CN204973138U - Alcohol recovery system - Google Patents
Alcohol recovery system Download PDFInfo
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- CN204973138U CN204973138U CN201520401476.6U CN201520401476U CN204973138U CN 204973138 U CN204973138 U CN 204973138U CN 201520401476 U CN201520401476 U CN 201520401476U CN 204973138 U CN204973138 U CN 204973138U
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- chromatogram
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Abstract
The utility model belongs to the technical field of the pharmaceutical equipment technique and specifically relates to an alcohol recovery system is related to, including one -level recovery unit and second grade recovery unit, one -level recovery unit include the one -level liquid storage pot and with the one -level chromatographic column that the one -level liquid storage pot is linked together, the inside of one -level chromatographic column is provided with a plurality of one -level chromatograms and retrieves the board, the one -level chromatogram is retrieved the board and has been plated zirconia layer and yittrium oxide layer, second grade recovery unit include the second grade liquid storage pot and with the second grade chromatographic column that the second grade liquid storage pot is linked together, the inside of second grade chromatographic column is provided with a plurality of second grade chromatograms and retrieves the board, the second grade chromatogram is retrieved the board and has been plated zirconia layer and europia layer, the one -level chromatographic column with the second grade liquid storage pot is linked together. The utility model provides an alcohol recovery system, it is few, highly low to have an equipment occupation space, and fast to the recovery of alcohol, the alcohol proportion of goods damageds are low, and the energy resource consumption rate is low, and the running cost is low to can realize the characteristics of automatic operation.
Description
Technical field
The utility model relates to pharmaceutical equipment technical field, especially relates to a kind of alcohol recovery system.
Background technology
The industries such as pharmacy, food, light industry, chemical industry need to reclaim alcohol usually.For pharmacy, pharmacy corporation uses alcohol in high concentration to purify some effective ingredients in process of production in a large number, and in use alcohol in high concentration can become low-concentration ethanol.For cost-saving, recycling to be carried out to the alcohol after use.Current enterprise still continues to use vacuum absorption method and reclaims alcohol, first low-concentration ethanol is collected, alcohol in high concentration is reclaimed in the mode of rectifying again with rectifying column, whole removal process divides above-mentioned two steps to carry out, but it is high to there are the alcohol proportion of goods damageds in this method, recovery speed is slow, the problems such as energy consumption is high, and device height is too high, installation environment is limited.
Because the alcohol proportion of goods damageds are up to about 25%, enterprise must spend high capital to purchase alcohol and supplement, and the loss of annual pharmaceutical industry alcohol is up to more than 20,000,000,000 yuan; Because rectifying column way of recycling will add thermal distillation repeatedly to the alcohol after use, reclaim speed very slow, enterprise has to lay in a large amount of alcohol for the production of turnover; In distillation process, will carry out heating for multiple times to the alcohol after use, this just needs to consume a large amount of coal, electricity, natural gas equal energy source; Rectifying column is up to tens meters in addition, bulky, can only carry out pre-installation at medicament compartment, pretty troublesome when needing to enhance production capacities, and rectifying all becomes the bottleneck that most enterprises improves production capacity; In addition, the process need of alcohol recycle manually carries out, and will use large quantities of technology and operating personnel in production process, operating cost is high.
Utility model content
The purpose of this utility model is to provide a kind of alcohol recovery system, to solve in the alcohol recycle process that exists in prior art, and the technical problem that equipment occupation space is many, alcohol recycle speed slow and the alcohol proportion of goods damageds are high.
The utility model provides a kind of alcohol recovery system, comprises one-level retracting device and secondary recovery device;
The one-level chromatographic column that described one-level retracting device comprises one-level fluid reservoir and is connected with described one-level fluid reservoir, the inside of described one-level chromatographic column is provided with multiple one-level chromatogram and reclaims plate, and described one-level chromatogram reclaims plate and is coated with zirconia layer and yttrium oxide layer;
The secondary chromatographic column that described secondary recovery device comprises secondary fluid reservoir and is connected with described secondary fluid reservoir, the inside of described secondary chromatographic column is provided with multiple secondary chromatogram and reclaims plate, and described secondary chromatogram reclaims plate and is coated with zirconia layer and europium oxide layer;
Described one-level chromatographic column is connected with described secondary fluid reservoir.
Further, also comprise heater and gathering-device, described heater is connected with described one-level fluid reservoir; Described gathering-device is connected with described secondary chromatographic column.
Further, it is layered distribution that multiple described one-level chromatogram reclaims plate, and each described one-level chromatogram recovery plate is provided with multiple through hole;
It is layered distribution that multiple described secondary chromatogram reclaims plate, and each described secondary chromatogram recovery plate is provided with multiple through hole.
Further, described one-level chromatographic column is arranged on the top of described one-level fluid reservoir;
Described one-level retracting device is provided with primary cycle pump, for by the top of the Liquid transfer in described one-level fluid reservoir to described one-level chromatographic column.
Further, described secondary chromatographic column is arranged on the top of described secondary fluid reservoir;
Described secondary recovery device is provided with secondary cycle pump, for by the top of the Liquid transfer in described secondary fluid reservoir to described secondary chromatographic column.
Further, the top of described one-level chromatographic column is provided with condenser, and described condenser is connected with condensation cycle pump.
Further, the top of described secondary chromatographic column is provided with at least one condenser, and described condenser is connected with condensation cycle pump; Described secondary chromatographic column is also provided with at least one heat exchanger.
Further, described one-level chromatographic column and described secondary chromatographic column are provided with temperature sensor;
Described one-level chromatographic column and described secondary chromatographic column are provided with pressure sensor.
Further, also comprise controller, described controller is electrically connected with described temperature sensor, described pressure sensor respectively.
Further, described gathering-device comprises the condensation column at the top of collecting flow container and being arranged on described collection flow container, and described condensation column is provided with condenser; Described condensation column is connected with described secondary chromatographic column.
Compared with prior art, the beneficial effects of the utility model are:
The alcohol recovery system that the utility model provides, utilize chromatographic principles to reclaim on plate in one-level chromatogram and plate zirconia layer and yttrium oxide layer, reclaim on plate in secondary chromatogram and plate zirconia layer and europium oxide layer, when gaseous state alcohol molecule and gaseous state stream of water molecule reclaim plate through one-level chromatogram, when secondary chromatogram reclaims plate, gaseous state alcohol molecule can be quickly through, and the flowing of vaporous water molecule is very slow, and slowly enrichment, now pass through condensation, even if vaporous water molecule is liquefied, due to Action of Gravity Field, liquefaction water flow is in one-level fluid reservoir and secondary fluid reservoir, and enrichment gradually, thus a step can reclaim out alcohol in high concentration from low-concentration ethanol solution.The alcohol recovery system that the utility model provides, has equipment occupation space few, highly low, and fast to the recovery speed of alcohol, the alcohol proportion of goods damageds are low, and energy resource consumption rate is low, and operating cost is low, and can realize the feature of automatic operating.
Accompanying drawing explanation
In order to be illustrated more clearly in the utility model detailed description of the invention or technical scheme of the prior art, be briefly described to the accompanying drawing used required in detailed description of the invention or description of the prior art below, apparently, accompanying drawing in the following describes is embodiments more of the present utility model, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to these accompanying drawings.
The structural representation of the alcohol recovery system provided that Fig. 1 is the utility model embodiment.
Reference numeral:
101-one-level fluid reservoir; 102-one-level chromatographic column; 103-secondary fluid reservoir;
104-secondary chromatographic column; 105-pressure sensor; 106-heater;
107-temperature sensor; 108-flowmeter; 109-primary cycle pump;
110-first valve; 111-sewage draining valve; 112-secondary cycle pump;
113-second valve; 114-the 3rd valve; 115-condenser;
116-condensation cycle pump; 117-heat exchanger; 118-pressure reduction liquid level gauge;
119-collects flow container; 120-condensation column; 121-collecting pump;
122-the 4th valve.
Detailed description of the invention
Be clearly and completely described the technical solution of the utility model below in conjunction with accompanying drawing, obviously, described embodiment is the utility model part embodiment, instead of whole embodiments.
Based on the embodiment in the utility model, those of ordinary skill in the art are not making the every other embodiment obtained under creative work prerequisite, all belong to the scope of the utility model protection.
In description of the present utility model, it should be noted that, orientation or the position relationship of the instruction such as term " " center ", " on ", D score, "left", "right", " vertically ", " level ", " interior ", " outward " they be based on orientation shown in the drawings or position relationship; be only the utility model and simplified characterization for convenience of description; instead of instruction or imply the device of indication or element must have specific orientation, with specific azimuth configuration and operation, therefore can not be interpreted as restriction of the present utility model.In addition, term " first ", " second ", " the 3rd " only for describing object, and can not be interpreted as instruction or hint relative importance.
In description of the present utility model, it should be noted that, unless otherwise clearly defined and limited, term " installation ", " being connected ", " connection " should be interpreted broadly, and such as, can be fixedly connected with, also can be removably connect, or connect integratedly; Can be mechanical connection, also can be electrical connection; Can be directly be connected, also indirectly can be connected by intermediary, can be the connection of two element internals.For the ordinary skill in the art, concrete condition the concrete meaning of above-mentioned term in the utility model can be understood.
Embodiment
The structural representation of the alcohol recovery system provided that Fig. 1 is the utility model embodiment, shown in Figure 1, present embodiments provide a kind of alcohol recovery system, comprise one-level retracting device and secondary recovery device; The one-level chromatographic column 102 that one-level retracting device comprises one-level fluid reservoir 101 and is connected with one-level fluid reservoir 101, the inside of one-level chromatographic column 102 is provided with multiple one-level chromatogram and reclaims plate (not shown), and one-level chromatogram reclaims plate and is coated with zirconia layer and yttrium oxide layer; The secondary chromatographic column 104 that secondary recovery device comprises secondary fluid reservoir 103 and is connected with secondary fluid reservoir 103, the inside of secondary chromatographic column 104 is provided with multiple secondary chromatogram and reclaims plate (not shown), and secondary chromatogram reclaims plate and is coated with zirconia layer and europium oxide layer; One-level chromatographic column 102 is connected with secondary fluid reservoir 103, and one-level chromatographic column 102 and secondary fluid reservoir 103 are by pipeline communication specifically, and this pipeline is provided with pressure sensor 105.The alcohol recovery system that the utility model provides, utilize chromatographic principles to reclaim on plate in one-level chromatogram and plate zirconia layer and yttrium oxide layer, reclaim on plate in secondary chromatogram and plate zirconia layer and europium oxide layer, when gaseous state alcohol molecule and gaseous state stream of water molecule reclaim plate through one-level chromatogram, when secondary chromatogram reclaims plate, gaseous state alcohol molecule can be quickly through, and the flowing of vaporous water molecule is very slow, and slowly enrichment, now pass through condensation, even if vaporous water molecule is liquefied, due to Action of Gravity Field, liquefaction water flow is in one-level fluid reservoir 101 and secondary fluid reservoir 103, and enrichment gradually, thus a step can reclaim out alcohol in high concentration from low-concentration ethanol solution.The alcohol recovery system that the utility model provides, has equipment occupation space few, highly low, and fast to the recovery speed of alcohol, the alcohol proportion of goods damageds are low, and energy resource consumption rate is low, and operating cost is low, and can realize the feature of automatic operating.
It should be noted that, in the present embodiment, one-level chromatogram reclaims plate and secondary chromatogram reclaims the oxide layer can with selective absorption that plate can also plate other.
In the present embodiment, alcohol recovery system also comprises heater 106 and gathering-device; Heater 106 is connected with one-level fluid reservoir 101, and specifically, heater 106 and one-level fluid reservoir 101 by pipeline communication, and this pipeline are provided with pressure sensor 105, temperature sensor 107 and flowmeter 108; Gathering-device is connected with secondary chromatographic column 104, and specifically, gathering-device and secondary chromatographic column 104 by pipeline communication, and this pipeline are provided with pressure sensor 105.During work, the mode of heating of heater 106 pairs of low-concentration ethanols is jacket steam heating.
In the present embodiment, it is layered distribution that multiple one-level chromatogram reclaims plate, and each one-level chromatogram recovery plate is provided with multiple through hole; It is layered distribution that multiple secondary chromatogram reclaims plate, and each secondary chromatogram recovery plate is provided with multiple through hole.Specifically, one-level chromatogram reclaims the material that plate and secondary chromatogram reclaim plate and is stainless steel, and what one-level chromatogram reclaimed that plate and secondary chromatogram reclaim the plate face of plate is oriented above-below direction, and during work, according to the principle that hot gas rises, steam is upwards flowed by through hole.It should be noted that, in the present embodiment, one-level chromatogram reclaims the quantity of plate and secondary chromatogram recovery plate, can determine, be provided with quantity more according to the situation of reality, better to the recovering effect of alcohol; The size and shape of through hole also can be determined according to situation about realizing in addition, such as, the aperture of through hole can be 1.5mm ~ 32mm, and the shape of through hole can be circular, oval, square etc., when through hole is non-circular through hole, aperture refers to the maximum of any distance between two points on through hole.
In the present embodiment, one-level chromatographic column 102 is arranged on the top of one-level fluid reservoir 101; One-level retracting device is provided with primary cycle pump 109, for by the top of the Liquid transfer in one-level fluid reservoir 101 to one-level chromatographic column 102.Specifically, primary cycle pump 109 is connected with the bottom of one-level fluid reservoir 101, the top of one-level chromatographic column 102 respectively by pipeline, wherein, the install pipeline be connected between primary cycle pump 109 and the top of one-level chromatographic column 102 has the first valve 110, and primary cycle pump 109 is also communicated with sewage draining valve 111.
In the present embodiment, secondary chromatographic column 104 is arranged on the top of secondary fluid reservoir 103; Secondary recovery device is provided with secondary cycle pump 112, for by the top of the Liquid transfer in secondary fluid reservoir 103 to secondary chromatographic column 104.Specifically, secondary cycle pump 112 is connected with the bottom of secondary fluid reservoir 103, the top of secondary chromatographic column 104 respectively by pipeline, wherein, the install pipeline be connected between secondary cycle pump 112 and the top of secondary chromatographic column 104 has the second valve 113, and secondary cycle pump 112 is also communicated with sewage draining valve 111; The 3rd valve 114 is also communicated with between first valve 110 and the second valve 113, by the cooperation of the first valve 110, second valve 113 and the 3rd valve 114, can by the top of the Liquid transfer one-level chromatographic column 102 of secondary fluid reservoir 103, can reduce like this and reduce the alcohol proportion of goods damageds, improve the rate of recovery of alcohol further.
In the present embodiment, the top of one-level chromatographic column 102 is provided with condenser 115, and condenser 115 is connected with condensation cycle pump 116.By the cooperation of condenser 115 and condensation cycle pump 116, the heat discharged during to take away steam liquefied in one-level chromatographic column 102.
In the present embodiment, the top of secondary chromatographic column 104 is provided with at least one condenser 115, condenser 115 is connected with condensation cycle pump 116, the quantity of condenser 115 is 5 specifically, by the cooperation of condenser 115 and condensation cycle pump 116, the heat discharged during to take away steam liquefied in secondary chromatographic column 104; Secondary chromatographic column 104 is also provided with at least one heat exchanger 117, specifically in the present embodiment, the quantity of heat exchanger 117 is 4, can be heated or condensation by heat exchanger to secondary chromatographic column 104, to ensure temperature best in secondary chromatographic column 104; 5 condensers 115 and 4 heat exchangers 117 are spaced is arranged in secondary chromatographic column 104.It should be noted that, the condensation cycle pump 116 in Fig. 1 in secondary chromatographic column 104 merely illustrates one.
In the present embodiment, one-level chromatographic column 102 and secondary chromatographic column 104 are provided with temperature sensor 107; One-level chromatographic column 102 and secondary chromatographic column 104 are provided with pressure sensor 105, wherein the quantity of temperature sensor 107 can be arranged on the diverse location in one-level chromatographic column 102 and secondary chromatographic column 104 as required, to monitor the temperature of the inside diverse location of one-level chromatographic column 102 and secondary chromatographic column 104.
In the present embodiment, alcohol recovery system also comprises controller (not shown), and controller is electrically connected with temperature sensor 107, pressure sensor 105 respectively.Controller can be computer or PLC.
In the present embodiment, gathering-device comprises the condensation column 120 collected flow container 119 and be arranged on the top of collecting flow container 119, and condensation column 120 is provided with condenser 115; Condensation column 120 is connected with secondary chromatographic column 104.The bottom of collecting flow container 119 is communicated with collecting pump 121, the 4th valve 122 and flowmeter 108 successively by pipeline.It should be noted that, in the present embodiment, vavuum pump can be set at the top of condensation column 120, to ensure the quality reclaiming the alcohol obtained further.
In the present embodiment, one-level fluid reservoir 101 and secondary fluid reservoir 103 are also provided with pressure reduction liquid level gauge 118, are measured the height of pot liquid by pressure reduction liquid level gauge 118, when liquid exceeds setting value, by opening sewage draining valve 111 with discharge liquid.
In the present embodiment, the first valve 110, second valve 113, the 3rd valve 114, the 4th valve 122 and sewage draining valve 111 are magnetic valve.
In the present embodiment, condenser 115 is shell and tube condenser, and heat exchanger 117 is interlayer heat exchanger.It should be noted that in the present embodiment, the particular type of condenser 115, heat exchanger 117 also freely can be chosen according to actual conditions.
In the present embodiment, controller is also electrically connected with the first valve 110, second valve 113, the 3rd valve 114, the 4th valve 122, sewage draining valve 111, condensation cycle pump 116, primary cycle pump 109, secondary cycle pump 112, collecting pump 121, flowmeter 108, by controller to realize the Automated condtrol to this alcohol recovery system.Controller can control heat exchanger makes it heat or condensation secondary chromatographic column 104.
In sum, the alcohol recovery system that the present embodiment provides can realize Automated condtrol, and simple to operate, also has that floor space is little, energy resource consumption rate is low, high and reclaim the good feature of the alcohol quality that obtains to the rate of recovery of alcohol.
Last it is noted that above each embodiment is only in order to illustrate the technical solution of the utility model, be not intended to limit; Although be described in detail the utility model with reference to foregoing embodiments, those of ordinary skill in the art is to be understood that: it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein some or all of technical characteristic; And these amendments or replacement, do not make the essence of appropriate technical solution depart from the scope of each embodiment technical scheme of the utility model.
Claims (10)
1. an alcohol recovery system, is characterized in that, comprises one-level retracting device and secondary recovery device;
The one-level chromatographic column that described one-level retracting device comprises one-level fluid reservoir and is connected with described one-level fluid reservoir, the inside of described one-level chromatographic column is provided with multiple one-level chromatogram and reclaims plate, and described one-level chromatogram reclaims plate and is coated with zirconia layer and yttrium oxide layer;
The secondary chromatographic column that described secondary recovery device comprises secondary fluid reservoir and is connected with described secondary fluid reservoir, the inside of described secondary chromatographic column is provided with multiple secondary chromatogram and reclaims plate, and described secondary chromatogram reclaims plate and is coated with zirconia layer and europium oxide layer;
Described one-level chromatographic column is connected with described secondary fluid reservoir.
2. alcohol recovery system according to claim 1, is characterized in that, also comprises heater and gathering-device, and described heater is connected with described one-level fluid reservoir; Described gathering-device is connected with described secondary chromatographic column.
3. alcohol recovery system according to claim 1 and 2, is characterized in that, it is layered distribution that multiple described one-level chromatogram reclaims plate, and each described one-level chromatogram recovery plate is provided with multiple through hole;
It is layered distribution that multiple described secondary chromatogram reclaims plate, and each described secondary chromatogram recovery plate is provided with multiple through hole.
4. alcohol recovery system according to claim 1 and 2, is characterized in that, described one-level chromatographic column is arranged on the top of described one-level fluid reservoir;
Described one-level retracting device is provided with primary cycle pump, for by the top of the Liquid transfer in described one-level fluid reservoir to described one-level chromatographic column.
5. alcohol recovery system according to claim 1 and 2, is characterized in that, described secondary chromatographic column is arranged on the top of described secondary fluid reservoir;
Described secondary recovery device is provided with secondary cycle pump, for by the top of the Liquid transfer in described secondary fluid reservoir to described secondary chromatographic column.
6. alcohol recovery system according to claim 1 and 2, is characterized in that, the top of described one-level chromatographic column is provided with condenser, and described condenser is connected with condensation cycle pump.
7. alcohol recovery system according to claim 1 and 2, is characterized in that, the top of described secondary chromatographic column is provided with at least one condenser, and described condenser is connected with condensation cycle pump; Described secondary chromatographic column is also provided with at least one heat exchanger.
8. alcohol recovery system according to claim 1 and 2, is characterized in that, described one-level chromatographic column and described secondary chromatographic column are provided with temperature sensor;
Described one-level chromatographic column and described secondary chromatographic column are provided with pressure sensor.
9. alcohol recovery system according to claim 8, is characterized in that, also comprises controller, and described controller is electrically connected with described temperature sensor, described pressure sensor respectively.
10. alcohol recovery system according to claim 2, is characterized in that, described gathering-device comprises the condensation column at the top of collecting flow container and being arranged on described collection flow container, and described condensation column is provided with condenser; Described condensation column is connected with described secondary chromatographic column.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520401476.6U CN204973138U (en) | 2015-06-11 | 2015-06-11 | Alcohol recovery system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520401476.6U CN204973138U (en) | 2015-06-11 | 2015-06-11 | Alcohol recovery system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204973138U true CN204973138U (en) | 2016-01-20 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520401476.6U Withdrawn - After Issue CN204973138U (en) | 2015-06-11 | 2015-06-11 | Alcohol recovery system |
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| Country | Link |
|---|---|
| CN (1) | CN204973138U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104888494A (en) * | 2015-06-11 | 2015-09-09 | 四川九渊医药科技有限公司 | Alcohol recovery system |
-
2015
- 2015-06-11 CN CN201520401476.6U patent/CN204973138U/en not_active Withdrawn - After Issue
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104888494A (en) * | 2015-06-11 | 2015-09-09 | 四川九渊医药科技有限公司 | Alcohol recovery system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20160120 Effective date of abandoning: 20161019 |
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| C25 | Abandonment of patent right or utility model to avoid double patenting |