CN204502555U - Equipment for separating liquid from solid - Google Patents
Equipment for separating liquid from solid Download PDFInfo
- Publication number
- CN204502555U CN204502555U CN201520125314.4U CN201520125314U CN204502555U CN 204502555 U CN204502555 U CN 204502555U CN 201520125314 U CN201520125314 U CN 201520125314U CN 204502555 U CN204502555 U CN 204502555U
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- vapor tight
- tight tank
- rotating shaft
- pipeline
- liquid
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Abstract
The utility model discloses a kind of equipment for separating liquid from solid, relate to chemical reactant equipment for separating liquid from solid technical field.Device comprises vapor tight tank, and vapor tight tank top is provided with charge door, and interior middle and lower part is provided with filter course, and outside is provided with rotating shaft, and rotating shaft is that hollow shaft is connected with power turnover device; Be connected with air compressor machine by rotating shaft, air compression pipeline above vapor tight tank inner filtration layer; Be provided with tapping valve and Drainage pipe bottom vapor tight tank, another termination gas-liquid separator of Drainage pipe, gas-liquid separator top is connected with vavuum pump by vacuum pipe, is provided with tap hole bottom gas-liquid separator; Connected by pipeline between pneumatics and Drainage pipe, pipeline, Drainage pipe and air compression pipeline are respectively equipped with valve, feed liquor and pneumatics valve.This device good effect of separating solid from liquid, production efficiency is high; Use this device to produce hopcalite agent cost low, with short production cycle, and can reclaim sulfuric acid potassium and sodium sulphate be distinguished, potassium sulfate and sodium sulphate can be recycled.
Description
Technical field
The utility model relates to chemical reactant equipment for separating liquid from solid technical field.
Background technology
Hopcalite agent is a kind of catalyst prod of filtering carbon monoxide, and its main component is the mixture of manganese oxide and cupric oxide.Generated by chemical reaction, produce simultaneously with the sulfate ion such as sodium sulphate, potassium sulfate, it is a kind of material harmful to hopcalite agent product, needs from hopcalite agent, remove sulfate ion and just can produce qualified hopcalite agent.
Hopcalite agent is a kind of solid, is not dissolved in water, and sulfate ion is soluble in water, and the production technology device of traditional hopcalite agent as shown in Figure 2, comprises the following steps: 1, Jiang Shui adds reactor, adds the concentrated sulfuric acid, as the medium solution of reaction; 2, in reactor, add manganese sulfate, dissolve; Add potassium permanganate reaction, generate manganese dioxide (active ingredient), and potassium sulfate (useless material), there is dilute sulfuric acid to exist simultaneously; 3, in reactor, add copper sulphate dissolves, then add soda ash, generate basic copper carbonate (active ingredient) and sodium sulphate (useless material); 4, reactant liquor is imported washing tank, utilize active ingredient water insoluble, the characteristic that useless material is water-soluble, add water, dilute sulphuric acid radical ion; 5, staticly settled through about 8 hours, active ingredient is deposited in bottom washing tank, is discharged by the liquid of the sulphate-containing ion on washing tank top; And again add water, repeat 6 ~ 8 times washings, until there is no sulfate ion.6, centrifuge will be imported containing more juicy reactant liquor, dehydration; 7, the reactant containing less moisture is put into oven drying, slough all moisture, the hopcalite agent semi-finished product being needs (also need granulation and activation below; During activation, basic copper carbonate pyrolytic is carbon dioxide and cupric oxide).There is following shortcoming in the production technology of traditional hopcalite agent: the sulfate ion of 1, discharging is the mixture of potassium sulfate and sodium sulphate, can not recycle; 2, production cost is high, the use amount of soda ash large (process generating basic copper carbonate will use a large amount of soda ash, in coming and dilute sulfuric acid, makes it to change into sodium sulphate); 3, production efficiency is low, and general needs just can complete for 8 days.
Utility model content
The technical problems to be solved in the utility model is to provide a kind of equipment for separating liquid from solid, and this apparatus structure is reasonable, good effect of separating solid from liquid, and production efficiency is high; Use this device to produce hopcalite agent cost low, with short production cycle, and can reclaim sulfuric acid potassium and sodium sulphate be distinguished, potassium sulfate and sodium sulphate can be recycled.
For solving the problems of the technologies described above, technical solution adopted in the utility model is: a kind of equipment for separating liquid from solid, comprises vapor tight tank, air compressor machine, vavuum pump and gas-liquid separator;
The top of vapor tight tank is provided with charge door, and also make discharging opening, in vapor tight tank, middle and lower part is provided with filter course simultaneously;
Be provided with rotating shaft outside vapor tight tank, rotating shaft is connected with vapor tight tank power turnover device; Rotating shaft is hollow shaft, is connected above vapor tight tank inner filtration layer by rotating shaft, air compression pipeline with air compressor machine;
Be provided with tapping valve and Drainage pipe bottom vapor tight tank, another termination gas-liquid separator of Drainage pipe, gas-liquid separator top is connected with vavuum pump by vacuum pipe, is provided with tap hole bottom gas-liquid separator;
Connected by pipeline between air compression pipeline and Drainage pipe, pipeline, Drainage pipe and air compression pipeline are respectively equipped with valve, liquid feed valve and pneumatics valve.
Preferably, charging valve and snap joint is provided with at the charge door at vapor tight tank top; Tapping valve place bottom vapor tight tank is provided with snap joint.
Preferably, interlayer, heating fluid inlet ductwork and heating fluid export pipeline is provided with outside vapor tight tank.
Preferably, be provided with vapor tight tank support outside vapor tight tank, vapor tight tank support is connected with the axis of rotation of vapor tight tank by the vapor tight tank left and right sides; Side rotating shaft connects air compression pipeline, and opposite side rotating shaft connects heating fluid inlet ductwork and heating fluid export pipeline.
When the utility model equipment for separating liquid from solid uses: chemical reactant is placed in above vapor tight tank inner filtration layer, normal pressure is applied to above vapor tight tank filter course, or apply negative pressure in the below of filter course, or apply below normal pressure, to apply these three kinds of modes of negative pressure above filter course simultaneously, make chemical reactant solid be filtered layer stop and stay on filter course, liquid is subject to pressure action, is separated with solid through filter course.
The utility model vapor tight tank power turnover device is conventional power turnover device, as: motor reducer.
The beneficial effect adopting technique scheme to produce is:
(1) this apparatus structure is reasonable, and Separation of Solid and Liquid adopts pressure mode, and principal mode has 1. malleation; 2. negative pressure; 3. comprehensive, malleation+negative pressure; This device can also realize simultaneously, upset; The functions such as heating, insulation.This device can be applied in other chemical reactions, realizes Separation of Solid and Liquid, drying, pulverizing.
(2) use this device to produce hopcalite agent cost low, production efficiency is high, the technique that past 8 days completed, and improves and completes for latter 2 days, also mitigate labour intensity simultaneously.
(3) use this device production hopcalite agent can reclaim fluid sulphuric acid potassium and the sodium sulphate of high concentration respectively, potassium sulfate and sodium sulphate can be recycled.
(4) use this device to produce hopcalite agent and improve the effect being separated sulfate ion in hopcalite agent, improve the purity of hopcalite agent product.
(5) use this device to produce hopcalite agent and saved water, wash can to reach for 2-4 time in hopcalite agent sulfate ion residual quantity ten thousand/below, avoid the waste of water.
Accompanying drawing explanation
Below in conjunction with the drawings and specific embodiments, the utility model is described in further detail;
Fig. 1 is the structural representation of equipment for separating liquid from solid of the present utility model;
Fig. 2 is the production technology device schematic diagram of traditional hopcalite agent;
In figure: 1, charge door; 2, vapor tight tank; 3, rotating shaft; 4, heating fluid inlet ductwork; 5, heating fluid export pipeline; 6, filter course; 7, interlayer; 8, vapor tight tank support; 9, tapping valve; 10, snap joint; 11, Drainage pipe; 12, tap hole; 13, gas-liquid separator; 14, vavuum pump; 15, vacuum pipe; 16, air compressor machine; 17, liquid feed valve; 18, pneumatics valve; 19, pipeline; 20, valve; 21, air compression pipeline; 22, charging valve; 23, reactor; 24, washing tank; 25, centrifuge; 26, baking oven.
Detailed description of the invention
Embodiment 1
A kind of equipment for separating liquid from solid, as shown in Figure 1, comprises vapor tight tank 2, air compressor machine 16, vavuum pump 14 and gas-liquid separator 13; The top of vapor tight tank 2 is provided with charge door 1, and also can make discharging opening, in vapor tight tank 2, middle and lower part is provided with filter course 6 simultaneously; Be provided with rotating shaft 3 outside vapor tight tank 2, rotating shaft 3 is connected with vapor tight tank 2 power turnover device; Rotating shaft 3 is hollow shaft, is connected above vapor tight tank 2 inner filtration layer 6 by rotating shaft 3, air compression pipeline 21 with air compressor machine 16; Be provided with tapping valve 9 and Drainage pipe 11 bottom vapor tight tank 2, another termination gas-liquid separator 13 of Drainage pipe 11, gas-liquid separator 13 top is connected with vavuum pump 14 by vacuum pipe 15, is provided with tap hole 12 bottom gas-liquid separator 13; Connected by pipeline 19 between air compression pipeline 21 and Drainage pipe 11, pipeline 19, Drainage pipe 11 and air compression pipeline 21 are respectively equipped with valve 20, liquid feed valve 17 and pneumatics valve 18.
Charging valve 22 and snap joint 10 is provided with at the charge door 1 at vapor tight tank 2 top; Tapping valve 9 place bottom vapor tight tank 2 is provided with snap joint 10.
Interlayer 7, heating fluid inlet ductwork 4 and heating fluid export pipeline 5 is provided with outside vapor tight tank 2.
Be provided with vapor tight tank support 8 outside vapor tight tank 2, vapor tight tank support 8 and vapor tight tank 2 are rotationally connected by the rotating shaft 3 of vapor tight tank 2 left and right sides; Heating fluid import 4 is connected with interlayer 7 through left side rotating shaft 3 with heating fluid outlet 5, and it is inner that air compression pipeline 21 enters vapor tight tank 2 through right side rotating shaft 3.
Use above-mentioned equipment for separating liquid from solid to produce the method for hopcalite agent, comprise the following steps:
1) in reactor, add water respectively, the concentrated sulfuric acid, manganese sulfate, potassium permanganate carries out chemical reaction, generate the mixed material of manganese dioxide, potassium sulfate and sulfuric acid.
2) joined in above-mentioned equipment for separating liquid from solid by the mixed material after reaction kettle for reaction and apply pressure, carry out Separation of Solid and Liquid, obtain solid manganese dioxide and fluid sulphuric acid, potassium sulfate respectively, concrete operations are:
A, the mixed material after reaction kettle for reaction is loaded vapor tight tank 2 from charge door 1, close the charging valve 22 of charge door 1;
B, valve 20 are closed, and open pneumatics valve 18, open air compressor machine 16 pairs of vapor tight tanks 2 and add malleation, make the liquid in material accelerate through filter course 6;
And/or c, open tapping valve 9, liquid feed valve 17, open vavuum pump 14, make to add negative pressure below vapor tight tank 2 filter course 6, all liq is entered knockout drum 13 fast;
In d, vapor tight tank 2 in material liquid drained after, close air compressor machine 16 and vavuum pump 14, discharged by tap hole 12 by the liquid in gas-liquid separator 13, main component is potassium sulfate, sulfuric acid, can reclaim.
3) by step 2) the solid manganese dioxide material that obtains again imports in reactor, adds copper-bath respectively, sodium carbonate liquor carries out chemical reaction, newly increase and generate solid basic copper carbonate and fluid sulphuric acid sodium mixed material in reactor.
4) mixed material after step 3) reaction kettle for reaction joined in above-mentioned equipment for separating liquid from solid apply pressure, carry out Separation of Solid and Liquid, operate same step 2), obtain solid manganese dioxide, basic copper carbonate and fluid sulphuric acid sodium respectively.
5) washed by the solid material that step 4) process obtains in equipment for separating liquid from solid, namely in vapor tight tank, add water, the sulfate ion in dilution solid material, disconnects snap joint 10, and vapor tight tank 2 power turnover device upset vapor tight tank 2 washs; Afterwards, connect snap joint 10, repeat b, the c in step 4) and Step d, the sulfate ion of filtering trace.
6), after repeating operation 1-3 time of step 5), the hopcalite agent semi-finished product of humidity are namely obtained.
7) the hopcalite agent semi-finished product of humidity step 6) obtained carry out dewatering, pulverizing and blowing process:
Dewater: make pneumatics valve 18 be in closed condition, make tapping valve 9, liquid feed valve 17 and valve 20 be in opening, open vavuum pump 14, negative pressure is added to vapor tight tank 2 filter course upper and lower part; Interlayer 7, heating fluid inlet ductwork 4 and heating fluid export pipeline 5 is provided with outside vapor tight tank 2; Vapor tight tank 2 is heated, makes moisture boiling volatilization in tank, moisture in the emptying vapor tight tank 2 of vavuum pump 14;
Pulverize: close vavuum pump 14, tapping valve 9, disconnect snap joint 10, vapor tight tank 2 power turnover device upset vapor tight tank 2, makes the hopcalite agent semi-finished product after dewatering in vapor tight tank 2 overturn and pulverizes;
Blowing: vapor tight tank 2 is turned to charge door 1 downward, opens charge door 1, releases the hopcalite agent semi-finished product after dewatering, after granulation, activation, obtain hopcalite agent finished product.
Step 2), apply pressure in step 4) and be: apply normal pressure to above vapor tight tank 2 filter course 6, or apply negative pressure in the below of filter course 6, or above filter course 6, apply normal pressure, these three kinds of modes of below applying negative pressure simultaneously, apply normal pressure 0.1-2MPa and/or apply negative pressure-0.1MPa.
Step 6): be 0.5-10 times of solid material quality in step 6) vapor tight tank 2 to the amount of adding water in vapor tight tank 2.
Step 7): water removal phase, vapor tight tank 2 filter course upper and lower part is added to the pressure of negative pressure for-0.1MPa, the heating-up temperature of vapor tight tank 2 is 60-120 DEG C, and the time of dewatering is 4 hours.
The utility model is rational in infrastructure, good effect of separating solid from liquid, and production efficiency is high; Use this device to produce hopcalite agent cost low, with short production cycle, and can reclaim sulfuric acid potassium and sodium sulphate be distinguished, potassium sulfate and sodium sulphate can be recycled.
This device Separation of Solid and Liquid adopts pressure mode, and principal mode has 1. malleation; 2. negative pressure; 3. comprehensive, malleation+negative pressure; This device can also realize simultaneously, upset; The functions such as heating, insulation.This device and principle thereof can be applied in other like products (molecule is moisture), realize Separation of Solid and Liquid, drying, pulverizing.
Claims (4)
1. an equipment for separating liquid from solid, is characterized in that: comprise vapor tight tank (2), air compressor machine (16), vavuum pump (14) and gas-liquid separator (13);
The top of described vapor tight tank (2) is provided with charge door (1), and also make discharging opening, vapor tight tank (2) interior middle and lower part is provided with filter course (6) simultaneously;
Vapor tight tank (2) outside is provided with rotating shaft (3), and rotating shaft (3) is connected with vapor tight tank (2) power turnover device; Described rotating shaft (3) is hollow shaft, and vapor tight tank (2) inner filtration layer (6) top is connected with air compressor machine (16) by rotating shaft (3), air compression pipeline (21);
Vapor tight tank (2) bottom is provided with tapping valve (9) and Drainage pipe (11), another termination gas-liquid separator (13) of Drainage pipe (11), gas-liquid separator (13) top is connected with vavuum pump (14) by vacuum pipe (15), and gas-liquid separator (13) bottom is provided with tap hole (12);
Connected by pipeline (19) between air compression pipeline (21) and Drainage pipe (11), pipeline (19), Drainage pipe (11) and air compression pipeline (21) are respectively equipped with valve (20), liquid feed valve (17) and pneumatics valve (18).
2. equipment for separating liquid from solid according to claim 1, is characterized in that, is provided with charging valve (22) and snap joint (10) at the charge door (1) at vapor tight tank (2) top; Snap joint (10) is provided with at tapping valve (9) place of vapor tight tank (2) bottom.
3. equipment for separating liquid from solid according to claim 1, is characterized in that described vapor tight tank (2) outside is provided with interlayer (7), heating fluid inlet ductwork (4) and heating fluid export pipeline (5).
4. equipment for separating liquid from solid according to claim 1, it is characterized in that described vapor tight tank (2) outside is provided with vapor tight tank support (8), vapor tight tank support (8) and vapor tight tank (2) are rotationally connected by the rotating shaft (3) of vapor tight tank (2) left and right sides; Side rotating shaft (3) connects air compression pipeline (21), and opposite side rotating shaft (3) connects heating fluid inlet ductwork (4) and heating fluid export pipeline (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520125314.4U CN204502555U (en) | 2015-03-04 | 2015-03-04 | Equipment for separating liquid from solid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520125314.4U CN204502555U (en) | 2015-03-04 | 2015-03-04 | Equipment for separating liquid from solid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204502555U true CN204502555U (en) | 2015-07-29 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520125314.4U Withdrawn - After Issue CN204502555U (en) | 2015-03-04 | 2015-03-04 | Equipment for separating liquid from solid |
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| Country | Link |
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| CN (1) | CN204502555U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104689637A (en) * | 2015-03-04 | 2015-06-10 | 邯郸市同达矿用电器有限公司 | Solid-liquid separation device and method for producing Hopcalite |
| CN105330098A (en) * | 2015-10-26 | 2016-02-17 | 黄文龙 | Advanced wastewater treatment process where hydrostatic and hydrodynamic principle is applied |
| CN110215751A (en) * | 2019-04-12 | 2019-09-10 | 四川宝石机械石油钻头有限责任公司 | Negative pressure solid-liquid separation system applied to roller air exciting |
| CN112436187A (en) * | 2020-11-24 | 2021-03-02 | 徐文忠 | Gel electrolyte for lithium battery |
-
2015
- 2015-03-04 CN CN201520125314.4U patent/CN204502555U/en not_active Withdrawn - After Issue
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104689637A (en) * | 2015-03-04 | 2015-06-10 | 邯郸市同达矿用电器有限公司 | Solid-liquid separation device and method for producing Hopcalite |
| CN104689637B (en) * | 2015-03-04 | 2016-06-01 | 邯郸市同达矿用电器有限公司 | The method of equipment for separating liquid from solid and production hopcalite agent |
| CN105330098A (en) * | 2015-10-26 | 2016-02-17 | 黄文龙 | Advanced wastewater treatment process where hydrostatic and hydrodynamic principle is applied |
| CN110215751A (en) * | 2019-04-12 | 2019-09-10 | 四川宝石机械石油钻头有限责任公司 | Negative pressure solid-liquid separation system applied to roller air exciting |
| CN112436187A (en) * | 2020-11-24 | 2021-03-02 | 徐文忠 | Gel electrolyte for lithium battery |
| CN112436187B (en) * | 2020-11-24 | 2022-12-02 | 徐文忠 | Gel electrolyte for lithium battery |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20150729 Effective date of abandoning: 20160601 |
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| C25 | Abandonment of patent right or utility model to avoid double patenting |