CN203620619U - Fullerene electric arc device - Google Patents
Fullerene electric arc device Download PDFInfo
- Publication number
- CN203620619U CN203620619U CN201320710393.6U CN201320710393U CN203620619U CN 203620619 U CN203620619 U CN 203620619U CN 201320710393 U CN201320710393 U CN 201320710393U CN 203620619 U CN203620619 U CN 203620619U
- Authority
- CN
- China
- Prior art keywords
- anode
- negative electrode
- fullerene
- source device
- trigger
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 title claims abstract description 37
- 229910003472 fullerene Inorganic materials 0.000 title claims abstract description 37
- 238000010891 electric arc Methods 0.000 title claims abstract description 17
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 40
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 39
- 239000010439 graphite Substances 0.000 claims abstract description 39
- 239000000203 mixture Substances 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims description 6
- 239000000498 cooling water Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 4
- 238000010923 batch production Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000001291 vacuum drying Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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Abstract
The utility model discloses a fullerene electric arc device. The fullerene electric arc device comprises an anode, a cathode and a cathode graphite plate, wherein the anode and the cathode are positioned at the same side of the cathode graphite plate and form a guide loop shaped like a Chinese character 'hui', the cathode graphite plate is arranged at one end of the cathode, a graphite rod of the anode and the cathode graphite plate come into contact to generate electric arc and evaporate the triggering end of the anode to generate a fullerene-containing mixture. The design structure of the guide loop shaped like a Chinese character 'hui' is adopted, and a furnace body mounting plate (a flange) is fixed on a vacuum furnace, so that electric arc discharge occurs in a vacuum environment; multiple fullerene electric arc devices can be arranged according to the size of the furnace body and the demand, therefore, high-efficiency batch production of fullerene can be achieved.
Description
Technical field
The utility model discloses a kind of fullerene arc source device, divides and belongs to the arc source device technique field that graphite acr method production fullerene is used by International Patent Classification (IPC) (IPC).
Background technology
Fullerene is carbon, the allotropes such as graphite, modal have a C60, the empty fullerenes such as C70 and the metal fullerene that comprises other elements, the preparation of fullerene at present also rests on the laboratory gram level production phase, along with the application of fullerene and metal fullerene thereof, market rolls up fullerene and metal fullerene demand, and original laboratory section grinding device cannot meet the demands.
It is current conventional method that arc process is prepared fullerene, be by arc crucible oven by anodic-cathodic arc discharge, graphite electrode evaporation is formed, make after cooling, anodic-cathodic is oppositely arranged and is arranged in body of heater, and the anodic-cathodic in body of heater is linearly aligned scattered distribution.
China document CN201010591761.0 discloses a kind of rotating the arc synthetic furnace of preparing fullerene nano material, and the anode electrode in its arc source is oppositely arranged with cathode electrode and the cathode rod that is connected and anode push rod extend in opposite direction and pass body of heater left and right side; China document CN 200510124525.7 discloses a kind of method of producing fullerene in temperature-controlling arc furnace, wherein electric arc furnaces has adopted the anode rotating disk that the consumable anode rod of 1-6 root is installed, but the layout of arc source yin, yang electrode is identical with aforementioned documents, and its production capacity and efficiency are all lower.
Summary of the invention
For the deficiencies in the prior art, the utility model provides a kind of fullerene arc source device rational in infrastructure, designs by back-shaped electrode loop, realizes multiple arcs source and is arranged on the object in same fullerenes synthesis stove.
For achieving the above object, the utility model is achieved through the following technical solutions:
A kind of fullerene arc source device, comprise that anode, negative electrode and negative electrode trigger body, described anode, negative electrode and negative electrode trigger a back-shaped water conservancy diversion loop of body composition, negative electrode wherein triggers body and is arranged at negative electrode one end, and the trigger end of anode and negative electrode trigger body and contact afterwards generation electric arc and evaporate the trigger end of positive electrode and produce the mixture that contains fullerene.
Further, described anode and negative electrode are fixed on installing plate, and the trigger end of anode can move forward and backward to keep itself and negative electrode to trigger the relative position of body.
Further, described anode trigger end is graphite rod, and this graphite rod is connected with anode cardan shaft and moves forward and backward to realize, and this cardan shaft is through installing plate and by the control of linear slide module, and described linear slide module is placed in installing plate opposite side.
Further; described linear slide module and servomotor composition Automatic Propulsion System promote anode cardan shaft; thereby advance the graphite rod being arranged on anode; anode cardan shaft employing anodized insulation fixture is fixed on slide block and with linear slide module and is connected, and the part that anode cardan shaft is positioned at installing plate graphite rod side is provided with anodic protection cover.
Further, it is graphite sheet or bar or other graphite bodies that described negative electrode triggers body, and it is placed in the front end of the graphite rod of anode, and optimal way negative electrode triggers that body is vertical with graphite rod to be arranged.
Further, described negative electrode triggers body and is connected with cathode axis, and this cathode axis is through installing plate.
Further, in described anode cardan shaft and cathode axis, be provided with cooling duct and passway and form cooling water nozzle.
The project organization in the back-shaped water conservancy diversion of the utility model loop, is fixed on vacuum drying oven by installing plate (flange), thereby arc discharge is occurred under vacuum environment.The utility model arc source device can be according to demand and body of heater size install multiple, thereby realize efficient batch production fullerene.
Accompanying drawing explanation
Fig. 1 is the utility model structural representation.
The specific embodiment
Below in conjunction with accompanying drawing, the utility model is described in further detail:
Embodiment: refer to Fig. 1, a kind of fullerene arc source device, comprise that anode, negative electrode and negative electrode trigger body 13, described anode, negative electrode are positioned at negative electrode and trigger body 13 homonymies and back-shaped water conservancy diversion loop of composition, negative electrode wherein triggers body 13 and is arranged at negative electrode one end, generation electric arc evaporate the trigger end of positive electrode and produce the mixture that contains fullerene after the trigger end of anode and negative electrode trigger body and contact, carries out subsequent treatment to mixture and isolates fullerene.Anode of the present utility model and negative electrode are fixed on installing plate 8 or flange, the trigger end of anode can move forward and backward to keep itself and negative electrode to trigger the relative position of body, described anode trigger end is graphite rod 11, this graphite rod is connected with anode cardan shaft 5 and moves forward and backward to realize, this cardan shaft passes installing plate 8 and is controlled by linear slide module 6, and linear slide module 6 of the present utility model is placed in installing plate 8 opposite sides.Linear slide module 6 forms Automatic Propulsion System with servomotor 1 and promotes anode cardan shaft; thereby advance the graphite rod 11 being arranged on anode; anode cardan shaft 5 adopts anodized insulation fixture 4 to be fixed on slide block 3 and with linear slide module 6 to be connected; the part that anode cardan shaft 5 is positioned at installing plate graphite rod side is provided with anodic protection cover 10, has cooling duct and passway to form cooling water nozzle 2 in anode cardan shaft.
It is graphite sheet or bar or other graphite bodies that negative electrode of the present utility model triggers body 13, and it is placed in the front end of the graphite rod of anode, and optimal way negative electrode triggers body 13 setting vertical with graphite rod 11.Negative electrode triggers body and is connected with cathode axis 12, and this cathode axis, through installing plate, has cooling duct and passway to form negative electrode cooling water nozzle 7 in cathode axis.
The utility model arc source device is by servomotor 1, linear slide module 6, anode, negative electrode, negative electrode graphite cake composition.The Automatic Propulsion System of servomotor and linear slide module composition promotes anode, thereby advances the graphite rod being arranged on anode.Anode cardan shaft 5 adopts anodized insulation fixture to be fixed on slide block with linear slide module 6, and in anode cardan shaft body of heater, part is installed anodic protection cover, the high temperature that in isolated body of heater, electric arc produces.
Arc source device is fixed on vacuum drying oven by body of heater installing plate (flange), and in Fig. 1, dotted line is body of heater inside 9, thereby arc discharge is occurred under vacuum environment.Anode, graphite rod and negative electrode, negative electrode graphite cake form a back-shaped water conservancy diversion loop in body of heater, after graphite rod contacts with negative electrode graphite cake, produce arc discharge phenomenon, arc discharge phenomenon produces by making graphite rod evaporate rapidly to consume in electric arc rapidly the mixture that contains fullerene.Anode cathode arc interdischarge interval, is undertaken cooling by cooling water nozzle target anode.Graphite anode rod of the present utility model and cathode axis are positioned at negative electrode graphite cake homonymy, and negative electrode graphite cake is fixed on the top of cathode axis.
Above record, only, for utilizing the embodiment of this origination techniques content, modification, variation that any those skilled in the art use this creation to do, all belong to the scope of the claims that this creation is advocated, and be not limited to those disclosed embodiments.
Claims (7)
1. a fullerene arc source device, it is characterized in that: comprise that anode, negative electrode and negative electrode trigger body, described anode, negative electrode and negative electrode trigger a back-shaped water conservancy diversion loop of body composition, negative electrode wherein triggers body and is arranged at negative electrode one end, and the trigger end of anode and negative electrode trigger body and contact afterwards generation electric arc and evaporate the trigger end of positive electrode and produce the mixture that contains fullerene.
2. fullerene arc source device according to claim 1, is characterized in that: described anode and negative electrode are fixed on installing plate, and the trigger end of anode can move forward and backward to keep itself and negative electrode to trigger the relative position of body.
3. fullerene arc source device according to claim 1, it is characterized in that: described anode trigger end is graphite rod, this graphite rod is connected with anode cardan shaft and moves forward and backward to realize, cardan shaft is through installing plate and by the control of linear slide module, and described linear slide module is placed in installing plate opposite side.
4. fullerene arc source device according to claim 3; it is characterized in that: described linear slide module and servomotor composition Automatic Propulsion System promote anode cardan shaft; thereby advance the graphite rod being arranged on anode; anode cardan shaft employing anodized insulation fixture is fixed on slide block and with linear slide module and is connected, and the part that anode cardan shaft is positioned at installing plate graphite rod side is provided with anodic protection cover.
5. fullerene arc source device according to claim 1, is characterized in that: it is graphite sheet or bar that described negative electrode triggers body.
6. fullerene arc source device according to claim 1, is characterized in that: described negative electrode triggers body and is connected with cathode axis, and this cathode axis is through installing plate.
7. according to the fullerene arc source device one of claim 1 to 5 Suo Shu, it is characterized in that: in described anode cardan shaft and cathode axis, be provided with cooling duct and passway and form cooling water nozzle.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320710393.6U CN203620619U (en) | 2013-11-12 | 2013-11-12 | Fullerene electric arc device |
| JP2016550917A JP6039866B2 (en) | 2013-11-12 | 2014-07-30 | Fullerene arc source and fullerene manufacturing apparatus equipped with an arc source |
| EP14861746.7A EP3050617B1 (en) | 2013-11-12 | 2014-07-30 | Fullerene arc source and fullerene production apparatus comprising arc source |
| US14/784,289 US9452410B2 (en) | 2013-11-12 | 2014-07-30 | Fullerene arc source and fullerene production apparatus comprising the same |
| PCT/CN2014/083313 WO2015070642A1 (en) | 2013-11-12 | 2014-07-30 | Fullerene arc source and fullerene production apparatus comprising arc source |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320710393.6U CN203620619U (en) | 2013-11-12 | 2013-11-12 | Fullerene electric arc device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203620619U true CN203620619U (en) | 2014-06-04 |
Family
ID=50807146
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320710393.6U Expired - Lifetime CN203620619U (en) | 2013-11-12 | 2013-11-12 | Fullerene electric arc device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203620619U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104362064A (en) * | 2014-11-21 | 2015-02-18 | 厦门福纳新材料科技有限公司 | Electrode structure for vacuum arc discharge |
| WO2015070642A1 (en) * | 2013-11-12 | 2015-05-21 | 厦门福纳新材料科技有限公司 | Fullerene arc source and fullerene production apparatus comprising arc source |
-
2013
- 2013-11-12 CN CN201320710393.6U patent/CN203620619U/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015070642A1 (en) * | 2013-11-12 | 2015-05-21 | 厦门福纳新材料科技有限公司 | Fullerene arc source and fullerene production apparatus comprising arc source |
| US9452410B2 (en) | 2013-11-12 | 2016-09-27 | Xiamen Funano New Material Technology Company. Ltd | Fullerene arc source and fullerene production apparatus comprising the same |
| CN104362064A (en) * | 2014-11-21 | 2015-02-18 | 厦门福纳新材料科技有限公司 | Electrode structure for vacuum arc discharge |
| CN104362064B (en) * | 2014-11-21 | 2016-08-17 | 厦门福纳新材料科技有限公司 | A kind of electrode structure of vacuum arc discharge |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term |
Granted publication date: 20140604 |
|
| CX01 | Expiry of patent term |