of oxidation of silver layer 21,31,41, reference layer is attached on silver chloride layer 22,32 respectively, sodium, potassium ion selective membrane are attached on solid state reference layer 23,33, and polymeric membrane is directly attached on silver chloride layer 42; Salt bridge is sealed between middle layer 5 and top layer 7, and 2 sodium, potassium, Chloride selective electrode 2,3,4 align with middle layer 5 pore location, and middle layer and supporting layer 1 align and be bondingly assembled into dry plate.
Sodium, potassium, chlorion biochemical analysis dry plate long-term storage conditions are :-18 ~-10 DEG C.
Sodium, potassium, chlorion biochemical analysis dry plate using method, use after needing to place 1h at normal temperatures when taking out from low temperature environment, keeps probe temperature 37 ± 0.1 DEG C during test.Insert in test trough by dry plate during test, two lateral opening dropping reference liquid and test fluid respectively, required sample 10 ~ 15 μ L, the test duration is less than 30s.
In order to advantage of the present utility model is better described, the utility model provides 1 group of experimental data, specific as follows.
Example 1, respond electromotive force with sodium, potassium, chlorion biochemical analysis dry plate test concentration known solution (Na ion concentration 140mmol/L, potassium concentration 5mmol/L, chlorine ion concentration 110mmol/L), test result as shown in Figure 3.
The above its object is to person skilled in the art can be understood content of the present utility model and implement according to this only for technical conceive of the present utility model and feature are described, can not limit protection domain of the present utility model with this.All modifications done according to the Spirit Essence of the utility model main technical schemes, all should be encompassed within protection domain of the present utility model.
Claims (9)
1. sodium, potassium, a chlorion biochemical analysis dry plate, is characterized in that: described sodium, potassium, chlorion biochemical analysis dry plate comprise supporting layer, insulation course, salt bridge, electrode, reference layer, sodium selective electrode, potassium ion-selective electrode, Chloride selective electrode.
2. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described sodium, potassium ion-selective electrode comprise electrode, reference layer, ion-selective membrane; Described Chloride selective electrode comprises electrode, polymeric membrane.
3. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described electrode is metal/metal salt thin electrode, and electrode comprises metal level and metal salt.
4. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described sodium, potassium ion-selective electrode reference layer comprise non-conductive polymer cementing agent, surfactant, bactericidal agent, spreading agent, buffering agent, slaine.
5. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described sodium, potassium ion-selective electrode reference layer are attached on the electrode of sodium, potassium ion-selective electrode, water cut 30% ~ 40%.
6. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described sodium, potassium ion selective membrane comprise high polymer binder, negative ion agent interfering, carrier, carrier solvent, surfactant.
7. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described sodium, potassium ion selective membrane be attached to dry after on reference layer.
8. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described Chloride selective electrode polymeric membrane comprises cementing agent, solvent, volatile solvent, plastifier, surfactant.
9. sodium, potassium, chlorion biochemical analysis dry plate according to claim 1, is characterized in that: described Chloride selective electrode polymeric membrane is attached on electrode.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520830904.7U CN205091292U (en) | 2015-10-23 | 2015-10-23 | Sodium, potassium, biochemical analysis dry plate of chlorion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520830904.7U CN205091292U (en) | 2015-10-23 | 2015-10-23 | Sodium, potassium, biochemical analysis dry plate of chlorion |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205091292U true CN205091292U (en) | 2016-03-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520830904.7U Expired - Fee Related CN205091292U (en) | 2015-10-23 | 2015-10-23 | Sodium, potassium, biochemical analysis dry plate of chlorion |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205091292U (en) |
-
2015
- 2015-10-23 CN CN201520830904.7U patent/CN205091292U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170203 Address after: 276000 Shandong city of Linyi province high tech Zone bimonthly road innovation building the first floor of block B Patentee after: High and new technology industrial development zone, Linyi Shuan Hang material Science and Technology Ltd. Address before: 100094 Beijing city Haidian District Yongfeng Road, sea Feng Lian villa 17-2-902 Patentee before: Wu Guoqing |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160316 Termination date: 20171023 |