CN204017442U - A kind of solvent separation unit - Google Patents
A kind of solvent separation unit Download PDFInfo
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- CN204017442U CN204017442U CN201420484492.1U CN201420484492U CN204017442U CN 204017442 U CN204017442 U CN 204017442U CN 201420484492 U CN201420484492 U CN 201420484492U CN 204017442 U CN204017442 U CN 204017442U
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- demixing
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Abstract
The utility model belongs to liquid separation technology field, relate to a kind of solvent separation unit, comprise retort and demixing of solvents room, described retort is communicated with condenser and trident woven hose successively by conduit, the conduit of the outlet of trident woven hose stretches to the inner chamber middle and lower part of demixing of solvents room, the conduit passed through with the inner chamber of demixing of solvents room that the outer bottom of demixing of solvents room connects is communicated with valve successively, depending on cup and valve, one end of the solvent refluxing pipe of horizontally set is communicated with the inner chamber top of demixing of solvents room, the other end is communicated with the inner chamber top of retort, structure of the present utility model is simple, easy and simple to handle, the separating rate of solvent is fast, separating effect is better, be applicable to gaseous state or liquid solvent quick separating.
Description
Technical field
The utility model belongs to liquid separation technology field, refers in particular to a kind of solvent separation unit.
Background technology
At present, two kinds of solvents dissolved each other mix generally takes the method for distilling they to be separated, utilize the difference of two kinds of solvent boiling points, when temperature reach a kind of boiling point of solvent and boiling point lower than another kind of solvent time, a kind of solvent is just gasificated into gas, then makes two kinds of separated from solvent by condensing reflux.Separation temperature is difficult to control in this way, and when particularly the boiling point of two kinds of solvents is more or less the same, segregation ratio is more difficult.
Summary of the invention
The purpose of this utility model is to provide a kind of simple easy solvent separation unit.
The purpose of this utility model is achieved in that
A kind of solvent separation unit, comprise retort and demixing of solvents room, described retort is communicated with condenser and trident woven hose successively by conduit, the conduit of the outlet of trident woven hose stretches to the inner chamber middle and lower part of demixing of solvents room, the conduit passed through with the inner chamber of demixing of solvents room that the outer bottom of demixing of solvents room connects is communicated with valve successively, looks cup and valve, and one end of the solvent refluxing pipe of horizontally set is communicated with the inner chamber top of demixing of solvents room, the other end is communicated with the inner chamber top of retort.
Above-mentioned solvent refluxing pipe is provided with and stops that the U-shaped trapping of gas backstreaming is curved to be connect.
Above-mentioned trident woven hose is Y-shaped three-way pipe.
The utility model gives prominence to compared to existing technology and useful technique effect is:
1, solvent separation unit of the present utility model, utilize two kinds of solvents dissolved each other only wherein a kind of solvent-soluble in the characteristic of the third solvent, separation and recovery can be insoluble to the solvent of the third solvent effectively rapidly.
3, structure of the present utility model is simple, easy and simple to handle, and the separating rate of solvent is fast, and separating effect is better, is applicable to gaseous state or liquid solvent quick separating.
Accompanying drawing explanation
Fig. 1 is structural principle schematic diagram of the present utility model.
Detailed description of the invention
The utility model is further described with specific embodiment below in conjunction with accompanying drawing, see Fig. 1:
A kind of solvent separation unit, comprise retort 10 and demixing of solvents room 50, described retort 10 is communicated with condenser 30 and trident woven hose 40 successively by conduit 21, the conduit 23 of the outlet of trident woven hose 40 stretches to the inner chamber middle and lower part of demixing of solvents room 50, the outer bottom of demixing of solvents room 50 the connects conduit 24 passed through with inner chamber 51 that is demixing of solvents room 50 is communicated with valve 52 successively, depending on cup 53 and valve 54, one end of the solvent refluxing pipe 22 of horizontally set is communicated with inner chamber 51 top of demixing of solvents room 50, the other end is communicated with the inner chamber top of retort 10.
Above-mentioned solvent refluxing pipe 22 is provided with and stops that the U-shaped trapping of gas backstreaming is curved to be connect.
Above-mentioned trident woven hose 40 is Y-shaped three-way pipe.
Such as, there are in retort 10 dimethylbenzene and methyl alcohol two kinds of solvents dissolved each other, inner chamber 51 middle and lower part of liquid by Y-shaped three-way pipe instillation demixing of solvents room 50 is condensed into through condenser 30 after two kinds of solvent gasifications of dissolving each other in the process of reaction, simultaneously, the third solvent---the aqueous solution dissolving in methyl alcohol is added from another opening part 41 of Y-shaped three-way pipe, the aqueous solution and dimethylbenzene and methyl alcohol two kinds of solution dissolved each other together enter inner chamber 51 middle and lower part of demixing of solvents room 50 by conduit 23, ratio after methyl alcohol in inner chamber 51 middle and lower part of demixing of solvents room 50 and the aqueous solution dissolve each other is great, bottom the inner chamber 51 sinking to demixing of solvents room 50, and pass through the valve 52 of bottom, another container is entered depending on cup 24 and valve 53, and water-fast dimethylbenzene floats, by-pass valve control 52, the aperture of 54, the liquid level in the inner chamber 51 of demixing of solvents room 50 is made to be positioned near the import of solvent refluxing pipe 22, isolated liquid paraxylene is back in reactor 10 by solvent refluxing pipe 22, in the process of solvent refluxing, because curved the connecing in 121 of U-shaped trapping stores liquid paraxylene always, there is the effect of trapping, cause the dimethylbenzene in reactor 10 and methyl alcohol two kinds of gaseous solvents dissolved each other directly can not enter in demixing of solvents room 50 from solvent refluxing pipe 22, the xylene solvent of gaseous state is refluxed utilization timely, certainly, the utility model not only can separating dimethyl benzene and methyl alcohol two kinds of solvents dissolved each other, utilize above-mentioned characteristic, other solvent with These characteristics can be separated.
Above-described embodiment is only preferred embodiment of the present utility model, not limits protection domain of the present utility model according to this, therefore: all equivalence changes done according to structure of the present utility model, shape, principle, all should be covered by within protection domain of the present utility model.
Claims (3)
1. a solvent separation unit, comprise retort and demixing of solvents room, it is characterized in that: described retort is communicated with condenser and trident woven hose successively by conduit, the conduit of the outlet of trident woven hose stretches to the inner chamber middle and lower part of demixing of solvents room, the conduit passed through with the inner chamber of demixing of solvents room that the outer bottom of demixing of solvents room connects is communicated with valve successively, looks cup and valve, and one end of the solvent refluxing pipe of horizontally set is communicated with the inner chamber top of demixing of solvents room, the other end is communicated with the inner chamber top of retort.
2. solvent separation unit according to claim 1, is characterized in that: described solvent refluxing pipe is provided with and stops that the U-shaped trapping of gas backstreaming is curved to be connect.
3. solvent separation unit according to claim 1, is characterized in that: described trident woven hose is Y-shaped three-way pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420484492.1U CN204017442U (en) | 2014-08-26 | 2014-08-26 | A kind of solvent separation unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420484492.1U CN204017442U (en) | 2014-08-26 | 2014-08-26 | A kind of solvent separation unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204017442U true CN204017442U (en) | 2014-12-17 |
Family
ID=52057357
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420484492.1U Active CN204017442U (en) | 2014-08-26 | 2014-08-26 | A kind of solvent separation unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204017442U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106546067A (en) * | 2015-09-18 | 2017-03-29 | 海南椰国食品有限公司 | Bacterial cellulose gel film replaces low temperature integrated dry drying system |
-
2014
- 2014-08-26 CN CN201420484492.1U patent/CN204017442U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106546067A (en) * | 2015-09-18 | 2017-03-29 | 海南椰国食品有限公司 | Bacterial cellulose gel film replaces low temperature integrated dry drying system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: ZHEJIANG SILVER-ELEPHANT BIO-ENGINEERING Co.,Ltd. Assignor: ZHEJIANG SHENGDA BIO-PHARM Co.,Ltd. Contract record no.: X2021330000155 Denomination of utility model: A solvent separation device Granted publication date: 20141217 License type: Common License Record date: 20210828 |