CN203315789U - Ultrasonic wave and microwave combined tubular leaching device - Google Patents
Ultrasonic wave and microwave combined tubular leaching device Download PDFInfo
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- CN203315789U CN203315789U CN2013203460370U CN201320346037U CN203315789U CN 203315789 U CN203315789 U CN 203315789U CN 2013203460370 U CN2013203460370 U CN 2013203460370U CN 201320346037 U CN201320346037 U CN 201320346037U CN 203315789 U CN203315789 U CN 203315789U
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- microwave
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- agitator tank
- leaching device
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Abstract
The utility model provides an ultrasonic wave and microwave combined tubular leaching device. The ultrasonic wave and microwave combined tubular leaching device comprises a stirring tank, a delivery pump, an ultrasonic wave reactor and a microwave reaction tank, wherein the ultrasonic wave reactor is connected with the delivery pump by virtue of a first delivery pipe, the delivery pump is connected with the microwave reaction tank by virtue of a second delivery pipe, the ultrasonic wave reactor is connected with the microwave reaction tank by virtue of a third delivery pipe, and the microwave reaction tank is also connected with the stirring tank by virtue of a circulation return pipe and is used for delivering the mixed material treated by ultrasonic wave and microwave back to the stirring tank to be circulated. The ultrasonic wave and microwave combined tubular leaching device is short in leaching time, high in leaching efficiency and good in leaching quality and is applicable to large-scale industrialized application.
Description
Technical field
The utility model relates to the leaching technical field, particularly the tubular type leaching device of a kind of ultrasonic wave and microwave combination.
Background technology
Leaching (claiming again liquid-solid extraction) is a kind of application leaching agent dipping solid mixture, take the unit operations that separates soluble constituent and residue (can be with chemical reaction or be only physical dissolution), it is widely used in the industry such as chemistry, metallurgy, food and atomic energy, to obtain the component solution with using value or to be used for removing the solable matter be mingled with in insoluble solid.
The method that relates to the auxiliary leaching of microwave or ultrasonic wave of now having announced is mainly: (one) adopts merely microwave or adopts merely the auxiliary leaching of ultrasonic wave, and its leaching effect is limited; (2) the auxiliary leaching of microwave and ultrasonic wave being placed in to same container carries out.The Chinese patent that for example notification number is CN101274157B " a kind of cross current intrinsic cycle ultrasonic leaching reactor and leaching method thereof ", the apparatus structure complexity, be difficult for looking up the fault and maintenance; Another this container is stainless steel, and not only cost is high, and acid-alkali-corrosive-resisting not.
The utility model content
The purpose of this utility model is that a kind of leaching time of proposition is short, extraction rate is high, the leaching quality is good, is applicable to the ultrasonic wave of heavy industrialization application and the tubular type leaching device of microwave combination.
For achieving the above object, the utility model proposes the tubular type leaching device of a kind of ultrasonic wave and microwave combination, comprise: for the agitator tank of uniform stirring compound, for delivery of the delivery pump of the compound after stirring, the ultrasound reactor for generation of ul-trasonic irradiation in the compound after stirring; And for carry out the microwave reaction tank of microwave leaching to mixing rear material; Described ultrasound reactor is connected with delivery pump by the first carrier pipe, and described delivery pump is delivered to ultrasound reactor by the compound after stirring; Described delivery pump is connected with the microwave reaction tank by the second carrier pipe, is delivered directly to the microwave reaction tank for the mixed material after stirring and carries out the heating using microwave leaching; Be connected by the 3rd conveyance conduit between described ultrasound reactor and microwave reaction tank, for the compound after ul-trasonic irradiation being delivered to the microwave reaction tank, carry out that microwave is auxiliary to be leached; Described microwave reaction tank also is connected in agitator tank by the circulating reflux pipe, for the conveying of the compound after ultrasonic wave, microwave action is got back to agitator tank, is circulated.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, described circulating reflux pipe is provided with main finished product discharge pipe.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, be respectively equipped with thermometric on the outer wall of described agitator tank and take into account liquid level gauge.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, described agitator tank is provided with a rabbling mechanism, described rabbling mechanism comprises stirring motor and the puddler of being located at described agitator tank top, described puddler one end is connected in described stirring motor, and the other end is provided with paddle and stretches into described agitator tank inside.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, described paddle is double-deck paddle.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, the bottom of described microwave reaction tank is supported fixing by tank support.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, the bottom of described agitator tank is provided with discharging opening, and this discharging opening is extended with auxiliary finished product discharge pipe, and this discharging opening also is connected in delivery pump by the first carrier pipe.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, the top of described agitator tank also is provided with leaching agent charging aperture, material inlet and circulating reflux charging aperture, and described agitator tank is connected in the circulating reflux pipe by the circulating reflux charging aperture.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, the outer wall of described microwave reaction tank is provided with a plurality of microwave sources, and described microwave reaction tank inside is provided with anticorrosion carrier pipe, and the top of described microwave reaction tank is connected in the circulating reflux pipe.
Further, in the tubular type leaching device of above-mentioned ultrasonic wave and microwave combination, described a plurality of microwave sources are connected with circulating water cooling system.
The utility model microwave tube type leaching device leaching time is short, extraction rate is high, the leaching quality is good, is applicable to the heavy industrialization application.
The accompanying drawing explanation
The schematic flow sheet of tubular type leaching device one embodiment that Fig. 1 is the utility model ultrasonic wave and microwave combination.
The specific embodiment
Describe preferred embodiment of the present utility model in detail below in conjunction with accompanying drawing.
The tubular type leaching device of the utility model ultrasonic wave and microwave combination comprises agitator tank 1, delivery pump 2, ultrasound reactor 3 and microwave reaction tank 5; Described agitator tank 1, for uniform stirring compound (raw material and leaching agent), is respectively equipped with thermo detector 13 and liquid level gauge 11 on the outer wall of described agitator tank 1, described thermo detector 13 is stirred the temperature of material for measurement; Described delivery pump 2 is connected with ultrasound reactor 3 by the first carrier pipe 4; Described the first carrier pipe 4 is provided with a pressure gauge 42, for measuring the mixed material discharge pressure after stirring; Described delivery pump 2 also is connected with microwave reaction tank 5 by the second carrier pipe 6, is delivered directly to microwave reaction tank 5 for the mixed material after stirring and carries out the auxiliary leaching of microwave; Described ultrasound reactor 3 is connected with microwave reaction tank 5 by the 3rd conveyance conduit 7, for the compound after ul-trasonic irradiation being delivered to microwave reaction tank 5, carries out the auxiliary leaching of microwave; The charging of described delivery pump 2, discharging opening are equipped with respectively for shockproof and are flexible coupling 22; Described microwave reaction tank 5 also is connected in agitator tank 1 by circulating reflux pipe 8, for the conveying of the compound after ultrasonic wave, microwave action is got back to agitator tank 1, is circulated.
Wherein, described pressure gauge 42 is for the variation of Real-Time Monitoring delivery pump 2 material conveying force value, and described circulating reflux pipe 8 is provided with main finished product discharge pipe 82.
Described agitator tank 1 is the tank body shape, which is provided with a rabbling mechanism 12, described rabbling mechanism 12 comprises stirring motor 122 and the puddler 124 of being located at described agitator tank 1 top, described puddler 124 1 ends are connected in described stirring motor 122, and the other end is provided with paddle 126 and stretches into described agitator tank 1 inside.Paddle described in the present embodiment 126 is double-deck paddle.Described puddler 124 is controlled and is rotated by rabbling mechanism 12, thereby drive paddle 126 high speed rotating, compound is stirred, make the solid in raw material mix more even with liquid, more be conducive to leach the material in raw material, also reduced the granular size in the raw material, reduced the transporting resistance of compound simultaneously.
The top of described agitator tank 1 also is provided with leaching agent charging aperture 14, material inlet 15 and circulating reflux charging aperture 16, described leaching agent charging aperture 14 is for adding leaching agent toward agitator tank 1, described material inlet 15 is for adding raw material toward agitator tank 1, described agitator tank 1 is connected in circulating reflux pipe 8 by circulating reflux charging aperture 16, for the raw material circulation that will fully not leach, adds agitator tank 1 again to leach.
The bottom of described agitator tank 1 is provided with discharging opening 17, and this discharging opening 17 is extended with auxiliary finished product discharge pipe 18, and simultaneously, this discharging opening 17 also is connected in delivery pump 2 by the first carrier pipe 4.
Described agitator tank 1 bottom is provided with supporting and location support 10, for supporting fixedly agitator tank 1.
Described delivery pump 2 one ends are connected in agitator tank 1, the other end is connected in ultrasound reactor 3, be delivered to ultrasound reactor 3 and microwave reaction tank 5 for the compound through being uniformly mixed, described delivery pump 2 can accelerate the flowing velocity of solution in whole leaching device pipeline, prevents precipitation.
Described delivery pump 2 bottoms are provided with rack platform 26, for support, fixed delivery pump 2.
Described ultrasound reactor 3 inwalls are provided with a plurality of ultrasonic wave vibration plates 32 and two conveying pipes 34, and the bottom of described ultrasound reactor 3 is provided with feet 36, for support, mounting ultrasonic reactor 3.
The bottom of described microwave reaction tank 5 is supported fixing by tank support 52, the outer wall of described microwave reaction tank 5 is provided with a plurality of microwave sources 54, described microwave reaction tank 5 inside are provided with anticorrosion carrier pipe 56, described a plurality of microwave source 54 is connected with circulating water cooling system 58, for microwave source 54 is cooled.
Described the first carrier pipe 4, the second carrier pipe 6, the 3rd conveyance conduit 7 and anticorrosion carrier pipe 56 are S2.5 Series P PR anti-corrosion heat-resisting pipe, and its microwave transmission performance is better; Described the first carrier pipe 4, the second carrier pipe 6, the 3rd conveyance conduit 7 do not draw by insulation material 66() parcel, to prevent heat loss.
The top of described microwave reaction tank 5 is connected in circulating reflux pipe 8, for being delivered to agitator tank 1 by circulating reflux pipe 8 through the raw material of heating using microwave leaching.
It should be noted that, described agitator tank 1 adopts anticorrosion inner chamber design, and all parts junction of the utility model microwave tube type leaching device has all adopted acid and alkali-resistance preserving and sealing structure.
The work engineering of the tubular type leaching device of the utility model ultrasonic wave and microwave combination is as follows: at first, compound to be leached is added into to agitator tank 1 by leaching agent charging aperture 14, the material inlet 15 on agitator tank 1 top, by 12 pairs of compounds of rabbling mechanism, stirred, can effectively improve the contact area of compound, make it to mix and prevent precipitation, more be conducive to leach the material in raw material, also reduced the size particles layering in the raw material, reduced the transporting resistance of compound simultaneously; Then, through the compound stirred, by the first carrier pipe 4, by delivery pump 2, flow to ultrasound reactor 3, described ultrasound reactor 3 produces the ul-trasonic irradiation compound of section in the inner, to improve the extraction rate of leaching device; The compound of process ul-trasonic irradiation is delivered to microwave reaction tank 5 by the 3rd conveyance conduit 7 and carries out the auxiliary leaching of microwave; Perhaps described delivery pump 2 is delivered directly to microwave reaction tank 5 by the second carrier pipe 6 by the mixed material after stirring and carries out the auxiliary leaching of microwave; Described microwave reaction tank 5 produces microwave by a plurality of microwave sources 54 of its outer wall, compound to its inside carries out the auxiliary leaching of microwave, valuable metal component in microwave selective heating mineral, make the inner thermal stress that forms of ore particle, and then crack and hole, and the contact interface of continuous renewal valuable metal component and solvent, the promotion valuable metal reacts with solvent, has greatly improved the leaching effect; Microwave has the electromagnetic agitation effect simultaneously, and under the microwave high-frequency electromagnetic field effect, the polar molecule generation higher-order of oscillation in solvent and diffusion strengthening, played the effect of stirring, and makes to leach product and constantly peel off, and is conducive to the carrying out of leaching reaction.
Finally, compound, through ultrasonic wave, the auxiliary leaching of microwave, can obtain qualified leaching finished product with auxiliary finished product discharge pipe 18 through main finished product discharge pipe 82 after meeting the requirements.Simultaneously, fully the raw material of leaching can not circulate again, by circulating reflux pipe 6, reenters circulation leaching again in agitator tank 1.
Than prior art, the utility model microwave tube type leaching device has following advantage: (1), by the ultrasonic double action that involves microwave, has improved leaching speed and leaching effect greatly; (2) adopt agitator tank to stir raw material, make solid in raw material mix with liquid more even, more be conducive to leach; (3) ultrasound reactor and microwave reaction tank divide and are arranged, and have not only further improved leaching speed and leaching quality, and have made the leaching equipment enlarging, have met the requirement of heavy industrialization application; (4) ultrasound reactor and microwave reaction tank arranged apart after, each function device is relatively independent, not only simple to operate, and maintenance is convenient, maintenance cost also will reduce much in the future.(5) by the circulating reflux pipe, fully the raw material of leaching can recycle leaching, leaches more thoroughly, and " circulation " is conducive to the industrialization leached.
In fact, by ultrasonic wave and microwave arranged apart be consideration for many factors, relevant with the mechanism of action of ultrasonic wave and microwave.Due to the limitation of ultrasonic wave and the depth of microwave penetration, the selection of tubular structure can allow leaching more evenly, fully.
The tubular type leaching device of the utility model ultrasonic wave and microwave combination divides stirring, ultrasound reactor, microwave reactor to be arranged, and dividing is arranged stirs more evenly, can prevent precipitation, layering, reacts more thorough, and each other without impact; Various container inner walls in the utility model microwave tube type leaching device or pipeline are all the materials that adopt high temperature resistant, anti-soda acid.
To sum up, the utility model microwave tube type leaching device has that leaching time is short, extraction rate is high, the measured advantage of leaching matter, is applicable to the heavy industrialization application.
Here description of the present utility model and application is illustrative, not wants by scope restriction of the present utility model in the above-described embodiments.Here the distortion of disclosed embodiment and change is possible, and for those those of ordinary skill in the art, the various parts of the replacement of embodiment and equivalence are known.Those skilled in the art are noted that in the situation that do not break away from spirit of the present utility model or substantive characteristics, the utility model can, with other form, structure, layout, ratio, and realize with other assembly, material and parts.In the situation that do not break away from the utility model scope and spirit, can carry out other distortion and change to disclosed embodiment here.
Claims (10)
1. the tubular type leaching device of a ultrasonic wave and microwave combination, it is characterized in that, comprise: for the agitator tank of uniform stirring compound, for delivery of the delivery pump of the compound after stirring, the ultrasound reactor for generation of ul-trasonic irradiation in the compound after stirring; And for compound being carried out to the microwave reaction tank of microwave leaching; Described ultrasound reactor is connected with delivery pump by the first carrier pipe, and described delivery pump will be delivered to ultrasound reactor by compound after stirring; Described delivery pump is connected with the microwave reaction tank by the second carrier pipe, is delivered directly to the microwave reaction tank for the compound after stirring and carries out the auxiliary leaching of microwave; Be connected by the 3rd conveyance conduit between described ultrasound reactor and microwave reaction tank, for the compound after ul-trasonic irradiation being delivered to the microwave reaction tank, carry out that microwave is auxiliary to be leached; Described microwave reaction tank also is connected in agitator tank by the circulating reflux pipe, for the conveying of the compound after ultrasonic wave, microwave action is got back to agitator tank, is circulated.
2. the tubular type leaching device of ultrasonic wave according to claim 1 and microwave combination, is characterized in that, described circulating reflux pipe is provided with main finished product discharge pipe.
3. the tubular type leaching device of ultrasonic wave according to claim 2 and microwave combination, is characterized in that, is respectively equipped with thermometric on the outer wall of described agitator tank and takes into account liquid level gauge.
4. the tubular type leaching device that ultrasonic wave according to claim 1 and microwave combine, it is characterized in that, described agitator tank is provided with a rabbling mechanism, described rabbling mechanism comprises stirring motor and the puddler of being located at described agitator tank top, described puddler one end is connected in described stirring motor, and the other end is provided with paddle and stretches into described agitator tank inside.
5. the tubular type leaching device of ultrasonic wave according to claim 4 and microwave combination, is characterized in that, described paddle is double-deck paddle.
6. the tubular type leaching device of ultrasonic wave according to claim 1 and microwave combination, is characterized in that, the bottom of described microwave reaction tank is supported fixing by tank support.
7. the tubular type leaching device of ultrasonic wave according to claim 6 and microwave combination, is characterized in that, the bottom of described agitator tank is provided with discharging opening, and this discharging opening is extended with auxiliary finished product discharge pipe, and this discharging opening also is connected in delivery pump by the first carrier pipe.
8. the tubular type leaching device that ultrasonic wave according to claim 1 and microwave combine, it is characterized in that, the top of described agitator tank also is provided with leaching agent charging aperture, material inlet and circulating reflux charging aperture, and described agitator tank is connected in the circulating reflux pipe by the circulating reflux charging aperture.
9. the tubular type leaching device that ultrasonic wave according to claim 1 and microwave combine, it is characterized in that, the outer wall of described microwave reaction tank is provided with a plurality of microwave sources, and described microwave reaction tank inside is provided with anticorrosion carrier pipe, and the top of described microwave reaction tank is connected in the circulating reflux pipe.
10. the tubular type leaching device of ultrasonic wave according to claim 1 and microwave combination, is characterized in that, described a plurality of microwave sources are connected with circulating water cooling system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013203460370U CN203315789U (en) | 2013-06-18 | 2013-06-18 | Ultrasonic wave and microwave combined tubular leaching device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013203460370U CN203315789U (en) | 2013-06-18 | 2013-06-18 | Ultrasonic wave and microwave combined tubular leaching device |
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| Publication Number | Publication Date |
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| CN203315789U true CN203315789U (en) | 2013-12-04 |
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| CN2013203460370U Expired - Fee Related CN203315789U (en) | 2013-06-18 | 2013-06-18 | Ultrasonic wave and microwave combined tubular leaching device |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105521619A (en) * | 2014-09-30 | 2016-04-27 | 李肥生 | Coupled device for plant extraction |
| CN112794929A (en) * | 2021-01-25 | 2021-05-14 | 西藏天虹科技股份有限责任公司 | Highland barley beta-glucan extraction process based on ultrasonic assistance |
-
2013
- 2013-06-18 CN CN2013203460370U patent/CN203315789U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105521619A (en) * | 2014-09-30 | 2016-04-27 | 李肥生 | Coupled device for plant extraction |
| CN105521619B (en) * | 2014-09-30 | 2017-06-06 | 李肥生 | For the coupling device of plant extract |
| CN112794929A (en) * | 2021-01-25 | 2021-05-14 | 西藏天虹科技股份有限责任公司 | Highland barley beta-glucan extraction process based on ultrasonic assistance |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190424 Address after: 410013 No. 178 Changxing Road, Furong District, Changsha City, Hunan Province Patentee after: Hunan Longtai Environmental Energy Technology Co., Ltd. Address before: 410126 Zhanggongling Longping High-tech Park, Furong District, Changsha City, Hunan Province, 178 Changxing Road Patentee before: ChangSha SYNO-THERM Co., Ltd. |
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| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131204 Termination date: 20180618 |
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| CF01 | Termination of patent right due to non-payment of annual fee |