CN203365266U - System for detecting essence release amount of adsorbing material - Google Patents

System for detecting essence release amount of adsorbing material Download PDF

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Publication number
CN203365266U
CN203365266U CN 201320443866 CN201320443866U CN203365266U CN 203365266 U CN203365266 U CN 203365266U CN 201320443866 CN201320443866 CN 201320443866 CN 201320443866 U CN201320443866 U CN 201320443866U CN 203365266 U CN203365266 U CN 203365266U
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China
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cigarette
essence
material layer
detection system
steel pipe
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CN 201320443866
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孔浩辉
陈森林
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China Tobacco Guangdong Industrial Co Ltd
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China Tobacco Guangdong Industrial Co Ltd
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Abstract

The utility model discloses a system for detecting the essence release amount of an absorbing material. The system comprises a constant temperature water bath device, a vapor absorbing device, a simulation cigarette, a suction device and a weighing device, wherein the simulation cigarette comprises a steel pipe with the same size as that of a cigarette; the interior of the steel pipe is sequentially filled with a first breathable material layer, a material layer absorbing samples to be detected, a second breathable material layer and a cigarette filter layer; openings are formed in the two sides of the steel pipe; the opening close to one side of the cigarette filter layer is connected with the suction device; the opening close to one side of the first breathable material layer is connected with the vapor absorbing device; the simulation cigarette is arranged on the water bath of the constant temperature water bath device. The system for detecting the essence release amount of an absorbing material is simple in structure and low in cost, can simulate negative pressure desorption process of sucking the cigarette more quickly and conveniently, and can satisfy the use demand of a general test.

Description

The detection system of essence burst size on a kind of sorbing material
Technical field
The utility model relates to the cigarette analysis field, is specifically related to the detection system of essence burst size on a kind of sorbing material.
Background technology
In the preparation process of cigarette, in order to improve the organoleptic factors such as mouthfeel, smell, tend to add appropriate essence in cigarette.Due to these essence, by adding on sorbing material in cigarette, its release relates to the process of a desorption attached (being desorption).Different essence has different desorption performances on sorbing material, and therefore, the research staff often is difficult to accurately differentiate the addition of different essence.Desorption performance to different essence on sorbing material is investigated, and sums up its rule and contributes to instruct the research staff to carry out the content of preparing essence in cigarette according to actual needs.In actual application, have the smoking machine of employing to be studied, but smoking machine equipment is larger, and somewhat expensive, be difficult to meet the use of general experiment.
Summary of the invention
The purpose of this utility model is to overcome the deficiencies in the prior art, provides a kind of easy, and cost low energy meets the detection system of essence burst size on the practical sorbing material of general experiment.
Above-mentioned purpose of the present utility model is achieved by following technical solution:
The detection system of essence burst size on a kind of sorbing material, comprise constant temperature water bath apparatus, water vapor adsorption device, simulation cigarette, aspirator and meausring apparatus; Described analog roll tobacco bale draw together one with the measure-alike steel pipe of cigarette, the inside of steel pipe is filled with successively the first breathable material layer, has adsorbed the material layer of testing sample, the second breathable material layer and cigarette filter layer; The both sides of steel pipe are provided with opening; Opening near cigarette filter layer one side is connected with aspirator, and the opening of close the first breathable material layer one side is connected with the water vapor adsorption device; Described simulation cigarette is placed in the water-bath of described constant temperature water bath apparatus.
Be placed in the water-bath of described constant temperature water bath apparatus by simulating cigarette, can be by the environment temperature when aspirating to the accurate control simulation cigarette of the adjusting of bath temperature.
Wherein, described water vapor adsorption device is the pipe that a hollow and two ends are provided with opening; The opening of water vapor adsorption device one end is connected with the simulation cigarette; Absorbent material is filled in the inside of water vapor adsorption device.Due to the simulation cigarette, as in water-bath, the air entered in the simulation cigarette contains relatively many moisture, and absorbent material can be removed by contained humidity in the gas of simulation cigarette, avoids disturbing for accurate calibration tape.
As a kind of preferred version, the pipe diameter of described simulation cigarette is 8mm.
Wherein, the connected mode of described water vapor adsorption device and simulation cigarette is for removably connecting.Dismountable mode, can be so that change the absorbent material in the water vapor adsorption device.
Wherein, the connected mode of described aspirator and simulation cigarette is for removably connecting.Adopt this two kinds of connected modes, be convenient to the weight of simulation cigarette is measured.
As a kind of preferred version, the simulation cigarette is connected with the water vapor adsorption device by silicone tube; By silicone tube, with aspirator, be connected.This connected mode is convenient to dismounting on the one hand, and on the other hand, the sealing function that silicone tube can play, while guaranteeing suction in pipeline gas leak phenomenon do not occur.Silicone tube can also provide dirigibility and convenience for dismounting.
Wherein, described simulation cigarette is connected with aspirator by three-way connection.The first path of three-way connection is connected with the simulation cigarette, and alternate path is connected with aspirator, and an elastic mechanism is set on three-way, and this elastic mechanism makes three-way form: (1) and atmospheric isolation; Or (2) this two states that communicates with atmosphere.When needs are aspirated, by elastic mechanism, make three-way and atmospheric isolation; When needs are dismantled or be emptying, three-way is communicated with atmosphere.
Wherein, described the first breathable material layer and described the second breathable material layer are the silica wool layer.The purpose of adding the first breathable material layer and described the second breathable material layer is in steel pipe, to move with the material layer that has adsorbed testing sample in order to intercept the filter tip layer.
Wherein, described constant temperature water bath apparatus is comprised of water-bath and temp controlling heater; Temp controlling heater is controlled the water temperature in water-bath.
In the utility model, described testing sample is essence.
Adopt the detection system of essence burst size on sorbing material described in the utility model, the method for being tested is:
Set the temperature of constant temperature water bath apparatus a ratings (being preferably 40 ℃), at first in the steel pipe of simulation cigarette, fill the first breathable material layer, the second breathable material layer and cigarette filter layer, adopt meausring apparatus to calculate the now quality of steel pipe, be designated as M1, then by steel pipe and water vapor adsorption device, aspirator is connected, repeatedly aspirate, until the quality of steel pipe does not change, record when now steel pipe weight is M2, rapidly the absorption of the quantitative M0 of weighing=0.05 g the material of essence load between the first breathable material layer and the second breathable material layer, weighing tube quality now, be designated as M3, then simulate suction, aspirate 50 ml at every turn, 2 s consuming time, evenly suction is 10 mouthfuls, the mass M 4 of the steel pipe after the weighing suction, the desorption rate of essence is △ M=M2+M0-M4.Desorption rate:
Figure 2013204438660100002DEST_PATH_IMAGE001
.
Compared with prior art, the utlity model has following beneficial effect:
On sorbing material described in the utility model, the detection system of essence burst size is simple in structure, can simulate more expediently cigarette smoking negative pressure desorption process, can do and contrast and set up corresponding relation with the essence desorption result with measuring under the smoking machine puffing regimens by the desorption result of essence on material under the smoking condition of this device Preliminary Determination, in later experiments, by the method, replacing smoking machine to carry out the screening of sorbing material in application facet.
The accompanying drawing explanation
The structural representation that Fig. 1 is the detection system of essence burst size on sorbing material described in the utility model.
Embodiment
Further describe the present invention below in conjunction with the drawings and specific embodiments.
Embodiment 1
The detection system of essence burst size on a kind of sorbing material, as shown in Figure 1, comprise constant temperature water bath apparatus 1, water vapor adsorption device 2, simulation cigarette 3, aspirator 4 and meausring apparatus 5; The structure of described simulation cigarette 3 as shown in Figure 2, comprise one with the measure-alike steel pipe 31 of cigarette, the inside of steel pipe 31 is filled with successively the first breathable material layer 32, has adsorbed material layer 33, the second breathable material layer 34 and the cigarette filter layer 35 of testing sample; The both sides of steel pipe are provided with opening; Near the opening of cigarette filter layer one side with by silicone tube 8, with three-way connection 6, be connected, three-way connection 6 is connected with aspirator 4, the opening of close the first breathable material layer one side is connected by silicone tube 7 with the water vapor adsorption device; Described simulation cigarette is placed in the water-bath of described constant temperature water bath apparatus.Described the first breathable material layer and described the second breathable material layer are the silica wool layer.Described constant temperature water bath apparatus 1 is comprised of water-bath 11 and temp controlling heater 12; By temp controlling heater, the water temperature in water-bath is controlled.The silica gel for water suction is filled in the inside of described water vapor adsorption device.
Adopt the detection system of essence burst size on sorbing material described in the utility model, the method for being tested is:
Set the temperature of constant temperature water bath apparatus a ratings (being preferably 40 ℃), at first in the steel pipe of simulation cigarette, fill the first breathable material layer, the second breathable material layer and cigarette filter layer, adopt meausring apparatus to calculate the now quality of steel pipe, be designated as M1, then by steel pipe and water vapor adsorption device, aspirator is connected, repeatedly aspirate, until the quality of steel pipe does not change, record when now steel pipe weight is M2, rapidly the absorption of the quantitative M0 of weighing=0.05 g the material of essence load between the first breathable material layer and the second breathable material layer, weighing tube quality now, be designated as M3, then simulate suction, aspirate 50 ml at every turn, 2 s consuming time, evenly suction is 10 mouthfuls, the mass M 4 of the steel pipe after the weighing suction, the desorption rate of essence is △ M=M2+M0-M4.Desorption rate:
Figure 102790DEST_PATH_IMAGE001
.

Claims (7)

1. the detection system of essence burst size on a sorbing material, is characterized in that, comprises constant temperature water bath apparatus, water vapor adsorption device, simulation cigarette, aspirator and meausring apparatus; Described analog roll tobacco bale draw together one with the measure-alike steel pipe of cigarette, the inside of steel pipe is filled with successively the first breathable material layer, has adsorbed the material layer of testing sample, the second breathable material layer and cigarette filter layer; The both sides of steel pipe are provided with opening; Opening near cigarette filter layer one side is connected with aspirator, and the opening of close the first breathable material layer one side is connected with the water vapor adsorption device; Described simulation cigarette is placed in the water-bath of described constant temperature water bath apparatus.
2. the detection system of essence burst size on sorbing material according to claim 1, is characterized in that, described water vapor adsorption device is the pipe that a hollow and two ends are provided with opening; The opening of water vapor adsorption device one end is connected with the simulation cigarette; Absorbent material is filled in the inside of water vapor adsorption device.
3. according to the detection system of essence burst size on the described sorbing material of claim 1 or 2, it is characterized in that, the connected mode of described water vapor adsorption device and simulation cigarette, aspirator and simulation cigarette is for removably connecting.
4. the detection system of essence burst size on sorbing material according to claim 1, is characterized in that, described simulation cigarette is connected with aspirator by three-way connection.
5. the detection system of essence burst size on sorbing material according to claim 4, is characterized in that, the connected mode of described simulation cigarette and three-way connection is for removably connecting.
6. the detection system of essence burst size on sorbing material according to claim 1, is characterized in that, described the first breathable material layer and described the second breathable material layer are the silica wool layer.
7. the detection system of essence burst size on sorbing material according to claim 1, its spy is, described constant temperature water bath apparatus is comprised of water-bath and temp controlling heater; Temp controlling heater is controlled the water temperature in water-bath.
CN 201320443866 2013-07-24 2013-07-24 System for detecting essence release amount of adsorbing material Expired - Lifetime CN203365266U (en)

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Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103884621A (en) * 2014-03-18 2014-06-25 广东中烟工业有限责任公司 Device and method for detecting desorption rate of cigarette materials
CN106959353A (en) * 2017-03-30 2017-07-18 河南中烟工业有限责任公司 Tobacco aromaticss essence smells fragrant pen and smells fragrant head
CN108490097A (en) * 2018-05-16 2018-09-04 云南中烟工业有限责任公司 A kind of detection method of the volatile organic compounds burst size of nanometer of filter tip
CN108535141A (en) * 2018-05-16 2018-09-14 云南中烟工业有限责任公司 The detection device and detection method of Rosa Damascana ingredient the amount of migration in a kind of filter stick
CN108535142A (en) * 2018-05-16 2018-09-14 云南中烟工业有限责任公司 A kind of detection method of the Peppermint essential oil ingredient the amount of migration of special flavoring filter stick
CN108535143A (en) * 2018-05-16 2018-09-14 云南中烟工业有限责任公司 A kind of detection method of the coffee aroma components the amount of migration of special flavoring filter stick
CN108627584A (en) * 2018-05-16 2018-10-09 云南中烟工业有限责任公司 The detection device and detection method of the aromatic amine burst size of a kind of nanometer of filter tip
CN108627583A (en) * 2018-05-16 2018-10-09 云南中烟工业有限责任公司 The detection method of royal jelly ingredient the amount of migration in a kind of filter stick
CN108645941A (en) * 2018-05-16 2018-10-12 云南中烟工业有限责任公司 The detection device and detection method of orange taste ingredient the amount of migration in a kind of filter stick
CN108663451A (en) * 2018-05-16 2018-10-16 云南中烟工业有限责任公司 The detection method of tea component the amount of migration in a kind of special flavoring filter stick
CN108663450A (en) * 2018-05-16 2018-10-16 云南中烟工业有限责任公司 The detection device and detection method of a kind of colorant migration amount for extraordinary filter tip
CN108680693A (en) * 2018-05-16 2018-10-19 云南中烟工业有限责任公司 It is a kind of to be used for the extraordinary phthalate compound of filter tip and the detection device and its detection method of tributyl phosphate the amount of migration
CN108693264A (en) * 2018-05-16 2018-10-23 云南中烟工业有限责任公司 The detection device and detection method of a kind of bouquet components the amount of migration for special flavoring filter stick
CN108918699A (en) * 2018-05-16 2018-11-30 云南中烟工业有限责任公司 A kind of detection method of the aldehyde material the amount of migration of nanometer of filter tip
CN108956748A (en) * 2018-05-16 2018-12-07 云南中烟工业有限责任公司 A kind of detection device and detection method of the heavy metal transformation amount for nanometer filter tip
CN110376091A (en) * 2019-08-26 2019-10-25 福建中烟工业有限责任公司 Measure the method and device of carbon dioxide adsorption in expanded cut tobacco
CN110879265A (en) * 2019-11-07 2020-03-13 云南中烟工业有限责任公司 Method for simulating and measuring heat migration quantity of formaldehyde and acetaldehyde to smoke in cigarette blasting beads

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103884621A (en) * 2014-03-18 2014-06-25 广东中烟工业有限责任公司 Device and method for detecting desorption rate of cigarette materials
CN103884621B (en) * 2014-03-18 2017-05-31 广东中烟工业有限责任公司 A kind of device and method of inspection smoking material desorption rate
CN106959353A (en) * 2017-03-30 2017-07-18 河南中烟工业有限责任公司 Tobacco aromaticss essence smells fragrant pen and smells fragrant head
CN108627583A (en) * 2018-05-16 2018-10-09 云南中烟工业有限责任公司 The detection method of royal jelly ingredient the amount of migration in a kind of filter stick
CN108663451A (en) * 2018-05-16 2018-10-16 云南中烟工业有限责任公司 The detection method of tea component the amount of migration in a kind of special flavoring filter stick
CN108535142A (en) * 2018-05-16 2018-09-14 云南中烟工业有限责任公司 A kind of detection method of the Peppermint essential oil ingredient the amount of migration of special flavoring filter stick
CN108535143A (en) * 2018-05-16 2018-09-14 云南中烟工业有限责任公司 A kind of detection method of the coffee aroma components the amount of migration of special flavoring filter stick
CN108627584A (en) * 2018-05-16 2018-10-09 云南中烟工业有限责任公司 The detection device and detection method of the aromatic amine burst size of a kind of nanometer of filter tip
CN108490097A (en) * 2018-05-16 2018-09-04 云南中烟工业有限责任公司 A kind of detection method of the volatile organic compounds burst size of nanometer of filter tip
CN108645941A (en) * 2018-05-16 2018-10-12 云南中烟工业有限责任公司 The detection device and detection method of orange taste ingredient the amount of migration in a kind of filter stick
CN108535141A (en) * 2018-05-16 2018-09-14 云南中烟工业有限责任公司 The detection device and detection method of Rosa Damascana ingredient the amount of migration in a kind of filter stick
CN108663450A (en) * 2018-05-16 2018-10-16 云南中烟工业有限责任公司 The detection device and detection method of a kind of colorant migration amount for extraordinary filter tip
CN108680693A (en) * 2018-05-16 2018-10-19 云南中烟工业有限责任公司 It is a kind of to be used for the extraordinary phthalate compound of filter tip and the detection device and its detection method of tributyl phosphate the amount of migration
CN108693264A (en) * 2018-05-16 2018-10-23 云南中烟工业有限责任公司 The detection device and detection method of a kind of bouquet components the amount of migration for special flavoring filter stick
CN108918699A (en) * 2018-05-16 2018-11-30 云南中烟工业有限责任公司 A kind of detection method of the aldehyde material the amount of migration of nanometer of filter tip
CN108956748A (en) * 2018-05-16 2018-12-07 云南中烟工业有限责任公司 A kind of detection device and detection method of the heavy metal transformation amount for nanometer filter tip
CN110376091A (en) * 2019-08-26 2019-10-25 福建中烟工业有限责任公司 Measure the method and device of carbon dioxide adsorption in expanded cut tobacco
CN110376091B (en) * 2019-08-26 2022-04-22 福建中烟工业有限责任公司 Method and device for measuring carbon dioxide adsorption quantity in expanded cut tobacco
CN110879265A (en) * 2019-11-07 2020-03-13 云南中烟工业有限责任公司 Method for simulating and measuring heat migration quantity of formaldehyde and acetaldehyde to smoke in cigarette blasting beads

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