CN205042480U - Chemical synthesis device - Google Patents
Chemical synthesis device Download PDFInfo
- Publication number
- CN205042480U CN205042480U CN201520827423.0U CN201520827423U CN205042480U CN 205042480 U CN205042480 U CN 205042480U CN 201520827423 U CN201520827423 U CN 201520827423U CN 205042480 U CN205042480 U CN 205042480U
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- China
- Prior art keywords
- reaction vessel
- gear
- shaft
- container cover
- fixed
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- Mixers Of The Rotary Stirring Type (AREA)
- Accessories For Mixers (AREA)
Abstract
The utility model discloses a chemical synthesis device, including reaction vessel, reaction vessel's top sets up the container lid, reaction vessel's the vertical (mixing) shaft that sets up in inside, set up the stirring rake on the (mixing) shaft, the stirring rake is extending structure, be equipped with the slider on the stirring rake, set up the baffle on the slider, the upside and the downside of (mixing) shaft still are equipped with first gear and dead lever, the one end that the (mixing) shaft was kept away from to the dead lever sets up fixed block and bearing, the inner of bearing is fixed in on the fixed block, the fixed second gear that sets up in outer end of bearing, the second gear is engaged with the first gear, set up the fixed axle between two second gears, set up stirring vane on the fixed axle, reaction vessel's inside sets up the zone of heating, the outside sets up the cooling water piping layer. The beneficial effects of the utility model are that: stirring range is more extensive, stirs more evenly, and can satisfy has the different experiments that require to the stirring, improves the experiment effect, container lid can be dismantled with reaction vessel and be connected, and is convenient to reaction vessel inside examining and repairing the maintenance.
Description
Technical field
The utility model relates generally to technical field of chemical reactions, specifically a kind of chemical synthesizer.
Background technology
In chemical experiment, stir and can promote that heating, cooling and device are to the heat transfer of material, and make the equalizing temperature of material; The carrying out of the chemical reactions such as dissolving, crystallization, cohesion can be promoted; The mixing uniformity of each composition in material can also be promoted.
In chemical synthesis, different experiments is different to the requirement of stirring, but in existing chemical synthesizer is all single agitating device, stirs scope less, and can not meet stirring the different experiment having requirement simultaneously.
Utility model content
The purpose of this utility model is to provide a kind of chemical synthesizer, it can solve deficiency of the prior art, paddle and stirring vane act on simultaneously can make stir wider general, stir evenly, and can meet stirring the experiment having different requirements, make experiment effect better; Removably connecting of container cover and reaction vessel, conveniently can carry out repair and maintenance to reaction vessel interior; The inside of reaction vessel can also be cleared up easily and efficiently by hairbrush.
The utility model for achieving the above object, is achieved through the following technical solutions:
A kind of chemical synthesizer, comprise reaction vessel, the top of described reaction vessel arranges container cover, described container cover and reaction vessel seal and removably connect, the inner vertical of described reaction vessel arranges shaft, described shaft arranges paddle, described paddle is stretching structure, described paddle is provided with slide block, described slide block slides along paddle length direction, described slide block arranges baffle plate, the top and bottom of described shaft are also provided with the first gear and fixed bar, described fixed bar is positioned at the outside of the first gear, described fixed bar arranges fixed block and bearing away from one end of shaft, the inner of described bearing is fixed on fixed block, the outer end of described bearing is fixedly installed the second gear, described second gear and the first gears meshing, between two the second gears, fixed axis is set, described fixed axis is fixedly connected with the inner of the second gear, described fixed axis arranges stirring vane, described shaft stretches out from the top of container cover, the top of described container cover is provided with drive motors, described drive motors is connected with shaft, the top of described container cover is provided with charging aperture, water filling port, vacuum orifice and exhaust outlet, the bottom of described reaction vessel is provided with discharging opening, the inside of described reaction vessel arranges zone of heating, electrical heating elements is provided with in described zone of heating, the outer setting cooling water pipe channel layer of described reaction vessel, the downside of described cooling water pipe channel layer is provided with cooling water inlet, the upside of described cooling water pipe channel layer is provided with coolant outlet, the inside set temperature sensor of described reaction vessel, the outer setting temperature controller of described cooling water pipe channel layer, described temperature controller is connected with temperature sensor.
Described baffle plate arranges hairbrush, and described hairbrush is detachably installed on baffle plate.
Be bolted connection between described container cover and reaction vessel.
Sealing gasket is provided with between described container cover and reaction vessel.
The bottom of described reaction vessel is arcuate structure.
Contrast prior art, the utility model beneficial effect is:
1, paddle and stirring vane act on simultaneously can make to stir evenly, stir wider general, and can meet and have the dissimilar experiment of requirement to stirring, make experiment effect better; Removably connecting of container cover and reaction vessel, conveniently can carry out repair and maintenance to reaction vessel interior.
2, hairbrush be arranged so that cleaning reaction vessel interior time more convenient, quick, clean; The detachable installation of hairbrush and baffle plate, facilitates it to change, and when testing, pulls down hairbrush, can not affect the normal operating of experiment.
3, be bolted connection between container cover and reaction vessel, the connection between container cover and reaction vessel can be made more fastening, certain pressure can be born.
4, the setting of sealing gasket makes the better tightness between container cover and reaction vessel.
5, the bottom of reaction vessel is arcuate structure, product can be made to discharge more complete.
Accompanying drawing explanation
Accompanying drawing 1 is structural representation of the present utility model.
Label shown in accompanying drawing: 1, reaction vessel; 2, container cover; 3, shaft; 4, paddle; 5, slide block; 6, baffle plate; 7, the first gear; 8, fixed bar; 9, fixed block; 10, bearing; 11, the second gear; 12, fixed axis; 13, stirring vane; 14, drive motors; 15, charging aperture; 16, water filling port; 17, vacuum orifice; 18, exhaust outlet; 19, discharging opening; 20, zone of heating; 21, cooling water pipe channel layer; 22, cooling water inlet; 23, coolant outlet; 24, temperature sensor; 25, temperature controller; 26, hairbrush; 27, bolt.
Detailed description of the invention
By reference to the accompanying drawings and specific embodiment, the utility model is described in further detail.Should be understood that these embodiments are only not used in restriction scope of the present utility model for illustration of the utility model.In addition should be understood that those skilled in the art can make various changes or modifications the utility model, and these equivalent form of values fall within the application's appended claims limited range equally after the content of having read the utility model instruction.
A kind of chemical synthesizer, comprise reaction vessel 1, the top of described reaction vessel 1 arranges container cover 2, and described container cover 2 seals with reaction vessel 1 and removably connects, and carries out repair and maintenance after conveniently pulling down container cover 2 to reaction vessel 1 inside.The inner vertical of described reaction vessel 1 arranges shaft 3, and described shaft 3 arranges paddle 4, and described paddle 4 is stretching structure, can regulate the length of paddle 4 as required, makes it adapt to different experiments.Described paddle 4 is provided with slide block 5, described slide block 5 slides along paddle 4 length direction, described slide block 5 arranges baffle plate 6, baffle plate 6 can increase stirring dynamics, when needs baffle plate 6 increases stirring dynamics, moving slider 5 makes it drive baffle plate 6 to move along paddle 4 to the inwall direction of reaction vessel 1, then uses holding screw to be fixed on paddle 4 by slide block 5; When without the need to increasing stirring dynamics, moving slider 5 makes it drive the direction of baffle plate 6 along paddle 4 to shaft 3 to move, and uses holding screw that slide block 5 is fixed on paddle 4 on the position of shaft 3.The top and bottom of described shaft 3 are also provided with the first gear 7 and fixed bar 8, and described fixed bar 8 is positioned at the outside of the first gear 7.First gear 7 uses steady pin to be fixedly installed on shaft 3, and shaft 3 drives the first gear 7 to rotate.Described fixed bar 8 arranges fixed block 9 and bearing 10 away from one end of shaft 3, and the inner of described bearing 10 is fixed on fixed block 9, uses steady pin to fix.The outer end of described bearing 10 is fixedly installed the second gear 11, steady pin is used the first half of the inner of the outer end of bearing 10 and the second gear 11 or the latter half to be fixed, the first half being positioned at the inner of bearing 10 on the upside of shaft 3 and the second gear 11 is fixed, and the latter half being positioned at the inner of bearing 10 on the downside of shaft 3 and the second gear 11 is fixed.Described second gear 11 engages with the first gear 7, and the first gear 7 drives the second gear 11 to rotate, and due to the effect of bearing 10, fixed bar 8 can not be rotated, and fixed bar 8 can play the effect of support second gear 11.Arrange fixed axis 12 between two the second gears 11, described fixed axis 12 is fixedly connected with the inner of the second gear 11, uses steady pin the latter half of the outer end of fixed axis 12 and the inner of the second gear 11 or the first half to be fixedly connected with.The top of fixed axis 12 is fixedly connected with the latter half of the inner of the second gear 11 be positioned on the upside of shaft 3, and the bottom of fixed axis 12 is fixedly connected with the first half of the inner of the second gear 11 be positioned on the downside of shaft 3.Described fixed axis 12 arranges stirring vane 13, and stirring vane 13 and paddle 4 be not in same level.Described shaft 3 stretches out from the top of container cover 2, the top of described container cover 2 is provided with drive motors 14, and described drive motors 14 is connected with shaft 3, drives shaft 3 to rotate by drive motors 14, thus drive paddle 4 and the first gear 7 to rotate, realize the effect of stirring.The top of described container cover 2 is provided with charging aperture 15, water filling port 16, vacuum orifice 17 and exhaust outlet 18, the bottom of described reaction vessel 1 is provided with discharging opening 19, reacted product can discharge reaction vessel 1 by discharging opening 19, and bottom is that arcuate structure can make discharge the most complete.The inside of described reaction vessel 1 arranges zone of heating 20, electrical heating elements is provided with in described zone of heating 20, electrical heating elements is resistance wire, the outer setting cooling water pipe channel layer 21 of described reaction vessel 1, the downside of described cooling water pipe channel layer 21 is provided with cooling water inlet 22, the upside of described cooling water pipe channel layer 21 is provided with coolant outlet 23, cooling water enters in cooling water pipe channel layer 21 by cooling water inlet 22, reaction vessel 1 is lowered the temperature, then through coolant outlet 23, the water playing effect is discharged.The inside set temperature sensor 24 of described reaction vessel 1, the outer setting temperature controller 25 of described cooling water pipe channel layer 21, described temperature controller 25 is connected with temperature sensor 24, by the temperature of temperature sensor 24 detection reaction container 1 inside, feed back to temperature controller 24, the heating state of electrical heating elements and the current intelligence of cooling water is regulated and controled, to control temperature required in reaction vessel 1 by temperature controller 24.
When using the utility model, drive shaft 3 to rotate by drive motors 14, thus drive paddle 4 and the first gear 7 to rotate, simultaneously because the second gear 11 engages with the first gear 7, make the first gear 7 drive the second gear 11 to rotate, realize the effect of stirring.The length of paddle 4 can also being regulated as required, making it adapt to stirring the different experiment having requirement.Stirring dynamics as required, the position of controllable register 6, when needs increase stirring dynamics, moving slider 5 makes it drive baffle plate 6 to move along paddle 4 to the inwall direction of reaction vessel 1, then uses holding screw to be fixed on paddle 4 by slide block 5; When without the need to increasing stirring dynamics, moving slider 5 makes it drive the direction of baffle plate 6 along paddle 4 to shaft 3 to move, and uses holding screw that slide block 5 is fixed on paddle 4 on the position of shaft 3.
Conveniently clear up inside of the present utility model, and do not affect the carrying out of normal experiment, described baffle plate 6 arranges hairbrush 26, and described hairbrush 26 is detachably installed on baffle plate 6, and the replacing of Convenient brush 26 is gone back in the detachable installation of hairbrush 26.
In order to make the connection between container cover 2 and reaction vessel 1 more fastening, certain pressure can be born, being fastenedly connected by bolt 27 between described container cover 2 and reaction vessel 1.
In order to make the better tightness between container cover 2 and reaction vessel 1, between described container cover 2 and reaction vessel 1, be provided with sealing gasket.
In order to make product discharge completely, the bottom of described reaction vessel 1 is arcuate structure.
Embodiment:
Embodiment 1
A kind of chemical synthesizer, comprise reaction vessel 1, the top of described reaction vessel 1 arranges container cover 2, and described container cover 2 seals with reaction vessel 1 and removably connects.The inner vertical of described reaction vessel 1 arranges shaft 3, and described shaft 3 arranges paddle 4, and described paddle 4 is stretching structure.Described paddle 4 is provided with slide block 5, and described slide block 5 slides along paddle 4 length direction.Described slide block 5 arranges baffle plate 6, described baffle plate 6 arranges hairbrush 26, described hairbrush 26 is detachably installed on baffle plate 6.The top and bottom of described shaft 3 are also provided with the first gear 7 and fixed bar 8, and described fixed bar 8 is positioned at the outside of the first gear 7, and the first gear 7 uses steady pin to be installed on shaft 3.Described fixed bar 8 arranges fixed block 9 and bearing 10 away from one end of shaft 3, and the inner of described bearing 10 is fixed on fixed block 9.The outer end of described bearing 10 is fixedly installed the second gear 11, and described second gear 11 engages with the first gear 7.Arrange fixed axis 12 between two the second gears 11, described fixed axis 12 is fixedly connected with the inner of the second gear 11, and described fixed axis 12 arranges stirring vane 13.Described shaft 3 stretches out from the top of container cover 2, and the top of described container cover 2 is provided with drive motors 14, and described drive motors 14 is connected with shaft 3.The top of described container cover 2 is provided with charging aperture 15, water filling port 16, vacuum orifice 17 and exhaust outlet 18, and the bottom of described reaction vessel 1 is provided with discharging opening 19.The inside of described reaction vessel 1 arranges zone of heating 20, is provided with electrical heating elements in described zone of heating 20.The outer setting cooling water pipe channel layer 21 of described reaction vessel 1, the downside of described cooling water pipe channel layer 21 is provided with cooling water inlet 22, and the upside of described cooling water pipe channel layer 21 is provided with coolant outlet 23.The inside set temperature sensor 24 of described reaction vessel 1, the outer setting temperature controller 25 of described cooling water pipe channel layer 21, described temperature controller 25 is connected with temperature sensor 24.The beneficial effect of the present embodiment is: the length adjusting paddle 4 after installing hairbrush 26, makes hairbrush 26 just in time can encounter the inwall of zone of heating 20, facilitate the cleaning of the utility model inside, and detachably easy for installation its of hairbrush 26 is changed.
Embodiment 2
A kind of chemical synthesizer, comprise reaction vessel 1, the bottom of described reaction vessel 1 is arcuate structure.The top of described reaction vessel 1 arranges container cover 2, and described container cover 2 seals with reaction vessel 1 and removably connects, and is fastenedly connected, is provided with sealing gasket between described container cover 2 and reaction vessel 1 between described container cover 2 and reaction vessel 1 by bolt 27.The inner vertical of described reaction vessel 1 arranges shaft 3, and described shaft 3 arranges paddle 4, and described paddle 4 is stretching structure.Described paddle 4 is provided with slide block 5, and described slide block 5 slides along paddle 4 length direction, and described slide block 5 arranges baffle plate 6.The top and bottom of described shaft 3 are also provided with the first gear 7 and fixed bar 8, and described fixed bar 8 is positioned at the outside of the first gear 7, and the first gear 7 uses steady pin to be installed on shaft 3.Described fixed bar 8 arranges fixed block 9 and bearing 10 away from one end of shaft 3, and the inner of described bearing 10 is fixed on fixed block 9, and the outer end of described bearing 10 is fixedly installed the second gear 11, and described second gear 11 engages with the first gear 7.Arrange fixed axis 12 between two the second gears 11, described fixed axis 12 is fixedly connected with the inner of the second gear 11, and described fixed axis 12 arranges stirring vane 13.Described shaft 3 stretches out from the top of container cover 2, and the top of described container cover 2 is provided with drive motors 14, and described drive motors 14 is connected with shaft 3.The top of described container cover 2 is provided with charging aperture 15, water filling port 16, vacuum orifice 17 and exhaust outlet 18, and the bottom of described reaction vessel 1 is provided with discharging opening 19, and the bottom that discharging opening 19 is positioned at reaction vessel 1 is the lowest part of arcuate structure.The inside of described reaction vessel 1 arranges zone of heating 20, is provided with electrical heating elements in described zone of heating 20.The outer setting cooling water pipe channel layer 21 of described reaction vessel 1, the downside of described cooling water pipe channel layer 21 is provided with cooling water inlet 22, and the upside of described cooling water pipe channel layer 21 is provided with coolant outlet 23.The inside set temperature sensor 24 of described reaction vessel 1, the outer setting temperature controller 25 of described cooling water pipe channel layer 21, described temperature controller 25 is connected with temperature sensor 24.The beneficial effect of the present embodiment is: be provided with sealing gasket between container cover 2 and reaction vessel 1 and be fastenedly connected by bolt 27, improves the connection tightness between container cover 2 and reaction vessel 1 and sealing, can bear certain pressure; The bottom of reaction vessel 1 is arcuate structure, and discharge can be made more complete.
Claims (5)
1. a chemical synthesizer, comprise reaction vessel (1), it is characterized in that: the top of described reaction vessel (1) arranges container cover (2), described container cover (2) and reaction vessel (1) seal and removably connect, the inner vertical of described reaction vessel (1) arranges shaft (3), described shaft (3) is arranged paddle (4), described paddle (4) is stretching structure, described paddle (4) is provided with slide block (5), described slide block (5) slides along paddle (4) length direction, described slide block (5) is arranged baffle plate (6), the top and bottom of described shaft (3) are also provided with the first gear (7) and fixed bar (8), described fixed bar (8) is positioned at the outside of the first gear (7), described fixed bar (8) arranges fixed block (9) and bearing (10) away from one end of shaft (3), the inner of described bearing (10) is fixed on fixed block (9), the outer end of described bearing (10) is fixedly installed the second gear (11), described second gear (11) is engaged with the first gear (7), between two the second gears (11), fixed axis (12) is set, described fixed axis (12) is fixedly connected with the inner of the second gear (11), described fixed axis (12) is arranged stirring vane (13), described shaft (3) stretches out from the top of container cover (2), the top of described container cover (2) is provided with drive motors (14), described drive motors (14) is connected with shaft (3), the top of described container cover (2) is provided with charging aperture (15), water filling port (16), vacuum orifice (17) and exhaust outlet (18), the bottom of described reaction vessel (1) is provided with discharging opening (19), the inside of described reaction vessel (1) arranges zone of heating (20), described zone of heating is provided with electrical heating elements in (20), the outer setting cooling water pipe channel layer (21) of described reaction vessel (1), the downside of described cooling water pipe channel layer (21) is provided with cooling water inlet (22), the upside of described cooling water pipe channel layer (21) is provided with coolant outlet (23), inside set temperature sensor (24) of described reaction vessel (1), the outer setting temperature controller (25) of described cooling water pipe channel layer (21), described temperature controller (25) is connected with temperature sensor (24).
2. a kind of chemical synthesizer according to claim 1, is characterized in that: described baffle plate (6) is arranged hairbrush (26), and described hairbrush (26) is detachably installed on baffle plate (6).
3. a kind of chemical synthesizer according to claim 1, is characterized in that: be fastenedly connected by bolt (27) between described container cover (2) and reaction vessel (1).
4. a kind of chemical synthesizer according to claim 1, is characterized in that: be provided with sealing gasket between described container cover (2) and reaction vessel (1).
5. a kind of chemical synthesizer according to claim 1, is characterized in that: the bottom of described reaction vessel (1) is arcuate structure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520827423.0U CN205042480U (en) | 2015-10-23 | 2015-10-23 | Chemical synthesis device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520827423.0U CN205042480U (en) | 2015-10-23 | 2015-10-23 | Chemical synthesis device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205042480U true CN205042480U (en) | 2016-02-24 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520827423.0U Expired - Fee Related CN205042480U (en) | 2015-10-23 | 2015-10-23 | Chemical synthesis device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205042480U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107456941A (en) * | 2017-09-20 | 2017-12-12 | 安庆泽远化工有限公司 | A kind of chemical reaction kettle for being easy to temperature adjustment |
| CN108786697A (en) * | 2018-06-08 | 2018-11-13 | 许笑 | A kind of biochemical explanation in middle school prepares auxiliary device with compound proportioning |
-
2015
- 2015-10-23 CN CN201520827423.0U patent/CN205042480U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107456941A (en) * | 2017-09-20 | 2017-12-12 | 安庆泽远化工有限公司 | A kind of chemical reaction kettle for being easy to temperature adjustment |
| CN107456941B (en) * | 2017-09-20 | 2018-09-25 | 安徽省福泰精细化工有限责任公司 | A kind of chemical reaction kettle adjusted convenient for temperature |
| CN108786697A (en) * | 2018-06-08 | 2018-11-13 | 许笑 | A kind of biochemical explanation in middle school prepares auxiliary device with compound proportioning |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160224 Termination date: 20161023 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |