CN204523010U - A kind of microwave chemical reaction intensified condenser tube - Google Patents
A kind of microwave chemical reaction intensified condenser tube Download PDFInfo
- Publication number
- CN204523010U CN204523010U CN201520184886.XU CN201520184886U CN204523010U CN 204523010 U CN204523010 U CN 204523010U CN 201520184886 U CN201520184886 U CN 201520184886U CN 204523010 U CN204523010 U CN 204523010U
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- China
- Prior art keywords
- pipe
- bulb
- tube
- adjusting knob
- end ground
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- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 14
- 230000003139 buffering effect Effects 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000007921 spray Substances 0.000 abstract description 8
- 238000012360 testing method Methods 0.000 abstract description 7
- 230000004907 flux Effects 0.000 abstract description 5
- 238000010992 reflux Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 description 7
- 239000007788 liquid Substances 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 241000168254 Siro Species 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
The utility model discloses a kind of microwave chemical reaction intensified condenser tube, mainly comprise outer layer sleeve, buffering bulb tube, series connection spheric bulb pipe and pressure regulator.Wherein, the internal diameter of internal diameter much larger than spheric bulb in series connection spheric bulb pipe of bulb tube is cushioned; Pressure regulator comprises gim peg, adjusting knob and spring, and adjusting knob and gim peg are threaded connection, and the bottom of spring and adjusting knob is affixed.The diameter of buffering bulb tube is large, when the quick-fried spray of flux, cushion spherical pipe and there is enough cushion spaces, effectively can reduce the effect that effluxvelocity also tentatively realizes condensing reflux, the quick-fried spray phenomenon of effective control, the accuracy of guarantee test result and the personal safety of testing crew; The utility model internal pressure can carry out timely regulation and control by spring, avoids internal pressure excessive and condenser pipe is broken.Therefore the utility model safe and efficient, reasonable in design, be easy to realize.
Description
Technical field
The present invention relates to a kind of chemical industry experimental rig, particularly relate to a kind of intensified condenser tube be applied in heating using microwave chemical reaction.
Background technology
Microwave heating technique has that firing rate is fast, homogeneous heating, Heating selectivity strong and efficiency of heating surface high, and it obtains increasingly extensive application in fields such as chemistry, material, environment.In heating using microwave test, need configuration condenser pipe to accelerate the liquefaction of evaporate.Traditional condenser pipe is made up of simple inner and outer tubes, makes the cooling of the gas in interior pipe and liquefaction becomes liquid by the cooling water between inner and outer tubes.For the microwave reaction that the rate of heat addition is fast, added hot solvent and easily occurred superheating phenomenon and the quick-fried spray causing flux, flux is caused externally to spread, if use traditional condenser pipe, because traditional condensation duct is limited, the solvent of quick-fried spray cannot within it be cushioned and brute force attack condenser pipe, condenser pipe is separated with Heated container, this not only can have a strong impact on the accuracy of result of the test, the more important thing is and easily causes security incident, and it is unfavorable to cause testing crew.
Summary of the invention
The utility model object is to provide and is a kind ofly applicable to microwave chemical reaction, can effectively prevent from reacting the quick-fried spray of flux and the microwave chemical reaction intensified condenser tube accelerating steam condensing reflux.
The purpose of this utility model can reach by the following technical programs: a kind of microwave chemical reaction intensified condenser tube, comprises outer layer sleeve, buffering bulb tube, series connection spheric bulb pipe, water inlet pipe, outlet pipe, lower end ground, upper end ground, rubber stopper and pressure regulator.Wherein, water inlet pipe and outlet pipe lay respectively at lower end and the upper end of outer layer sleeve; The internal diameter of buffering bulb tube is much larger than the internal diameter of spheric bulb in series connection spheric bulb pipe, and the top of buffering bulb tube and bottom are communicated with connect spheric bulb pipe and lower end ground respectively, and upper end ground is communicated with the top of spheric bulb pipe of connecting; Rubber stopper plug is in the ground of upper end, and the bottom of pressure regulator is fixedly connected with the top of upper end ground.
Pressure regulator comprises gim peg, adjusting knob and spring, and adjusting knob and gim peg are threaded connection, and the bottom of spring and adjusting knob is affixed.
The diameter of buffering bulb tube of the present utility model is large, when the quick-fried spray of flux, cushion spherical pipe and there is enough cushion spaces, effectively can reduce the effect that effluxvelocity also tentatively realizes condensing reflux, the quick-fried spray phenomenon of effective control, the accuracy of guarantee test result and the personal safety of testing crew; The utility model internal pressure can carry out timely regulation and control by spring, avoids internal pressure excessive and condenser pipe is broken.Therefore the utility model safe and efficient, reasonable in design, be easy to realize.
Accompanying drawing explanation
Fig. 1 is general structure schematic diagram of the present utility model;
Fig. 2 is the pressure regulator schematic diagram of the utility model.
Drawing illustrates: 1. outer layer sleeve 2. cushions bulb tube 3. soccer star that connects and steeps ground 7. upper end, pipe 4. water inlet pipe 5. outlet pipe 6. lower end ground 8. rubber stopper 9. pressure regulator 10. gim peg 11. adjusting knob 12. spring.
Detailed description of the invention
With reference to accompanying drawing 1, a kind of microwave chemical reaction intensified condenser tube, comprise outer layer sleeve 1, buffering bulb tube 2, series connection spheric bulb pipe 3, water inlet pipe 4, outlet pipe 5, lower end ground 6, upper end ground 7, rubber stopper 8 and pressure regulator 9.Wherein: water inlet pipe 4 and outlet pipe 5 lay respectively at lower end and the upper end of outer layer sleeve 1; The internal diameter of buffering bulb tube 2 is much larger than the internal diameter of spheric bulb in series connection spheric bulb pipe 3, and the top of buffering bulb tube 2 and bottom are communicated with connect spheric bulb pipe 3 and lower end ground 6 respectively, and upper end ground 7 is communicated with the top of spheric bulb pipe 3 of connecting; Rubber stopper 8 is filled in upper end ground 7, and the bottom of pressure regulator 9 is fixedly connected with the top of upper end ground 7.
With reference to accompanying drawing 2, pressure regulator 9 comprises gim peg 10, adjusting knob 11 and spring 12, and adjusting knob 11 and gim peg 10 are threaded connection, and spring 12 is affixed with the bottom of adjusting knob 11.
During use, the utility model is connected with reaction vessel by lower end ground 6, rotates adjusting knob 11 and regulates the sealing between rubber stopper 8 and upper end ground 7 to suitable.Cooling water continues to enter at water inlet pipe 4, flows out after being full of outer layer sleeve 1 from outlet pipe 5.When in reaction vessel reached the even quick-fried spray of boiling point by heating liquid time, jet and steam are introduced in buffering bulb tube 2 by lower end ground 6, because buffering bulb tube 2 has enough cushion spaces, liquid jet speed reduces even to eliminate, by realizing preliminary condensing reflux with the heat exchange of outside cold water; When reacting violent, jet and steam can reach in series connection spheric bulb pipe 3, and jet is eliminated by the frictional impact with top rubber plug 8, and steam is further cooling for reflux then.
Because whole reaction system is hedged off from the outer world, the pressure of its inside can constantly raise, when internal pressure reaches higher level, spring 12 in pressure regulator 9 is forced upwardly compression, and rubber stopper 8 weakens with the tightness of upper end ground 7, makes internal pressure obtain part release and reduce, spring 12 now in pressure regulator 9 recompresses rubber stopper 8, make itself and upper end ground 7 compact siro spinning technology realize sealing, internal pressure increases again, so repeatedly works.Compared with general condenser pipe, the utility model can regulate internal pressure in time, safe and reliable.
Claims (2)
1. a microwave chemical reaction intensified condenser tube, comprise outer layer sleeve (1), buffering bulb tube (2), series connection spheric bulb pipe (3), water inlet pipe (4), outlet pipe (5), lower end ground (6), upper end ground (7), rubber stopper (8) and pressure regulator (9), it is characterized in that: water inlet pipe (4) and outlet pipe (5) lay respectively at lower end and the upper end of outer layer sleeve (1); Cushion the internal diameter of internal diameter much larger than spheric bulb in series connection spheric bulb pipe (3) of bulb tube (2), top and the bottom of buffering bulb tube (2) are communicated with connect spheric bulb pipe (3) and lower end ground (6) respectively, and upper end ground (7) is communicated with the top of spheric bulb pipe (3) of connecting; Rubber stopper (8) is filled in upper end ground (7), and the bottom of pressure regulator (9) is fixedly connected with the top of upper end ground (7).
2. a kind of microwave chemical reaction intensified condenser tube according to claim 1, it is characterized in that: described pressure regulator (9) is made up of gim peg (10), adjusting knob (11) and spring (12), adjusting knob (11) and gim peg (10) are threaded connection, and spring (12) is affixed with the bottom of adjusting knob (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520184886.XU CN204523010U (en) | 2015-03-31 | 2015-03-31 | A kind of microwave chemical reaction intensified condenser tube |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520184886.XU CN204523010U (en) | 2015-03-31 | 2015-03-31 | A kind of microwave chemical reaction intensified condenser tube |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204523010U true CN204523010U (en) | 2015-08-05 |
Family
ID=53737065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520184886.XU Expired - Fee Related CN204523010U (en) | 2015-03-31 | 2015-03-31 | A kind of microwave chemical reaction intensified condenser tube |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204523010U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109908855A (en) * | 2019-03-04 | 2019-06-21 | 枣庄学院 | A kind of explosion-protection equipment and its application method extracted for plant proline with the processing of assay boiling water bath |
| CN111558233A (en) * | 2020-05-22 | 2020-08-21 | 青海省药品检验检测院 | Splash-proof device that backward flow was drawed |
-
2015
- 2015-03-31 CN CN201520184886.XU patent/CN204523010U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109908855A (en) * | 2019-03-04 | 2019-06-21 | 枣庄学院 | A kind of explosion-protection equipment and its application method extracted for plant proline with the processing of assay boiling water bath |
| CN109908855B (en) * | 2019-03-04 | 2021-04-23 | 枣庄学院 | Explosion-proof device for plant proline extraction and content determination boiling water bath treatment and use method thereof |
| CN111558233A (en) * | 2020-05-22 | 2020-08-21 | 青海省药品检验检测院 | Splash-proof device that backward flow was drawed |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150805 Termination date: 20160331 |